ENDODONTIC FILES AND METHOD OF PREPARATION THEREOF
    11.
    发明申请
    ENDODONTIC FILES AND METHOD OF PREPARATION THEREOF 有权
    ENDODONTIC文件及其制备方法

    公开(公告)号:US20130177871A1

    公开(公告)日:2013-07-11

    申请号:US13806495

    申请日:2011-06-21

    CPC classification number: A61C5/023 A61C5/42 A61C2201/007

    Abstract: The present invention provides a selective coating of an endodontic file, in which the distal end of the file is uncoated or alternatively leaving the outermost part of the blades of the distal end portion uncoated. The distribution of the nanoparticles is thus non uniform along the surface of the file leaving only a part of the file coated. In the present invention, the distal end of the device being subjected to the highest torque is either uncoated at all, or has a coated core and uncoated blades.

    Abstract translation: 本发明提供了一种牙髓锉的选择性涂层,其中锉刀的远端未被涂覆或者替代地使远端部分的刀片的最外部分未涂覆。 因此,纳米颗粒的分布沿着文件的表面是不均匀的,仅留下文件的一部分。 在本发明中,受到最高扭矩的装置的远端完全没有涂覆,或者具有涂覆的芯和未涂覆的刀片。

    Oriented polycrystalline thin films of transition metal chalcogenides
    16.
    发明授权
    Oriented polycrystalline thin films of transition metal chalcogenides 失效
    过渡金属硫族化物的定向多晶薄膜

    公开(公告)号:US5958358A

    公开(公告)日:1999-09-28

    申请号:US657431

    申请日:1996-06-03

    CPC classification number: B82Y30/00 C30B25/02 C30B29/46 Y10S977/734

    Abstract: A method of preparing a polycrystalline thin film of a transition metal chalcogenide of an orientation on a substrate which includes (a) depositing a layer of a transition metal material or mixtures thereof on the substrate; and (b) heating the layer in an open system in a gaseous reducing atmosphere containing one or more chalcogen materials for a time sufficient to allow the transition metal material and the chalcogen material to react and form the oriented polycrystalline thin film, the thin film being substantially exclusively oriented in the orientation. Also provided is a method of synthesizing structures of a transition metal chalcogenide selected from the group consisting of single layer or nested or stuffed inorganic fullerenes and nanotubes, including the step of reacting a transition metal compound with a volatile chalcogen compound in a reducing atmosphere at a temperature between about 750.degree. C. and about 1000.degree. C.

    Abstract translation: 一种在衬底上制备取向的过渡金属硫属元素化物的多晶薄膜的方法,该方法包括:(a)在衬底上沉积一层过渡金属材料或其混合物; 和(b)在含有一种或多种硫族元素材料的气态还原气氛中在开放系统中加热所述层足够长的时间以允许过渡金属材料和硫属元素材料反应并形成定向多晶薄膜,所述薄膜为 基本上是专门定向的。 还提供了一种合成选自单层或嵌套或填充的无机富勒烯和纳米管的过渡金属硫族化物的结构的方法,包括在还原气氛中使过渡金属化合物与挥发性硫族化合物反应的步骤 约750℃至约1000℃的温度

    Process and apparatus for producing inorganic fullerene-like nanoparticles
    19.
    发明授权
    Process and apparatus for producing inorganic fullerene-like nanoparticles 有权
    用于生产无机富勒烯样纳米颗粒的方法和设备

    公开(公告)号:US07641886B2

    公开(公告)日:2010-01-05

    申请号:US11911095

    申请日:2006-04-06

    Abstract: The present invention provides a process for obtaining fullerene-like metal chalcogenide nanoparticles, comprising feeding a metal precursor (INi) selected from metal halide, metal carbonyl, organo-metallic compound and metal oxyhalide vapor into a reaction chamber (12) towards a reaction zone to interact with a flow of at least one chalcogen material (IN2) in gas phase, the temperature conditions in said reaction zone being such to enable the formation of the fullerene-like metal chalcogenide nanoparticles product. The present invention further provides novel IF metal chalcogenides nanoparticles with spherical shape and optionally having a very small or no hollow core and also exhibiting excellent tribological behavior. The present invention further provides an apparatus for preparing various IF nanostructures.

    Abstract translation: 本发明提供了一种获得类富含类金属硫族化物纳米颗粒的方法,包括将选自金属卤化物,金属羰基,有机金属化合物和金属卤氧化物蒸气的金属前体(INi)反馈入反应区 与气相中的至少一种硫属原料(IN2)的流动相互作用,所述反应区中的温度条件使得能够形成富勒烯样金属硫族化物纳米颗粒产物。 本发明还提供具有球形形状的新型IF金属硫族化物纳米颗粒,并且任选地具有非常小的或不具有中空的核心并且还表现出优异的摩擦学行为。 本发明还提供了一种用于制备各种IF纳米结构的装置。

    Method and apparatus for producing inorganic fullerene-like nanoparticles
    20.
    发明授权
    Method and apparatus for producing inorganic fullerene-like nanoparticles 有权
    用于生产无机富勒烯样纳米颗粒的方法和设备

    公开(公告)号:US07641869B2

    公开(公告)日:2010-01-05

    申请号:US11326462

    申请日:2006-01-06

    Abstract: A process and apparatus are presented for obtaining inorganic fullerene-like nanostructures. A metal oxide is evaporated at predetermined temperature conditions, and is swept towards a reacting zone, to which first and second gas phase reacting agents are concurrently swept. The evaporated metal oxide thus interacts with the first reacting agent and is converted into metal suboxide nanoparticles in the gas phase. The condensing metal suboxide nanoparticles interact with the second reacting agent in the gas phase resulting in substantially pure phase of the inorganic fullerene-like nanoparticles.

    Abstract translation: 提出了一种获得无机富勒烯样纳米结构的方法和装置。 金属氧化物在预定的温度条件下蒸发,并且朝向反应区扫过,第一和第二气相反应剂同时被扫过。 因此,蒸发的金属氧化物与第一反应剂相互作用并在气相中转化成金属低氧化物纳米颗粒。 冷凝金属低氧化物纳米颗粒在气相中与第二反应剂相互作用,导致无机富勒烯样纳米颗粒的基本上纯的相。

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