Continuous process for sulfurizing polybutenes
    62.
    发明授权
    Continuous process for sulfurizing polybutenes 失效
    用于硫化聚氨酯的连续方法

    公开(公告)号:US3631019A

    公开(公告)日:1971-12-28

    申请号:US3631019D

    申请日:1968-10-17

    CPC classification number: B01J10/005 C08F8/34 C08F110/08

    Abstract: A CONTINUOUS PROCESS FOR SULFURIZING POLYBUTENES FOR USE IN METAL WORKING LUBRICANTS, AND A REACTOR FOR USE IN CARRYING OUT THE CONTINUOUS PROCESS, INCLUDING INTRODUCING MOLTEN SULFUR AND POLYBUTENES INTO AND ENCLOSED CHAMBER WHERE FLOW THERETHROUGH IS INTERCEPTED TO PROVIDE A SERIES OF REACTION ZONES, MIXING TO PROVIDE INTIMATE CONTACT IN AT LEAST EACH ZONE SITUATED IN THE INITIAL ONE THIRD OF THE CHAMBER VOLUME, RECYCLING SULFUR COLLECTING ON THE BOTTOM OF AT LEAST THE ZONES IN THE INITIAL ONE THIRD OF THE VOLUME, ALLOWING FLOW FROM ONE ZONE TO ANOTHER, MAINTAINING THE CHAMBER AT FROM 300*F. TO 400*F. AND COORDINATING THE VARIOUS FLOW RATES AND THE CHAMBER VOLUME WITH THE REACTION TEMPERATURE TO PROVIDE A PREDETERMINED CHAMBER RESIDENCE TIME.

    Method and apparatus for producing trichlorosilane
    63.
    发明授权
    Method and apparatus for producing trichlorosilane 失效
    用于生产三氯硅烷的方法和装置

    公开(公告)号:US3565590A

    公开(公告)日:1971-02-23

    申请号:US3565590D

    申请日:1968-07-11

    Inventor: BRACKEN RONALD C

    CPC classification number: C01B33/04 B01J10/005 C01B33/107

    Abstract: TRICHLOROSILANE IS PRODUCED IN A REACTOR PACKED WITH A POROUS MASS OF SINTERED SILICON PARTICLES. A FURNACE SURROUNDING THE UPPER END OF THE REACTION CHAMBER MELTS THE TOP PORTION OF THE POROUS MASS TO FORM A POOL OF MOLTEN SILICON. BY FLOWING SILICON TETRACHLORIDE THROUGH THE POROUS MASS, A REACTION TAKES PLACE WITHIN THE REACTOR WHEN THE SICL4 CONTACTS THE MOLTEN SILICON. THIS REACTION PRODUCES SILICON DICHLORIDE. TO PRODUCE TRICHLOROSILANE, THE SILICON DICHLORIDE IS REACTED WITH HCL DOWNSTREAM OF THE REACTOR OUTPUT.

    D R A W I N G

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