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    Mixing box, and apparatus and method for producing films
    82.
    发明授权
    Mixing box, and apparatus and method for producing films 有权
    混合箱，以及制造薄膜的装置和方法

    公开(公告)号：US08118935B2

    公开(公告)日：2012-02-21

    申请号：US11132173

    申请日：2005-05-19

    Applicant: Takakazu Yamada ,  Takeshi Masuda ,  Masahiko Kajinuma ,  Masaki Uematsu ,  Koukou Suu

    Inventor： Takakazu Yamada ,  Takeshi Masuda ,  Masahiko Kajinuma ,  Masaki Uematsu ,  Koukou Suu

    IPC: C23C16/455 ,  C23C16/00 ,  H01L21/306

    CPC classification number: C23C16/45502 ,  B01F3/02 ,  B01F5/0256 ,  B01F2215/0427 ,  B01J4/001 ,  B01J10/02 ,  B01J19/247 ,  C23C16/4412 ,  C23C16/45512 ,  C23C16/45519 ,  C23C16/4558 ,  C23C16/4585 ,  H01L21/67017

    Abstract: A thin film manufacturing system, wherein a stage for placing a substrate thereon is disposed within a vacuum reactor and a gas head for supplying a film forming gas to a central area on a top face of the vacuum reactor is arranged so that the gas head is opposed to the stage. A cylindrical sleeve member is disposed and comes in close contact with a side wall of the stage to surround a periphery of the stage. The height of the stage can be established at the position where the volume of a second space formed below the stage and connected to a vacuum discharge means is larger than that of a first space formed above the stage, in such a manner that an exhaust gas is isotropically discharged from the first space without causing any convection current therein through the interstice between the sleeve member and an inner wall surface constituting the reactor.

    Abstract translation: 一种薄膜制造系统，其中用于将基板放置在其上的载物台设置在真空反应器内，并且将用于将成膜气体供应到真空反应器的顶面上的中心区域的气体头设置为使得气体头 反对舞台。 圆柱形套筒构件设置成与舞台的侧壁紧密接触以围绕舞台的周边。 该台架的高度可以在形成在载物台下方并连接到真空排出装置的第二空间的体积大于形成在载物台上方的第一空间的体积的位置上， 从第一空间各向同性地排出，而不会通过套筒构件和构成反应器的内壁面之间的间隙引起任何对流。

    Continuous Production of Copolymers Suitable as Flow Agents
    83.
    发明申请
    Continuous Production of Copolymers Suitable as Flow Agents 审中-公开
    适用于流动剂的共聚物的连续生产

    公开(公告)号：US20110306696A1

    公开(公告)日：2011-12-15

    申请号：US13122663

    申请日：2009-10-08

    Applicant: Silke Flakus ,  Laurent Marc ,  Zhizhong Cai ,  Helmut Mack ,  Burkhard Walther ,  Jochen Mezger ,  Simone Klapdohr ,  Tobias Austermann

    Inventor： Silke Flakus ,  Laurent Marc ,  Zhizhong Cai ,  Helmut Mack ,  Burkhard Walther ,  Jochen Mezger ,  Simone Klapdohr ,  Tobias Austermann

    IPC: C08F2/48 ,  C08K3/34 ,  C09D133/02 ,  C08F220/06

    CPC classification number: B01J19/123 ,  B01J10/02 ,  B01J19/1887 ,  B01J19/247 ,  C08F267/00 ,  C08F267/04 ,  C08F283/06 ,  C08F290/062 ,  C08F290/142 ,  C08L51/08 ,  C08L2666/02

    Abstract: The invention relates to a process for the preparation of copolymers containing acid monomer structural units and polyether macromonomer structural units, which is carried out in a continuous mode of operation in a reactor which has α) a body B rotating about an axis of rotation and having a reaction surface, β) a metering system and γ) a device for irradiating the reaction surface, i) the components of a starting reaction composition being applied individually and/or as a mixture with the aid of the metering system in a thin film on an inner region of the reaction surface of the rotating body B so that the thin film flows over the reaction surface of the rotating body B to an outer region of the reaction surface of the rotating body B, the thin film on the reaction surface being electromagnetically irradiated by means of the device for the irradiation of the reaction surface, ii) the thin film leaving the reaction surface as a reaction composition which has copolymer containing acid monomer structural units and polyether macromonomer structural units and iii) the reaction composition being collected after leaving the reaction surface, an acid monomer, a polyether macromonomer and a photoinitiator being present as components of the starting reaction composition.

    Abstract translation: 本发明涉及一种制备含有酸单体结构单元和聚醚大分子单体结构单元的共聚物的方法，其在反应器中以连续的操作模式进行，所述反应器具有α）围绕旋转轴线旋转并具有 一个反应表面和一个计量系统，γ）一个用于照射反应表面的装置，i）起始反应组合物的组分被单独地和/或作为混合物，借助于计量系统施加在薄膜中 在旋转体B的反应面的内部区域，使得薄膜在旋转体B的反应面上流动到旋转体B的反应面的外侧区域，反应面上的薄膜为 通过用于照射反应表面的装置电磁照射，ii）离开反应表面的薄膜作为反应组合物，其具有含有 酸单体结构单元和聚醚大分子单体结构单元，和iii）离开反应表面后收集反应组合物，酸单体，聚醚大分子单体和光引发剂作为起始反应组合物的组分存在。

    Baffle assembly module for vertical staged polymerization reactors
    85.
    发明授权
    Baffle assembly module for vertical staged polymerization reactors 有权
    用于垂直分级聚合反应器的挡板组件模块

    公开(公告)号：US07435393B2

    公开(公告)日：2008-10-14

    申请号：US11122376

    申请日：2005-05-05

    Applicant: Thomas Lloyd Yount ,  Paul Keith Scherrer ,  Larry Cates Windes

    Inventor： Thomas Lloyd Yount ,  Paul Keith Scherrer ,  Larry Cates Windes

    IPC: B01J19/00

    CPC classification number: B01J19/247 ,  B01J10/02 ,  B01J19/0006 ,  B01J19/32 ,  B01J19/325 ,  B01J2219/0077 ,  B01J2219/32206 ,  B01J2219/32213 ,  B01J2219/32234 ,  B01J2219/32272 ,  B01J2219/3306 ,  C08G63/785

    Abstract: The present invention provides an assembly for use in vertical, gravity flow driven polymerization reactors for combinations of high viscosity, high throughput, and shallow polymer depths. The baffle assembly module of the invention includes a support structure having a plurality of side openings. The side openings allow the escape of vapor liberated from the polymeric melt. The assembly further includes a feed splitter followed by two or more vertically arranged rows of baffle plates with the feed splitter and baffles sequentially positioned in the support structure. The plurality of parallel baffles in a row are angled such that when a polymeric melt contacts a given baffle the polymeric melt moves in a downward direction under the force of gravity. The arrangement of the rows is such that each row (except the lowest row) transfers the polymeric melt to a lower vertically adjacent row until reaching the last row of baffles in the module. According to the vertical arrangement of the components in the baffle assembly module and by stacking additional baffle assembly modules if needed within the reactor, the polymeric melt cascades down the vertical length of the reaction vessel interior. The present invention also provides a polymerization reactor that incorporates the assembly of the invention and a method of increasing the degree of polymerization of a polymer melt by using the assembly of the invention.

    Abstract translation: 本发明提供了一种用于垂直重力流驱动的聚合反应器中用于高粘度，高通量和浅聚合物深度组合的组合体。 本发明的挡板组件模块包括具有多个侧面开口的支撑结构。 侧开口允许从聚合物熔体释放的蒸气逸出。 该组件还包括一个进料分流器，随后是两个或更多垂直排列的挡板排，其中进料分流器和挡板顺序地位于支撑结构中。 一排中的多个平行挡板是成角度的，使得当聚合物熔体接触给定的挡板时，聚合物熔体在重力作用下沿向下的方向移动。 排的布置使得每排（除了最下排）将聚合物熔体转移到下垂直相邻的排，直到到达模块中的最后一排挡板。 根据挡板组件模块中的部件的垂直布置以及如果需要在反应器内堆叠附加的挡板组件模块，聚合物熔体沿着反应容器内部的垂直长度逐渐降级。 本发明还提供一种聚合反应器，其包含本发明的组合物和通过使用本发明的组合物提高聚合物熔体的聚合度的方法。

    Apparatus for the Continuous Modification of Polymers in the Free-Flowing State by Means of Electron Radiation
    86.
    发明申请
    Apparatus for the Continuous Modification of Polymers in the Free-Flowing State by Means of Electron Radiation 失效
    用于通过电子辐射在自由流动状态下连续改性聚合物的装置

    公开(公告)号：US20080248149A1

    公开(公告)日：2008-10-09

    申请号：US12088512

    申请日：2006-09-05

    Applicant: Michael Stephan ,  Gert Heinrich ,  Helmut Dorschner

    Inventor： Michael Stephan ,  Gert Heinrich ,  Helmut Dorschner

    IPC: B01J19/08

    CPC classification number: B01J19/26 ,  B01J10/02 ,  B01J19/085 ,  B01J19/1887 ,  B01J19/20 ,  B01J19/22 ,  B01J2219/00033 ,  B01J2219/00119 ,  B01J2219/0869 ,  B01J2219/0871 ,  B01J2219/0877 ,  B01J2219/0879 ,  B29C71/04 ,  B29C2035/0877

    Abstract: The invention relates to the fields of polymer chemistry and relates to a device for the continuous modification of polymers that can be processed into molded articles or semifinished products before, during and after modification. The object of the invention lies in disclosing a device in which the combination of melt production and modification takes place in a continuous method and leads to improved properties of the polymers. The object is attained through a device comprising a device component for converting the polymers into the flowable state, a radiation guard for an electron irradiation and cooling devices, wherein an irradiation device for electron radiation as well as supply and discharge lines are present inside the radiation guard, wherein in the case of the production of solid formed and modified polymers inside the radiation guard, a forming device is present inside the radiation guard and the flowable polymers after the forming device are present floating freely in space in the region of the irradiation.

    Abstract translation: 本发明涉及聚合物化学领域，涉及在改性之前，期间和之后可加工成模制品或半成品的聚合物的连续改性的装置。 本发明的目的在于公开一种其中熔体生产和改性的组合以连续方法发生并且导致聚合物的改进性能的装置。 该目的通过包括用于将聚合物转化为可流动状态的装置部件，用于电子辐射和冷却装置的辐射防护件的装置来实现，其中用于电子辐射的照射装置以及供给和排出线存在于辐射内 防护件，其中在辐射防护件内部生产固体成形和改性聚合物的情况下，辐射防护件内部存在形成装置，并且成形装置之后的可流动聚合物在照射区域内在空间中自由浮动。

    Methods of operating surface reactors and reactors employing such methods
    87.
    发明申请
    Methods of operating surface reactors and reactors employing such methods 失效
    使用这种方法操作表面反应器和反应器的方法

    公开(公告)号：US20060286015A1

    公开(公告)日：2006-12-21

    申请号：US10570180

    申请日：2004-09-04

    Applicant: Richard Holl

    Inventor： Richard Holl

    IPC: B01J19/00

    CPC classification number: B01F7/008 ,  B01F5/221 ,  B01F7/00758 ,  B01F7/00783 ,  B01F7/00791 ,  B01F7/00825 ,  B01F7/00833 ,  B01F2215/0427 ,  B01J10/02 ,  B01J14/00 ,  B01J19/1887 ,  B01J2219/00085

    Abstract: New methods of operating surface reactors, and such reactors, particularly spinning disk reactors, require that a first reactant is fed to a reactor surface (20) and forms a thin radially outward moving film (60) thereon in a reaction passage (42) formed between the reaction surface (20) and a parallel, closely spaced (less than 1 mm) retaining surface (40). The passage thickness is precisely controllable and the surfaces (20, 40) move relative to one another so that strong shear is applied to the material between them. A second reactant is fed to the surface (20) as a second thin film (65) that as it enters the first film (60), preferably perpendicularly, it is immediately merged therewith along a correspondingly very narrow interaction line (66) by the shear at a rate such as to break up molecular clusters in the films, so that their molecules can aggressively and completely interact by forced interdiffusion. In spinning disk (18) apparatus the first film (60) is fed along the spin axis (14), while subsequent films (65, etc.) are fed at respective distances from the axis (14) such that there is adequate shear for the molecular cluster disruption. Preferably each film (65, etc.) after the first (60) is fed into the reaction passage (42) through a respective thin annular nozzle producing a thin circular film (65) that simultaneously merges with the first film (60) along its entire length.

    Abstract translation: 操作表面反应器和这种反应器，特别是旋转盘式反应器的新方法要求将第一反应物供入反应器表面（20），并在其上形成薄的径向向外的移动膜（60），形成在反应通道（42）中 在反应表面（20）和平行紧密间隔（小于1mm）的保持表面（40）之间。 通道厚度是精确可控的，并且表面（20,40）相对于彼此移动，使得强剪切被施加到它们之间的材料。 第二反应物作为第二薄膜（65）被馈送到表面（20），第二薄膜（65）当其进入第一薄膜（60）时，优选地垂直于其，沿相应的非常窄的相互作用线（66）立即与其合并 以一定的速率剪切，以破坏膜中的分子簇，使得它们的分子可以通过强制相互扩散而积极和完全地相互作用。 在旋转盘（18）装置中，第一膜（60）沿着旋转轴线（14）进给，而随后的膜（65等）以相对于轴线（14）的距离进给，使得存在足够的剪切 分子簇破坏。 优选地，第一（60）之后的每个膜（65等）通过相应的薄环形喷嘴供给到反应通道（42）中，产生薄的圆形膜（65），其同时与第一膜（60）沿其 全长。

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