Method of making a soot preform compositional profile
    172.
    发明授权
    Method of making a soot preform compositional profile 失效
    制作烟炱预制件成型轮廓的方法

    公开(公告)号:US4298365A

    公开(公告)日:1981-11-03

    申请号:US165652

    申请日:1980-07-03

    Abstract: A method of making solid glass articles by the flame hydrolysis technique. A thin stratum of low viscosity glass soot is applied to the surface of a mandrel. First and second coatings of glass soot are deposited on the surface of the thin stratum to form a porous preform. The refractive index of the soot particles of the first coating is greater than that of the soot of the second coating, and the soot of the first coating has a viscosity lower than that of the second coating. The mandrel is removed, and the soot preform is subjected to a high temperature whereby it is consolidated to form a dense glass blank. The glass surface tension and the relative viscosities of the inner and outer portions of the preform cause the aperture to close during the consolidation process. The thin stratum, which preferably includes P.sub.2 O.sub.5, smoothes over the damage caused by removing the mandrel and reduces or even eliminates seed formation at the axis of the resultant glass blank. The blank may be heated and drawn into a filament, or it may be sliced into optical windows, lenses or the like.

    Abstract translation: 通过火焰水解技术制备固体玻璃制品的方法。 将低粘度玻璃烟灰的薄层施加到心轴的表面。 玻璃烟灰的第一和第二涂层沉积在薄层的表面上以形成多孔预型体。 第一涂层的烟灰颗粒的折射率大于第二涂层的烟灰的折射率,第一涂层的烟灰的粘度低于第二涂层的烟灰。 去除心轴,并且将烟灰预制件经受高温,由此将其固结以形成致密的玻璃坯料。 预成型件的内部和外部的玻璃表面张力和相对粘度在固结过程中导致孔隙闭合。 优选地包括P2O5的薄层平滑了由去除心轴引起的损伤,并减少或甚至消除了在所得玻璃坯料的轴线处的种子形成。 坯料可以被加热并拉成长丝,或者可以将其切成光学窗口,透镜等。

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