Abstract:
The present invention relates to a process for reacting ammonia and wet process phosphoric acid to produce ammonium phosphates, which process comprises feeding the reagents to a vessel comprising two tubular members in fluid flow communication with one another and with a gas disengagement vessel, at least one of said tubular members being generally upright, the ammonia being fed to the basal portion of the upright member, the phosphoric acid being fed to the other tubular member; allowing the resultant reaction mixture to circulate spontaneously up the upright member, through the gas disengagement vessel and through the other member to the upright member; and recovering the ammonium phosphate reaction products from the reaction system.
Abstract:
The present disclosure relates to an apparatus for preparing an oligomer, the apparatus including: a reactor for oligomerizing a feed stream containing a fed monomer; a stirrer inserted into a hole formed in an upper portion of the reactor; and a solvent transfer line extending inward from a side of the reactor, wherein the stirrer includes a rotating shaft vertically extending downward from the upper portion of the reactor, and a blade having a conical shape whose vertex is positioned at a lower end of the rotating shaft and outer diameter increases from a bottom toward a top, and the solvent transfer line has a plurality of spray nozzles formed in a direction toward the blade.
Abstract:
A sparge for use in a high-pressure vessel operated at elevated temperatures and having high energy agitators for suspending mineral containing particles in a slurry. The sparge injects reagent fluids into the slurry to reduce reaction times and for controlling process parameters for extracting valuable minerals from the particles. The sparge has a vapor lock to inhibit the flow of particulate material and detritus material under low or no fluid flow situations which occur commonly in the operation of high pressure autoclaves. The sparge has a fluid flow path that increases in cross-sectional area in the direction of flow of reagent fluids so as to keep reagent fluids flowing at a velocity below a critical impingement velocity that can cause metal materials of the sparge to either wear rapidly, combust and in the worst case lead to loss of containment and violent and rapid depressurization of the high pressure vessel.
Abstract:
The present invention relates to a fluidized bed gas distribution nozzle with the following features in its functional position: a gas inlet pipe (10), having: an inner surface (10i), an outer surface (10o), a lower end section (10l) adapted to receive gas from an associated gas source, an upper end section (10u), a plurality of openings (12) formed in the upper end section (10u), each opening (12) extending form the inner surface (10i) of the gas inlet pipe (10) to the outer surface (10o) of the gas inlet pipe (10), a gas distribution cap (20) connected or connectable to the gas inlet pipe (10), having: an upper top (20u), a lower bottom (20l) arranged at a vertical distance below said upper top (20u) and surrounding the gas inlet pipe (10), a peripheral wall (20w) having an inner surface (20i) and an outer surface (20o) and extending between said upper top (20u) and said lower bottom (20l), outlets (22) within the peripheral wall (20w) extending from the inner surface (20i) of the peripheral wall (20w) to the outer surface (20o) of the peripheral wall (20w).
Abstract:
A reactor tank is provided having an enzyme inlet, a heating jacket positioned around the exterior center of the tank, a gas outlet for communicating with a vacuum apparatus to create a vacuum within the reactor tank and for communicating with a condensing unit, a first gas inlet for receiving gas from a feed tank and a first liquid outlet for recirculating the liquid from the first liquid outlet back to the feed tank. The reactor tank further includes a sparged unit and a screen positioned within the tank between the sparged unit and the first liquid outlet, where the sparged unit is connected to the first gas inlet for receiving gas from the feed tank. The reactor tank is utilized in a reactor system further including a condensing unit, vacuum pump or venturi valve, a first feed tank connected to the first gas inlet, a coalescer having at least one circulation pipe and a first circulation pump connected to the first liquid outlet for circulating a portion of the liquid dispelled from the liquid outlet to the coalescer, which after being filtered through coalescer is recirculated through circulation pipe back to the first feed tank.
Abstract:
The present invention discloses a hydrogen sulfide reactor vessel with an external heating system that is conductively and removably attached to an exterior portion of the reactor vessel. Also disclosed are processes for producing hydrogen sulfide utilizing the reactor vessel.
Abstract:
The present invention relates to a fluidized bed system having a sparger capable of minimizing a blockage by solids and controlling method thereof. And, more specifically, the present invention relates to a fluidized bed system having a sparger capable of minimizing a blockage by solids comprising a fluidized bed reactor to store a solid layer with a certain height and to fluidize the solid layer by using fluidization gases; a sparger having a pipe shape submerged in the solid layer and having a plurality of gas-discharging holes to spray fluidization gases onto the solid layer; and a gas-supplying line having its one end contacting a gas-supplying source and the other end connected to the sparger, wherein fluidization gases are introduced through the gas-supplying line into the sparger by driving the gas-supplying source, the fluidization gases are sprayed through the gas-discharging holes onto the solid layer, the gas-supplying source is placed higher than the sparger and the height difference (Hg) between the gas-supplying source and the sparger is greater than the height of the solid layer.
Abstract:
The present invention relates to a multiple-bed downflow reactor comprising vertically spaced beds of solid contact material and a mixing device positioned in an inter bed space between adjacent beds. The mixing device comprises a loop of first nozzles distributed around a vertical axis and arranged for ejecting a fluid in a first ejection direction into said inter bed space, on the one hand, and a loop of second nozzles distributed around the vertical axis and arranged for ejecting a fluid in a second ejection direction into said inter bed space, on the other hand. The first ejection direction is directed inwardly with respect to the loop of first nozzles. The second ejection direction is directed outwardly with respect to the loop of second nozzles.