Abstract:
An improved process for the production of polyolefins in an autoclave reactor having several reaction zones operated at a pressure of 100 to 300 MPa and a temperature of 100 to 300.degree. C. is disclosed. Dunng operation, temperatures are measured continuously inside the autoclave reactor at specific points distributed along the reactor length, each of said measured temperatures is compared with a corresponding preset temperature and the detected deviation between each pair of preset and measured temperatures is used in regulating the amount of monomer and initiator fed into the autoclave through several feed inlets distributed along the reactor length, in order to minimize the temperature deviations and thus obtain an improved control of the polymerization process.
Abstract:
A high pressure and temperature microwave digestion vessel assembly with enhanced safety features is disclosed. The assembly includes a membrane that is rupturable for pressure relief, and a secondary pressure relief mechanism including a seal cap with an annular stress relief region that shears or fractures when excess pressure is in the vessel interior. The membrane is positioned on a post extending from the seal cap into the inner liner. The diameter of the venting orifice may be adjusted to vary the desired pressure relief. The assembly also includes a piercing mechanism for venting the vessel after digestion is completed.
Abstract:
Cellulosic material is converted to ethanol by hydrolyzing the cellulosic material in a gravity pressure vessel (50), and fermenting the product thereof. The gravity pressure vessel (50) employed is adapted to accommodate a continuous hydrolysis reaction and maximize the fermentable product yield on a commercial scale. The gravity pressure vessel (50) employed is also adapted to maximize the thermodynamic efficiencies of the hydrolysis reaction, as well as the entire ethanol producing process.
Abstract:
A method for making a unit including a pressure-sealed container (2) with at least one connecting port (3), and an active solid (1) placed in said container (2). The container (2) is formed directly on a preformed body of the active solid (1) and made of a material having a thermal conductivity of more than 18 W/m. K. The resulting units are particularly useful for making portable air-conditioning devices for garments.
Abstract:
A process for preparing and/or extracting samples by heating them together with a solvent in a container under pressure, using a Soxhlet apparatus. The samples are dried by heating in a container; and the resultant vapors are drawn off to generate a vacuum in the container.
Abstract:
An autoclave having end walls sturdily attached to one another by rods and a mobile, cylindrical lateral wall. When the lateral wall is moved into an operable position over the end walls, thereby sealing a working chamber defined between the end walls and when steam is introduced into the working chamber, each end wall will counteract pressure acting on its opposing counterpart. The autoclave need not be reinforced to hold the walls together. The rods connecting the end walls are hollow, and have ports disposed within the working chamber, so that steam may be introduced into the working chamber through these rods. Air from within the working chamber may also be vented by the rods. The lateral wall is vertically oriented and moved. A retaining wall traps condensate, which would otherwise escape when the lateral wall is lifted. An optional powered apparatus lifts and lowers the lateral wall into positions respectively exposing and sealing the working chamber. In a further option, the lateral wall is frustoconical rather than cylindrical, thereby avoiding sliding contact with the end walls.
Abstract:
There is provided a microwave waste sterilizer comprising an upper outer shell, a lower outer shell, an upper means for guiding microwave energy, a lower means for guiding microwave energy, an upper means for dispersing microwave energy, and a lower means for dispersing microwave energy. There is also provided a method for sterilizing waste materials with dual sources of microwave energy. Further there is provided a method for dispersing microwave energy into a chamber such that the dispersed microwave energy creates a flux field of substantially uniform flux.
Abstract:
A process and apparatus for the supercritical water oxidation of organic waste materials which avoids or at least substantially reduces the corrosion and solids deposition problems associated with prior art techniques and which provides for efficient heating of the waste material to reaction conditions. Externally heated supercritical water is fed to a compound platelet tube reactor. The compound reactor includes a reaction zone and inner (smaller) and outer (larger) concentric platelet tubes supported concentrically within a shell. The water fed to the reactor both protectively coats surfaces of the inner and outer platelet tubes facing the reaction zone and heats the waste stream to oxidation reaction conditions. Higher reaction temperatures can be used as compared to prior art processes, which significantly improves the reaction rate and permits smaller reactors to be used. The protective films of water on the surfaces of the platelet tubes, coupled with the elimination of preheating of the waste material, substantially reduces solids deposition and corrosion.
Abstract:
A processing vessel in which a temperature control element defining a helical flow passage, disposed on an outer surface of an inner barrel within the processing vessel. The barrel contains a processing liquid and a heating or cooling temperature control medium is caused to flow through the flow passage. The inner barrel and temperature control element are disposed in a vessel body to define a chamber between the temperature control element and an inner surface of the vessel body. The chamber defined between the vessel body and the temperature control element is a closed chamber. Preferably, a system for generally equalizing the pressures in the inner barrel and the closed chamber is provided. The temperature control element can be assembled in the vessel body after being manufactured outside the vessel body. Therefore, the processing vessel can be manufactured with improved efficiency and can be serviced by ordinary in-vessel maintenance operations.
Abstract:
A method and device for high-pressure treatment of liquid substances, for example foodstuffs. The substance undergoes a cyclic process whereby a limited amount of the substance during each cycle is pressurized in a pressure intensifier (1) to a predetermined pressure and is then maintained at this pressure for a predetermined period of time. After the substance has been pressurized in the pressure intensifier (1), it is conducted to a pressure chamber (10) while maintaining the predetermined pressure. The substance is further caused to reside in the pressure chamber (10) for the predetermined period of time by being caused to pass over a predetermined distance between an inlet (9a) and an outlet (9b), which are arranged in the pressure chamber (10).