Abstract:
The invention proceeds from a vacuum process apparatus for an article which is processed or treated, resp. at two stations, whereby each station has a charging and/or removing opening for the article. A transporting device is supported for rotation and includes a supporting portion which is successively moved onto the openings of the stations. The process plant is designed in such a manner that the surface normals determined by the surfaces of the openings and the space axis defined by the axis of rotation of the transport device do not run parallel and rather enclose together an angle of 90.degree. or 45.degree.. By such an arrangement it is possible to design extremely compact vacuum vapor deposition apparatuses having a plurality of individual stations, whereby additionally short transporting distances are obtainable and the volumes to be conditioned can be minimized.
Abstract:
The present invention relates to a process and a device for introducing a catalytically active powder into a reactor (20) for gas phase alpha-olefin polymerization. The device comprises a storage vessel (3) containing the powder, a metering valve (4) delivering metered quantities of the powder into an intermediate chamber (5) comprising at least one obstacle (6) separating an upper part (5a) of the chamber (5) comprising an auxiliary gas inlet (2a) from a lower part (5b) terminated by an outlet orifice (5c). A connecting pipe (18) connects the outlet orifice (5c) to a mixing device (8) situated on a conveying pipework (15) communicating with the reactor (20). The powder is introduced into the reactor in a dilute suspension form and in a more uniform rate.
Abstract:
An apparatus and process for maintaining the purity of solid/granular product and dispensing high purity granular product from a vessel. A noncontaminating surface is provided by a cup, cylinder, or other structure having a surface of silicon, silicon carbide, silicon nitride, sialon, or similar materials and preferably operates as an angle of repose valve in a pressurized system to prevent contamination by undue contact of the high purity product with conventional gastight valves such as ball valves, butterfly valves, pinch valves, etc.
Abstract:
The invention relates to a method and device for feeding a mud-like catalyst mixture into a polymerization reactor. The catalyst mixture is fed from a container into a batching space of a feeder connected thereto, from which channel the catalyst mixture is further fed by batches into the polymerization reactor by the use of the pressure of a medium fed into the feeder. In accordance with the invention, after each catalyst batch fed into the polymerization reactor, the medium is substantially removed from the batching space of the feeder by leading the medium via an outlet channel into a space between two on/off valves before filling the batching space with a new catalyst batch.
Abstract:
A vaporizer and extractor apparatus for a laser isotope separation process is arranged as an assemblage of modular components in which equipment subject to maintenance is replaceable via vacuum casks while the apparatus is operational or briefly shut down without loss of vacuum. A vacuum transfer cask is provided for modular extractor substrate assemblies. The substrate assemblies are nestable and are mounted on extensible probes which permit them to be nested in the vacuum transfer cask for transport. During use the substrates extend from the cask, through a vacuum lock and are placed side by side in the vacuum chamber. A vacuum transfer cask is also provided for the vaporizer assembly which is mounted on an extensible arm which in turn positions the assembly in the chamber or retraces the vaporizer assembly from the chamber into the transfer cask, rotating it during the process in order to permit it to fit into the cask. The complete vaporizer unit consisting of a crucible, two electron beam guns, a combination thermal/vapor shield and an electrical ground plate along with the associated cooling and electrical services is suspended from the extensible arm out of the vacuum transfer cask.
Abstract:
A transfer vessel for transporting a specimen between two vacuum apparatuses while maintaining the specimen under a high vacuum. The device has a hermetic container for accommodating a specimen removed from a vacuum apparatus and for supporting the specimen. A pressure reducing device reduces the pressure in the hermetic container by adsorbing a gaseous matter contained therein.
Abstract:
A reaction product is formed by a process which involves the transfer of the reaction product from the autoclave to a receiving vessel at a substantially constant flow rate. Just prior to this transfer, the pressure in the receiving vessel is brought up to the pressure in the autoclave by passing gas from the autoclave to the receiving vessel. The flow of gas from the autoclave to the receiving vessel is then stopped, and the pressure in the receiving vessel is allowed to drop due to transfer of heat from the gas to the walls of the receiving vessel. The resulting pressure difference between the autoclave and the receiving vessel is used to initiate the transfer of the reaction products from the autoclave to the receiving vessel. A pressure release valve on the receiving vessel is then controlled by means a signal derived from a flow meter which measures the flow rate of the reaction products flowing from the autoclave to the receiving vessel to maintain constant this flow rate.
Abstract:
A method of forming titanium calcium oxide is disclosed comprising the steps of mixing titanium hydroxide, calcium hydroxide, and water in an autoclave, then heating these reaction constituents at a selected temperature and pressure for a time to allow the formation of titanium calcium oxide crystals of a desired size. Next, pressure in a receiving vessel is set below the pressure in the autoclave, and a valve is opened to allow the reaction product to flow from the autoclave to the receiving vessel at a constant flow rate. Heat is removed from the reaction product while the reaction product passes through a flow passage between the autoclave and the receiving vessel. This process can be modified to form zirconium calcium oxide.
Abstract:
Particulate solid fuel is conveyed from an atmospheric container into an atmospheric lock hopper which is then pressurized by a high pressure inert gas. The fuel is passed from the pressurized lock hopper into a pressure vessel and subsequently from this vessel into a gasification reactor. In the container and the lock hopper the solid fuel is fluidized by an inert gas. In the pressure vessel synthesis gas is used for this purpose, the latter gas also being applied for the pneumatic transport of the fuel from the vessel into the reactor.
Abstract:
An apparatus and method for stripping and depressurizing fine particulates mixed with gas discharged from a vessel operated at elevated temperature and pressure conditions to a low pressure vessel using a purge gas injected into a conduit designed for significant frictional pressure loss per unit length of conduit while maintaining a substantially constant velocity of the mixture conveyed.