Abstract:
Glycerol is used as a solvent medium for the precipitation of a complex of nickel and glycerol material. The precipitate is separated from the liquid solvent and dried and calcined in air to produce small (nanometer size) particles characterized by a nickel core encased in a nickel oxide shell. The proportions of nickel core and nickel oxide shell can be controlled by management of the time and temperature of heating in air. Prolonged heating in air can produce nickel oxide particles, or calcining of the precipitate in nitrogen produces nickel particles.
Abstract:
A method for treating a porous item constructed of metal powder, such as a powder made of Series 400 stainless steel, involves a step of preheating the porous item to a temperature of between about 700 and 900° C. degrees in an oxidizing atmosphere and then sintering the body in an inert or reducing atmosphere at a temperature which is slightly below the melting temperature of the metal which comprises the porous item. The thermal stability of the resulting item is enhanced by this method so that the item retains its porosity and metallic characteristics, such as ductility, at higher (e.g. near-melting) temperatures.
Abstract:
Compositions containing non-evaporable getter alloys are provided which, after having lost their functionality in consequence of exposure to reactive gases at a first temperature, can then be reactivated by a thermal treatment at a second temperature that is lower than the first temperature.
Abstract:
The present invention relates to a method of producing nanophase Cu—Al2O3 composite powder by means of 1) the producing precursor powders by centrifugal spray drying process using the water base solution, in which Cu-nitrate (Cu(NO3)23H2O) and Al-Nitrate (Al(NO3)39H2O) are solved to the point of final target composition (Cu-1 wt %/Al2O3),2) the heat treatment process (desaltation process) at the 850° C. for 30 min in air atmosphere to remove the volatile components such as the moisture and NO3 group in precursor powder and simultaneously to synthesize the nano CuO—Al2O3 composite powders by the oxidation of corresponded metal components and 3) the reduction heat treatment of CuO at 200° C. for 30 min in reducing atmosphere to produce the final nanophase Cu—Al2O3 composite powders with the size below 20 nm.
Abstract translation:本发明涉及一种通过以下方法制备纳米相Cu-Al2O3复合粉末的方法:1)使用水溶液进行离心喷雾干燥处理制备前体粉末,其中硝酸铜(Cu(NO 3)23H 2 O)和Al- 将硝酸盐(Al(NO 3)3·3H 2 O)溶解到最终目标组成(Cu-1重量%/ Al 2 O 3)的点,2)在空气气氛中在850℃下热处理(脱盐处理)30分钟, 去除前体粉末中挥发性成分如水分和NO3基团,同时通过相应金属组分的氧化合成纳米CuO-Al2O3复合粉末; 3)CuO在200℃下还原热处理30分钟 还原气氛,生产尺寸在20nm以下的最终纳米相Cu-Al2O3复合粉末。
Abstract:
The present invention provide metallic nickel powder in which the occurrence of delaminatoin can be prevented by providing superior sintering propreties in production processes for multilayer ceramic capacitors and by providind superior dispersion characteristics in the forming of conductive pastes. By being brought into contact with nickel chloride gas and a reducing gas at a temperature in the range of the reduction reaction, metallic nickel power is node gas and a reducing gas at a produced in which the oxigen content is 0.1 to 2.0% by weight and there is not absortion peak at wavelengths ranging from 3600 to 3700 cm−1 in infrared spectroscopy.
Abstract:
The present invention relates to a method of producing nanophase CunullAl2O3 composite powder by means of 1) the producing precursor powders by centrifugal spray drying process using the water base solution, in which Cu-nitrate (Cu(NO3)23H2O) and Al-Nitrate (Al(NO3)39H2O) are solved to the point of final target composition (Cu-1 wt %/Al2O3),2) the heat treatment process (desaltation process) at the 850null C. for 30 min in air atmosphere to remove the volatile components such as the moisture and NO3 group in precursor powder and simultaneously to synthesize the nano CuOnullAl2O3 composite powders by the oxidation of corresponded metal components and 3) the reduction heat treatment of CuO at 200null C. for 30 min in reducing atmosphere to produce the final nanophase CunullAl2O3 composite powders with the size below 20 nm.
Abstract translation:本发明涉及一种通过以下方法制备纳米相Cu-Al2O3复合粉末的方法:1)使用水溶液进行离心喷雾干燥处理制备前体粉末,其中硝酸铜(Cu(NO 3)23H 2 O)和Al- 将硝酸盐(Al(NO 3)3·3H 2 O)溶解到最终目标组成(Cu-1重量%/ Al 2 O 3)的点,2)在空气气氛中在850℃下热处理(脱盐处理)30分钟, 去除前体粉末中挥发性成分如水分和NO3基团,同时通过相应金属组分的氧化合成纳米CuO-Al2O3复合粉末; 3)CuO在200℃下还原热处理30分钟 还原气氛,生产尺寸在20nm以下的最终纳米相Cu-Al2O3复合粉末。
Abstract:
A method for manufacturing a porous metal body according to the present invention includes: a surface oxidizing step of heating a titanium-containing powder in an atmosphere containing oxygen at a temperature of 250° C. or more for 30 minutes or more to provide a surface-oxidized powder; and a sintering step of depositing the surface-oxidized powder in a dry process, and sintering the surface-oxidized powder by heating it in a reduced pressure atmosphere or an inert atmosphere at a temperature of 950° C. or more.
Abstract:
A method of producing a phosphate-coated SmFeN-based anisotropic magnetic powder, the method including stirring a slurry containing a raw material SmFeN-based anisotropic magnetic powder, water, a phosphate source, and an aluminum source to obtain a SmFeN-based anisotropic magnetic powder having a surface coated with a phosphate.
Abstract:
A method produces a workpiece including molybdenum, or tungsten, or chromium, or molybdenum alloy, or tungsten alloy, or chromium alloy by selective consolidation of successive layers of powder by an energy beam. The method includes performing the selective consolidation of the powder layer in a protective atmosphere including nitrogen.
Abstract:
The permanent magnet comprises a main phase structure of R2T14B crystal grains, and R is a rare earth element; T comprises at least Mn, Fe, and optionally a transition metal comprising Co; B is boron; the permanent magnet further comprises Mn and heavy rare earth elements which are distributed in a grain boundary in a diffusion mode. The heavy rare earth element is selected from at least one selected from Dy, Ho and Tb. According to the rare earth permanent magnet prepared through the preparation method, more heavy rare earth elements can be diffused into the magnet core along the grain boundary, Hcj distribution of the permanent magnet is improved, and meanwhile the corrosion resistance and the mechanical property of the permanent magnet are improved.