Equipment and method for producing polyhydroxycarboxylic acid
    92.
    发明授权
    Equipment and method for producing polyhydroxycarboxylic acid 有权
    多羟基羧酸的制备方法和设备

    公开(公告)号:US08153754B2

    公开(公告)日:2012-04-10

    申请号:US12544477

    申请日:2009-08-20

    Abstract: An equipment for producing polyhydroxycarboxylic acid, includes a ring-opening polymerization apparatus, a liquid phase devolatilizing apparatus, and a drying apparatus, wherein an indirect heat exchanger is connected to a vent gas discharge path of the liquid phase devolatilizing apparatus. The indirect heat exchanger captures a dispersed in-process substance containing hydroxycarboxylic acid cyclic dimers and transfers the substance to the ring-opening polymerization apparatus; a wet condenser and a hot well are connected to a vent gas discharge path of the indirect heat exchanger and that of the drying apparatus, respectively. The wet condenser captures a dispersed in process substance containing the cyclic dimers with the use of a refrigerant containing hydroxycarboxylic acid corresponding to the cyclic dimers and transfers the substance to the hot well; the hot well causes hydrolysis of the cyclic dimers for generation of hydroxycarboxylic acid; the generated hydroxycarboxylic acid is mixed with a refrigerant and the mixture is circulated to the wet condenser; and hydroxycarboxylic acid is highly concentrated via circulation between the wet condenser and the hot well and then discharged.

    Abstract translation: 用于制备聚羟基羧酸的设备包括开环聚合设备,液相脱挥发酵设备和干燥设备,其中间接热交换器连接到液相脱挥发设备的通气气体排放路径。 间接热交换器捕获含有羟基羧酸环二聚体的分散的在线物质并将物质转移到开环聚合装置中; 湿式冷凝器和热井分别连接到间接热交换器和干燥装置的排放气体排出路径。 湿式冷凝器使用含有对应于环状二聚体的羟基羧酸的制冷剂捕获含有环状二聚体的分散过程物质,并将物质转移到热井中; 热阱引起环状二聚体的水解产生羟基羧酸; 将所生成的羟基羧酸与制冷剂混合,并将混合物循环至湿式冷凝器; 并且羟基羧酸通过湿式冷凝器和热井之间的循环高度浓缩,然后排出。

    DEVICE FOR CARRYING OUT CHEMICAL REACTIONS UNDER HOMOGENOUS AND HETEROGENOUS CONDITIONS
    93.
    发明申请
    DEVICE FOR CARRYING OUT CHEMICAL REACTIONS UNDER HOMOGENOUS AND HETEROGENOUS CONDITIONS 有权
    在均质和异质条件下进行化学反应的装置

    公开(公告)号:US20120077992A1

    公开(公告)日:2012-03-29

    申请号:US13376434

    申请日:2010-06-14

    Abstract: The present invention relates to a device for treatment of material transported through the device comprising at least one porous element consisting of solid, for example metallic, structure which allows cross-flow of the material through the porous element. The invention also relates to various types of uses of the device. A device in accordance with the invention is particularly useful to carry out chemical reactions under homogenous and heterogeneous conditions. Such a device hereinafter also referred as reactor may comprises a tube (1) having a cylindrical wall (2) with one inlet end (3) and one outlet end (4). Arranged in the tube (1) is at least one cylindrical porous element (5) consisting of solid metal structure, wherein said porous element (5) comprises a plurality of hollow spaces that are connected to each other and form an interconnected cavity network and wherein the at least one porous element (5) and the cylindrical wall (2) are made in one piece. The porosity ε of the at least one porous element (5) is between 0.8 and 0.95.

    Abstract translation: 本发明涉及一种用于处理通过该装置输送的材料的装置,包括至少一个多孔元件,该多孔元件由固体例如金属结构构成,其允许材料跨过多孔元件的交叉流动。 本发明还涉及该装置的各种用途。 根据本发明的装置特别可用于在同质和异质条件下进行化学反应。 以下也称为反应器的这种装置可以包括具有带有一个入口端(3)和一个出口端(4)的圆柱形壁(2)的管(1)。 在管(1)中布置的是由固体金属结构构成的至少一个圆柱形多孔元件(5),其中所述多孔元件(5)包括彼此连接并形成互连腔网络的多个中空空间,并且其中 至少一个多孔元件(5)和圆柱形壁(2)制成一体。 孔隙度 的至少一个多孔元件(5)在0.8和0.95之间。

    SILICON MANUFACTURING APPARATUS AND SILICON MANUFACTURING METHOD
    94.
    发明申请
    SILICON MANUFACTURING APPARATUS AND SILICON MANUFACTURING METHOD 审中-公开
    硅制造设备和硅制造方法

    公开(公告)号:US20120063985A1

    公开(公告)日:2012-03-15

    申请号:US13321574

    申请日:2010-05-19

    Abstract: In a silicon manufacturing apparatus and its related manufacturing method, a zinc gas supply opening (18b, 180b, 181b, 182b, 183b, 184b, 185b, 280a) is placed above a silicon tetrachloride gas opening (16a, 160a). A part of a reactor (10, 100), heated by a heater (22), is set to a silicon depositing temperature range, during which silicon tetrachloride gas is supplied from the silicon tetrachloride gas opening to the reactor to which zinc gas is supplied from the zinc gas supply opening, whereby silicon tetrachloride is reduced with zinc in the reactor to form a silicon depositing region (S), in which silicon is deposited on a wall portion in the reactor corresponding to a region thereof that is set to the silicon depositing temperature range.

    Abstract translation: 在硅制造装置及其相关的制造方法中,在四氯化硅气体开口(16a,160a)的上方设置有锌气体供给开口(18b,180b,181b,182b,183b,184b,185b,280a)。 由加热器(22)加热的反应器(10,100)的一部分被设定为硅沉积温度范围,在此期间,四氯化硅气体从四氯化硅气体开口供应到供应有锌气体的反应器 从锌气体供给口开始,由于四氯化硅在反应器中用锌还原以形成硅沉积区域(S),其中硅沉积在反应器的壁部分上,对应于其设置于硅的区域 沉积温度范围。

    Optimized liquid-phase oxidation
    97.
    发明授权
    Optimized liquid-phase oxidation 有权
    优化液相氧化

    公开(公告)号:US08114356B2

    公开(公告)日:2012-02-14

    申请号:US12490442

    申请日:2009-06-24

    Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

    Abstract translation: 公开了一种用于更有效和经济地进行可氧化化合物的液相氧化的优化方法和装置。 这种液相氧化在气泡塔反应器中进行,其在相对低的温度下提供高效反应。 当氧化的化合物是对二甲苯并且来自氧化反应的产物是粗对苯二甲酸(CTA)时,可以通过更经济的技术将这种CTA产物纯化和分离,如果CTA通过常规的高温 氧化过程。

    Injector assemblies and microreactors incorporating the same
    98.
    发明授权
    Injector assemblies and microreactors incorporating the same 有权
    引入组件和包括其的微反应器

    公开(公告)号:US08101128B2

    公开(公告)日:2012-01-24

    申请号:US12396114

    申请日:2009-03-02

    Abstract: A microreactor assembly is provided comprising a fluidic microstructure and an injector assembly. The injector assembly comprises a liquid inlet, a gas inlet, a liquid outlet, a gas outlet, a liquid flow portion extending from the liquid inlet to the liquid outlet, and a gas flow portion extending from the gas inlet to the gas outlet. Further, the injector assembly defines an injection interface with a microchannel input port of the fluidic microstructure. The injector assembly is configured such that the gas outlet of the gas flow portion is positioned to inject gas into the liquid flow portion upstream of the liquid outlet, into the liquid flow portion at the liquid outlet, or into an extension of the liquid flow portion downstream of the liquid outlet and is configured such that gas is injected into the liquid flow portion or the extension thereof as a series of gas bubbles.

    Abstract translation: 提供了包括流体微结构和喷射器组件的微反应器组件。 喷射器组件包括液体入口,气体入口,液体出口,气体出口,从液体入口延伸到液体出口的液体流动部分,以及从气体入口延伸到气体出口的气体流动部分。 此外,喷射器组件限定了与流体显微组织的微通道输入端口的注入界面。 喷射器组件被构造成使得气体流动部分的气体出口定位成将气体注入到液体出口上游的液体流动部分中,在液体出口处进入液体流动部分,或者进入液体流动部分的延伸部分 在液体出口的下游并且被配置为使得气体作为一系列气泡注入到液体流动部分或其延伸部分中。

    LDPE TUBULAR REACTOR PEROXIDE MIXER
    99.
    发明申请
    LDPE TUBULAR REACTOR PEROXIDE MIXER 审中-公开
    低密度聚乙烯管状反应器过氧化物混合器

    公开(公告)号:US20110278379A1

    公开(公告)日:2011-11-17

    申请号:US13143571

    申请日:2010-02-04

    Abstract: An initiator injection nozzle for mixing an initiator with a process fluid, comprising: a body comprising an inlet port to receive the process fluid, an outlet port, and an injector inlet to receive initiator; a process fluid flow passage through which the process fluid traverses between the inlet port and outlet port along a central process flow axis, further comprising a constricting portion, a throat, and an expanding portion in that order, —an initiator fluid flow passage through which the initiator traverses between the injector inlet and injector outlet along an injector central vertical axis, where the initiator fluid flow passage intersects the process fluid flow passage in the constricting portion; a stylus at least partially containing the initiator fluid flow passage and further comprising a shaped injector tip forming the injector outlet of the initiator fluid flow passage; where the injector outlet is located in the constricting portion of the process fluid flow passage and upstream of the throat by a horizontal offset as determined along the central process flow axis; and where the injector outlet is located off the central process flow axis by a vertical offset as determined along the injector central vertical axis

    Abstract translation: 一种用于将引发剂与过程流体混合的引发剂喷嘴,包括:主体,其包括用于接收过程流体的入口端口,出口端口和用于接收引发器的注射器入口; 工艺流体流动通道,工艺流体沿着中心工艺流动轴线在入口端口和出口端口之间穿过该过程流体流道,还包括收缩部分,喉部和膨胀部分,该顺序为:起始物流体流动通道, 引发器沿注射器中心垂直轴在注射器入口和注射器出口之间穿过,其中引发剂流体流动通道与收缩部分中的过程流体流动通道相交; 至少部分地包含所述引发剂流体流动通道的触针,并且还包括形成所述引发剂流体流动通道的喷射器出口的成形喷射器尖端; 其中喷射器出口位于过程流体流动通道的收缩部分中并且沿着中心过程流动轴线确定的水平偏移位于喉部的上游; 并且其中喷射器出口沿着喷射器中心垂直轴线确定的垂直偏移位于中心过程流动轴线之外

    NANOPARTICLE MANUFACTURING DEVICE AND NANOPARTICLE MANUFACTURING METHOD AND METHOD OF MANUFACTURING NANOPARTICLE-DISPERSED LIQUID ALKALI METAL
    100.
    发明申请
    NANOPARTICLE MANUFACTURING DEVICE AND NANOPARTICLE MANUFACTURING METHOD AND METHOD OF MANUFACTURING NANOPARTICLE-DISPERSED LIQUID ALKALI METAL 审中-公开
    纳米材料制造装置和纳米材料制造方法及制备纳米颗粒分散液体碱金属的方法

    公开(公告)号:US20110209578A1

    公开(公告)日:2011-09-01

    申请号:US13014120

    申请日:2011-01-26

    Abstract: A nanoparticle manufacturing device capable of particle size control of nanoparticles made of a raw material metal powder and control of the occurrence condition of chaining of nanoparticles and of necking. The device 1 is provided for manufacturing nanoparticles by heating and melting a mixture of a raw material metal powder and a carrier gas in a heating space, cooling the mixture in a cooling space and collecting the mixture in a collection space. The heating space, the cooling space and the collection space form a continuous flow path without a back flow, and the cross-sectional area of the collection space is set at a large value compared to the cross-sectional area of the heating space and the cooling space. Further, there is provided a method of manufacturing a nanoparticle-dispersed liquid alkali metal by dispersing nanoparticles in a liquid alkali metal. A liquid alkali metal obtained by dispersing nanoparticles in the liquid alkali metal is manufactured by performing a rough dispersion step of stirring nanoparticles in the liquid alkali metal by a physical effect and a dispersion step of dispersing nanoparticles in the liquid alkali metal by irradiating the liquid alkali metal with ultrasonic waves after the rough dispersion step.

    Abstract translation: 一种纳米颗粒制造装置,其能够对由原料金属粉末制成的纳米颗粒进行粒度控制,并且控制纳米颗粒的链接和颈缩的发生状况。 设备1用于通过在加热空间中加热和熔化原料金属粉末和载气的混合物来制造纳米颗粒,在冷却空间中冷却混合物并将混合物收集在收集空间中。 加热空间,冷却空间和收集空间形成连续的流动路径而没有回流,并且与加热空间的横截面积相比,收集空间的横截面面积被设定为大的值, 冷却空间。 此外,提供了通过将纳米颗粒分散在液态碱金属中制造分散纳米颗粒的液态碱金属的方法。 通过将液态碱金属中的纳米粒子分散在液态碱金属中而得到的液态碱金属是通过进行通过物理效应搅拌纳米颗粒的分散步骤和通过照射液态碱将纳米颗粒分散在液态碱金属中的分散步骤来制备的 在粗分散步骤之后用超声波金属。

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