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    Process for the production of a lubricating oil additive concentrate
    27.
    发明授权
    Process for the production of a lubricating oil additive concentrate 失效
    用于生产润滑油添加剂浓缩物的方法

    公开(公告)号：US5433871A

    公开(公告)日：1995-07-18

    申请号：US157336

    申请日：1993-11-23

    Applicant: Sean P. O'Connor ,  John Crawford ,  Charles Cane

    Inventor： Sean P. O'Connor ,  John Crawford ,  Charles Cane

    IPC: C10M125/00 ,  C10M125/10 ,  C10M125/14 ,  C10M125/18 ,  C10M129/08 ,  C10M129/10 ,  C10M129/16 ,  C10M129/38 ,  C10M129/54 ,  C10M129/70 ,  C10M135/10 ,  C10M159/20 ,  C10M159/22 ,  C10M159/24 ,  C10M177/00 ,  C10N10/04 ,  C10N20/02 ,  C10N40/25 ,  C10N70/00

    CPC classification number: C10M159/24 ,  C10M159/20 ,  C10M159/22 ,  C10M2201/082 ,  C10M2201/10 ,  C10M2207/021 ,  C10M2207/022 ,  C10M2207/04 ,  C10M2207/046 ,  C10M2207/08 ,  C10M2207/122 ,  C10M2207/126 ,  C10M2207/281 ,  C10M2209/108 ,  C10N2210/02 ,  C10N2230/04 ,  C10N2230/52 ,  C10N2270/02

    Abstract: A process for the production of a lubricating oil additive concentrate having a TBN greater than 300 which process comprises reacting at elevated temperaturecomponent (A) a defined mixture selected from defined sulphurized or non-sulphurized acids or calcium salts thereof,component (B) an alkaline earth metal base added either in a single addition or in a plurality of additions at intermediate points during the reaction,component (C) at least one compound which is (i) water, (ii) a polyhydric alcohol having 2 to 4 carbon atoms, (iii) a di- (C.sub.3 or C.sub.4) glycol, (iv) a tri-(C.sub.2 -C.sub.4) glycol, (v) a mono- or poly-alkylene glycol alkyl ether of the formula (I)R(OR.sup.1).sub.x OR.sup.2 (I)wherein R is a C.sub.1 to C.sub.6 alkyl group, R.sup.1 is an alkylene group, R.sup.2 is hydrogen or a C.sub.1 to C.sub.6 alkyl group and x is an integer from 1 to 6, (vi) a C.sub.1 to C.sub.20 monohydric alcohol, (vii) a C.sub.1 to C.sub.20 ketone, (viii) a C.sub.1 to C.sub.10 carboxylic acid ester, or (ix) a C.sub.1 to C.sub.20 ether,component (D) a lubricating oil,component (E) carbon dioxide added subsequent to the, or each, addition of component (B),component (F) a defined carboxylic acid or derivative,component (G) at least one compound which is (i) an inorganic halide or (ii) an ammonium alkanoate or a mono-, di-, tri- or tetra-alkyl ammonium formate or alkanoate provided that when component (G) is (ii), component (F) is not an acid chloride,the weight ratios of all components being such as to produce a concentrate having a TBN greater than 300.

    Abstract translation: 一种生产TBN大于300的润滑油添加剂浓缩物的方法，该方法包括在升高的温度下将组分（A）与选自定义的硫化或非硫化酸或其钙盐的限定混合物反应，组分（B） （C）至少一种化合物，其为（i）水，（ii）具有2至4个碳原子的多元醇 ，（iii）二（C3或C4）二醇，（iv）三（C2-C4）二醇，（v）式（I）R（OR1）的单 - 或聚 - 亚烷基二醇烷基醚， xOR 2（I）其中R为C1至C6烷基，R1为亚烷基，R2为氢或C1至C6烷基，x为1至6的整数，（vi）C1至C20一元醇， （vii）C1至C20酮，（viii）C1至C10羧酸酯，或（ix）C1至C20醚，组分（D）润滑油，组分（E）碳二 组分（B），组分（F），所定义的羧酸或衍生物，组分（G），至少一种化合物（i）无机卤化物或（ii）链烷酸铵 或（C）是（ⅱ）组分（F）不是酰基氯，所有组分的重量比例如 产生TBN大于300的浓缩物。

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