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    Method for preparation of olefin oxidation catalyst
    81.
    发明授权
    Method for preparation of olefin oxidation catalyst 失效
    烯烃氧化催化剂的制备方法

    公开(公告)号：US3844981A

    公开(公告)日：1974-10-29

    申请号：US25992972

    申请日：1972-06-05

    Applicant: EXXON RESEARCH ENGINEERING CO

    Inventor： CUSUMANO J

    IPC: B01J23/48 ,  B01J23/50 ,  B01J23/68 ,  B01J23/70 ,  B01J23/89 ,  B01J11/08 ,  B01J11/22

    CPC classification number: B01J23/8926 ,  B01J23/48 ,  B01J23/50 ,  B01J23/688 ,  B01J23/70 ,  B01J23/89 ,  B01J23/8946

    Abstract: A method for preparing an olefin oxidation catalyst, which comprises impregnating silver oxide or a water-insoluble silver salt, e.g. silver carbonate, silver carboxylates (having from 1 to 10 carbon atoms), silver chloride, etc., having a surface area of from 20 to 40 m2/g, preferably from 25 to 35 m2/g, with a solution containing a decomposable salt, selected from the group consisting of salts of Groups VII-B, I-B, or the iron group of Group VIII of the Periodic Table of the Elements, drying said impregnated salt, and activating by contacting with a reducing environment. Preferably the silver compound is silver oxide and said decomposable salt is selected from the group consisting of gold, copper, rhenium, manganese, and iron salts. The catalysts prepared by the instant method are especially effective in the oxidation of ethylene to ethylene oxide.

    Abstract translation: 一种制备烯烃氧化催化剂的方法，其包括将氧化银或不溶于水的银盐浸渍在其中。 表面积为20〜40m2 / g，优选为25〜35m2 / g的碳酸银，羧酸银（具有1〜10个碳原子），氯化银等，与含有可分解盐的溶液 ，选自元素周期表第VII-B族，第IB族或第VIII族的铁族的组，干燥所述浸渍的盐，并通过与还原环境的接触进行活化。 优选地，银化合物是氧化银，并且所述可分解盐选自金，铜，铼，锰和铁盐。 通过本方法制备的催化剂在乙烯氧化成环氧乙烷方面特别有效。

    Process for preparing a catalyst based on ruthenium
    83.
    发明授权
    Process for preparing a catalyst based on ruthenium 失效
    用于制备基于钌的催化剂的方法

    公开(公告)号：US3819536A

    公开(公告)日：1974-06-25

    申请号：US31833972

    申请日：1972-12-26

    Applicant: FORD MOTOR CO

    Inventor： BETTA R ,  SHELEF M ,  GANDHI H ,  KUMMER J

    IPC: B01D53/94 ,  B01J23/46 ,  B01J23/56 ,  B01J23/58 ,  B01J23/63 ,  B01J11/08

    CPC classification number: B01J23/63 ,  B01D53/9413 ,  B01D2255/1026 ,  B01D2255/2042 ,  B01J23/56 ,  B01J23/58

    Abstract: A process is taught for producing a ruthenium catalyst. A fixing compound, selected from alkaline earth materials or rare earth materials which decompose to an oxide of the material, is deposited on a catalytic support. A hydrated, halogenated ruthenium compound which reduces to ruthenium is also deposited on the catalytic support. The materials on the support are heated in a reducing atmosphere to form the ruthenium metal. After the reducing step the materials are fixed by heating them to a ruthenate forming temperature. The product produced in this manner is desirable for use in the catalytic conversion, in a reducing atmosphere, of oxides of nitrogen. The ruthenium catalyst of the product produced by this method is resistant to volatilization when exposed to an oxidizing ambient.

    Abstract translation: 教导了一种制备钌催化剂的方法。 选自碱土金属或分解成材料的氧化物的稀土材料的固定化合物沉积在催化载体上。 还原成钌的水合卤化钌化合物也沉积在催化载体上。 载体上的材料在还原气氛中加热以形成钌金属。 在还原步骤之后，通过将其加热至钌酸盐形成温度来固定材料。 以这种方式生产的产品在用于在还原气氛中的氮氧化物的催化转化中是理想的。 通过该方法生产的产品的钌催化剂在暴露于氧化环境中时耐挥发。

    Regeneration of a coke deactivated catalyst comprising a combination of platinum rhenium and halogen with a porous carrier material
    84.
    发明授权
    Regeneration of a coke deactivated catalyst comprising a combination of platinum rhenium and halogen with a porous carrier material 失效
    包含铑和铀与多孔载体材料的组合的焦糖活化催化剂的再生

    公开(公告)号：US3753926A

    公开(公告)日：1973-08-21

    申请号：US3753926D

    申请日：1971-03-08

    Applicant: UNIVERSAL OIL PROD CO

    Inventor： HAYES J

    IPC: B01J23/96 ,  B01J38/44 ,  C10G35/09 ,  B01J11/08 ,  C10G35/06

    CPC classification number: B01J38/44 ,  B01J23/96 ,  C10G35/09

    Abstract: A DEACTIVATED HYDROCARBON CONVERSION CATALYST, WHICH IS A COMBINATION OF A PLATINUM GROUP COMPONENT, A RHENIUM COMPONENT AND A HALOGEN COMPONENT WITH A POROUS CARRIER MATERIAL AND WHICH HAS BENN DEACTIVATED BY DEPOSITION OF CARBONACEOUS MATERIAL THEREON DURING A PREVIOUS CONTACTING WITH A HYDROCARBON CHARGE STOCK AT AN ELEVATED TEMPERATURE, IS REGENERATED BY THE SEQUEENTIAL STEPS OF:(1E) BURNING CARBON THEREFRROM AT A RELATIVELY LOW TEMPERATURE WITH A GAS STREAM CONTAINING HALOGEN OR A HALOGEN-CONTAINING COMPOUND, H2O, AND A RELATIVELY SMALL AMOUNT OF 32, (2) TREATING THE RESULTING PARTIALLY REGENERATED CATLYST AT A RELATIVELY HIGHER TEMPERATURE WITH A GAS STREAM CONTAINING A HALOGEN OR A HALOGENCONTAINING COMPOUND, H2O, AND A RELATIVELY HIGHER AMOUNT OF O2, (3) PURGING O2 AND H2OO FROM CONTACT WITH THE RESULTING CATALYST, AND, (4) SUBJECTING THE RESULTING CATALYST TO CONTACT WITH A DRY HYDROGEN STREAM. KEY FEATURES OF THE DISCLOSED METHOD ARE: (1) PRESENCE OF WATER AND HALOGEN IN THE GAS STREAM USED IN THE CARBON-BURNING STEP AND IN THE OXYGEN-TREATING STEP, (2) CAREFUL CONTROL OF THE TEMPERATURE DURING EACH STEP, (3) MAINTENCE OF THE HALOGEN CONTENT OF THE CATALYST AT A RELATIVELY HIGH LEVEL DURING THE ENTIRE REGENERATION PROCEDURE, AND (4) CAREFUL CONTROL OVER THE COMPOSITION OF THE GAS STREAMS USED IN THE VARIOUS STEPS THEREOF.

    Catalytic reforming process
    87.
    发明授权
    Catalytic reforming process 失效
    催化重整工艺

    公开(公告)号：US3729408A

    公开(公告)日：1973-04-24

    申请号：US3729408D

    申请日：1970-12-28

    Applicant: EXXON RESEARCH ENGINEERING CO

    Inventor： CARTER J ,  SINFELT J

    IPC: B01J23/48 ,  B01J23/89 ,  C07C5/387 ,  C10G35/09 ,  C10G35/08 ,  B01J11/08 ,  B01J11/22

    CPC classification number: C10G35/09 ,  B01J23/48 ,  B01J23/8926 ,  C07C5/387 ,  Y02P20/52 ,  C07C15/04

    Abstract: A catalytic reforming process wherein naphtha feed streams, boiling from about 80* to 450* F, and comprising naphthenes, paraffins and aromatics, are contacted, in an initial reaction zone, with a hydrogen containing gas, in the presence of a catalyst comprising Pt and a group IB metal supported on a refractory oxide; passed into a tail zone wherein the feed stream is again contacted with a catalyst and thereby further reacted; and a high octane product is recovered. In a preferred embodiment the Group IB metal is Cu.

    Abstract translation: 在催化重整过程中，在初始反应区中，在含有Pt的催化剂存在下，将沸点为约80-450°F的石脑油进料流，包含环烷烃，链烷烃和芳族化合物与含氢气体接触， 和负载在难熔氧化物上的IB族金属; 进入尾区，其中进料流再次与催化剂接触，从而进一步反应; 并回收高辛烷值的产品。 在优选实施方案中，IB族金属是Cu。

    Particles featuring gamma alumina
    89.
    发明授权
    Particles featuring gamma alumina 失效
    颗粒特色佳玛铝

    公开(公告)号：US3669904A

    公开(公告)日：1972-06-13

    申请号：US3669904D

    申请日：1970-05-28

    Applicant: AIR PROD & CHEM

    Inventor： CORNELIUS EDWARD B ,  KOESTER DAVID W

    IPC: B01J21/04 ,  B01J23/40 ,  B01J23/88 ,  B01J37/00 ,  C10G35/09 ,  C10G45/08 ,  B01J11/06 ,  B01J11/08 ,  B01J11/32

    CPC classification number: B01J37/0009 ,  B01J21/04 ,  B01J23/40 ,  B01J23/88 ,  B01J37/0018 ,  C10G35/09 ,  C10G45/08

    Abstract: A propensity to form gummy mixtures with water is a troublesome characteristic of a technical grade of boehmite, said power comprising a total ignition loss of about 25 percent, a volatile alcohol content corresponding to less than 1 percent carbon, minor amounts of amorphous alumina and a major amount of alpha mono hydrate. A portion of the technical boehmite is mildly calcined at 400*-500* C. for at least 15 minutes to provide a dehydrated alumina powder, which then mixed with a significantly larger amount of the uncalcined technical grade of boehmite, can be mixed with water for providing a plastic mixture suitable for shaping into catalyst particles. The catalyst particles are calcined above about 600* C. for more than 1 hour in the presence of steam to form attrition resistant particles of gamma alumina having the pore size distribution desirable in certain types of catalysts.

    Abstract translation: 与水形成胶状混合物的倾向是勃姆石的技术级别的麻烦特征，所述功率包括约25％的总灼烧损失，对应于小于1％碳的挥发性醇含量，少量无定形氧化铝和 主要量的α一水合物。 将一部分技术勃姆石在400-500℃下轻度煅烧至少15分钟，以提供脱水氧化铝粉末，然后与明显更大量的未煅烧的工业级勃姆石混合，可与水混合 用于提供适合于成型为催化剂颗粒的塑料混合物。 催化剂颗粒在约600℃下在蒸汽存在下煅烧超过1小时，以形成具有在某些类型的催化剂中所需孔径分布的耐磨性的γ氧化铝颗粒。

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