Ni and Ni/NiO core-shell nanoparticles
    161.
    发明申请
    Ni and Ni/NiO core-shell nanoparticles 有权
    Ni和Ni / NiO核 - 壳纳米粒子

    公开(公告)号:US20070166455A1

    公开(公告)日:2007-07-19

    申请号:US11335211

    申请日:2006-01-19

    Abstract: Glycerol is used as a solvent medium for the precipitation of a complex of nickel and glycerol material. The precipitate is separated from the liquid solvent and dried and calcined in air to produce small (nanometer size) particles characterized by a nickel core encased in a nickel oxide shell. The proportions of nickel core and nickel oxide shell can be controlled by management of the time and temperature of heating in air. Prolonged heating in air can produce nickel oxide particles, or calcining of the precipitate in nitrogen produces nickel particles.

    Abstract translation: 甘油用作沉淀镍和甘油材料复合物的溶剂介质。 将沉淀物与液体溶剂分离并干燥并在空气中煅烧以产生特征在于包裹在氧化镍壳中的镍芯的小(纳米尺寸)颗粒。 可以通过管理空气中加热的时间和温度来控制镍芯和氧化镍壳的比例。 在空气中长时间加热可产生氧化镍颗粒,或在氮气中煅烧沉淀产生镍颗粒。

    Method of producing nanophase Cu-Al2O3 composite powder
    164.
    发明授权
    Method of producing nanophase Cu-Al2O3 composite powder 有权
    生产纳米相Cu-Al2O3复合粉末的方法

    公开(公告)号:US06521016B2

    公开(公告)日:2003-02-18

    申请号:US09827366

    申请日:2001-04-05

    Abstract: The present invention relates to a method of producing nanophase Cu—Al2O3 composite powder by means of 1) the producing precursor powders by centrifugal spray drying process using the water base solution, in which Cu-nitrate (Cu(NO3)23H2O) and Al-Nitrate (Al(NO3)39H2O) are solved to the point of final target composition (Cu-1 wt %/Al2O3),2) the heat treatment process (desaltation process) at the 850° C. for 30 min in air atmosphere to remove the volatile components such as the moisture and NO3 group in precursor powder and simultaneously to synthesize the nano CuO—Al2O3 composite powders by the oxidation of corresponded metal components and 3) the reduction heat treatment of CuO at 200° C. for 30 min in reducing atmosphere to produce the final nanophase Cu—Al2O3 composite powders with the size below 20 nm.

    Abstract translation: 本发明涉及一种通过以下方法制备纳米相Cu-Al2O3复合粉末的方法:1)使用水溶液进行离心喷雾干燥处理制备前体粉末,其中硝酸铜(Cu(NO 3)23H 2 O)和Al- 将硝酸盐(Al(NO 3)3·3H 2 O)溶解到最终目标组成(Cu-1重量%/ Al 2 O 3)的点,2)在空气气氛中在850℃下热处理(脱盐处理)30分钟, 去除前体粉末中挥发性成分如水分和NO3基团,同时通过相应金属组分的氧化合成纳米CuO-Al2O3复合粉末; 3)CuO在200℃下还原热处理30分钟 还原气氛,生产尺寸在20nm以下的最终纳米相Cu-Al2O3复合粉末。

    Metal nickel powder
    165.
    发明授权
    Metal nickel powder 有权
    金属镍粉

    公开(公告)号:US06391084B1

    公开(公告)日:2002-05-21

    申请号:US09508820

    申请日:2000-03-29

    Abstract: The present invention provide metallic nickel powder in which the occurrence of delaminatoin can be prevented by providing superior sintering propreties in production processes for multilayer ceramic capacitors and by providind superior dispersion characteristics in the forming of conductive pastes. By being brought into contact with nickel chloride gas and a reducing gas at a temperature in the range of the reduction reaction, metallic nickel power is node gas and a reducing gas at a produced in which the oxigen content is 0.1 to 2.0% by weight and there is not absortion peak at wavelengths ranging from 3600 to 3700 cm−1 in infrared spectroscopy.

    Abstract translation: 本发明提供金属镍粉末,其中通过在多层陶瓷电容器的制造方法中提供优异的烧结性能并且在形成导电浆料中提供优异的分散特性,可以防止脱层的发生。 通过在还原反应范围内的温度下与氯化镍气体和还原气体接触,金属镍电力是生成的氧化物含量为0.1〜2.0重量%的节点气体和还原气体, 红外光谱中波长3600〜3700cm-1处不存在绝缘峰。

    Method of producing nanophase Cu-Al2O3 composite power
    166.
    发明申请
    Method of producing nanophase Cu-Al2O3 composite power 有权
    生产纳米相Cu-Al2O3复合电力的方法

    公开(公告)号:US20010054328A1

    公开(公告)日:2001-12-27

    申请号:US09827366

    申请日:2001-04-05

    Abstract: The present invention relates to a method of producing nanophase CunullAl2O3 composite powder by means of 1) the producing precursor powders by centrifugal spray drying process using the water base solution, in which Cu-nitrate (Cu(NO3)23H2O) and Al-Nitrate (Al(NO3)39H2O) are solved to the point of final target composition (Cu-1 wt %/Al2O3),2) the heat treatment process (desaltation process) at the 850null C. for 30 min in air atmosphere to remove the volatile components such as the moisture and NO3 group in precursor powder and simultaneously to synthesize the nano CuOnullAl2O3 composite powders by the oxidation of corresponded metal components and 3) the reduction heat treatment of CuO at 200null C. for 30 min in reducing atmosphere to produce the final nanophase CunullAl2O3 composite powders with the size below 20 nm.

    Abstract translation: 本发明涉及一种通过以下方法制备纳米相Cu-Al2O3复合粉末的方法:1)使用水溶液进行离心喷雾干燥处理制备前体粉末,其中硝酸铜(Cu(NO 3)23H 2 O)和Al- 将硝酸盐(Al(NO 3)3·3H 2 O)溶解到最终目标组成(Cu-1重量%/ Al 2 O 3)的点,2)在空气气氛中在850℃下热处理(脱盐处理)30分钟, 去除前体粉末中挥发性成分如水分和NO3基团,同时通过相应金属组分的氧化合成纳米CuO-Al2O3复合粉末; 3)CuO在200℃下还原热处理30分钟 还原气氛,生产尺寸在20nm以下的最终纳米相Cu-Al2O3复合粉末。

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