Abstract:
An enclosure includes at least one packed bed and a mixture supply line for delivering at the bottom of the enclosure a mixture of a liquid with a gas. The enclosure includes a system for separating the liquid phase and the gas phase of the mixture, the system being arranged between the bed and the mixture supply line, and this system including a housing having a flow passage for the degassed liquid and discharge passages for the disengaged gas.
Abstract:
An equipment for producing polyhydroxycarboxylic acid, includes a ring-opening polymerization apparatus, a liquid phase devolatilizing apparatus, and a drying apparatus, wherein an indirect heat exchanger is connected to a vent gas discharge path of the liquid phase devolatilizing apparatus. The indirect heat exchanger captures a dispersed in-process substance containing hydroxycarboxylic acid cyclic dimers and transfers the substance to the ring-opening polymerization apparatus; a wet condenser and a hot well are connected to a vent gas discharge path of the indirect heat exchanger and that of the drying apparatus, respectively. The wet condenser captures a dispersed in process substance containing the cyclic dimers with the use of a refrigerant containing hydroxycarboxylic acid corresponding to the cyclic dimers and transfers the substance to the hot well; the hot well causes hydrolysis of the cyclic dimers for generation of hydroxycarboxylic acid; the generated hydroxycarboxylic acid is mixed with a refrigerant and the mixture is circulated to the wet condenser; and hydroxycarboxylic acid is highly concentrated via circulation between the wet condenser and the hot well and then discharged.
Abstract:
The present invention relates to a device for treatment of material transported through the device comprising at least one porous element consisting of solid, for example metallic, structure which allows cross-flow of the material through the porous element. The invention also relates to various types of uses of the device. A device in accordance with the invention is particularly useful to carry out chemical reactions under homogenous and heterogeneous conditions. Such a device hereinafter also referred as reactor may comprises a tube (1) having a cylindrical wall (2) with one inlet end (3) and one outlet end (4). Arranged in the tube (1) is at least one cylindrical porous element (5) consisting of solid metal structure, wherein said porous element (5) comprises a plurality of hollow spaces that are connected to each other and form an interconnected cavity network and wherein the at least one porous element (5) and the cylindrical wall (2) are made in one piece. The porosity ε of the at least one porous element (5) is between 0.8 and 0.95.
Abstract:
In a silicon manufacturing apparatus and its related manufacturing method, a zinc gas supply opening (18b, 180b, 181b, 182b, 183b, 184b, 185b, 280a) is placed above a silicon tetrachloride gas opening (16a, 160a). A part of a reactor (10, 100), heated by a heater (22), is set to a silicon depositing temperature range, during which silicon tetrachloride gas is supplied from the silicon tetrachloride gas opening to the reactor to which zinc gas is supplied from the zinc gas supply opening, whereby silicon tetrachloride is reduced with zinc in the reactor to form a silicon depositing region (S), in which silicon is deposited on a wall portion in the reactor corresponding to a region thereof that is set to the silicon depositing temperature range.
Abstract:
A method of assembling an injection device for use in a reactor injector feed assembly includes coupling a plurality of substantially concentric conduits to a modular tip. The method also includes coupling a first conduit of the reactor injector feed assembly to a modular tip and coupling a second conduit of the reactor injector feed assembly to the modular tip. The modular tip includes a first substantially annular nozzle and a second substantially annular nozzle defined therein. The first conduit and the first substantially annular nozzle are centered about an injection device centerline.
Abstract:
An SNCR distribution grid for introducing a NOx reducing reactant into a flue gas flow. The grid is made of one or more elements which are formed by fluid-cooled tubes to which membrane pieces are attached, preferably by welding, to form conduits in between the tubes. The fluid-cooled tubes may be cooled by water and/or steam and the distribution grid is disposed in the flue gas flow. To admit the reactant into the flue gas, nozzles are provided in the membrane and the reactant is conveyed from a location external of the furnace or combustor enclosure, into the conduits so formed, and thence out into the Flue gas flow via the nozzles.
Abstract:
Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.
Abstract:
A microreactor assembly is provided comprising a fluidic microstructure and an injector assembly. The injector assembly comprises a liquid inlet, a gas inlet, a liquid outlet, a gas outlet, a liquid flow portion extending from the liquid inlet to the liquid outlet, and a gas flow portion extending from the gas inlet to the gas outlet. Further, the injector assembly defines an injection interface with a microchannel input port of the fluidic microstructure. The injector assembly is configured such that the gas outlet of the gas flow portion is positioned to inject gas into the liquid flow portion upstream of the liquid outlet, into the liquid flow portion at the liquid outlet, or into an extension of the liquid flow portion downstream of the liquid outlet and is configured such that gas is injected into the liquid flow portion or the extension thereof as a series of gas bubbles.
Abstract:
An initiator injection nozzle for mixing an initiator with a process fluid, comprising: a body comprising an inlet port to receive the process fluid, an outlet port, and an injector inlet to receive initiator; a process fluid flow passage through which the process fluid traverses between the inlet port and outlet port along a central process flow axis, further comprising a constricting portion, a throat, and an expanding portion in that order, —an initiator fluid flow passage through which the initiator traverses between the injector inlet and injector outlet along an injector central vertical axis, where the initiator fluid flow passage intersects the process fluid flow passage in the constricting portion; a stylus at least partially containing the initiator fluid flow passage and further comprising a shaped injector tip forming the injector outlet of the initiator fluid flow passage; where the injector outlet is located in the constricting portion of the process fluid flow passage and upstream of the throat by a horizontal offset as determined along the central process flow axis; and where the injector outlet is located off the central process flow axis by a vertical offset as determined along the injector central vertical axis
Abstract:
A nanoparticle manufacturing device capable of particle size control of nanoparticles made of a raw material metal powder and control of the occurrence condition of chaining of nanoparticles and of necking. The device 1 is provided for manufacturing nanoparticles by heating and melting a mixture of a raw material metal powder and a carrier gas in a heating space, cooling the mixture in a cooling space and collecting the mixture in a collection space. The heating space, the cooling space and the collection space form a continuous flow path without a back flow, and the cross-sectional area of the collection space is set at a large value compared to the cross-sectional area of the heating space and the cooling space. Further, there is provided a method of manufacturing a nanoparticle-dispersed liquid alkali metal by dispersing nanoparticles in a liquid alkali metal. A liquid alkali metal obtained by dispersing nanoparticles in the liquid alkali metal is manufactured by performing a rough dispersion step of stirring nanoparticles in the liquid alkali metal by a physical effect and a dispersion step of dispersing nanoparticles in the liquid alkali metal by irradiating the liquid alkali metal with ultrasonic waves after the rough dispersion step.