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公开(公告)号：US10756306B2
公开(公告)日：2020-08-25
申请号：US16340472
申请日：2017-10-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Nicholas C. Erickson , Moses M. David , Xiaoguang Sun , Manoj Nirmal , Haeen Sykora , Hui Luo , Samuel J. Carpenter , Jilliann M. Nelson , Justin P. Meyer , Bert T. Chien , David J. Rowe , Robert L. Brott , David G. Freier , Hyacinth L. Lechuga
Abstract: A nanostructured article having a first layer with a nanostructured surface is described. The nanostructured surface includes a plurality of pillars extending from a base surface of the first layer. The pillars have an average height greater than an average lateral dimension of the pillars. An average center-to-center spacing between pillars is no more than 2000 nm. The average lateral dimension is no less than 50 nm. Each pillar in the plurality of pillars has at least a lower portion and an upper portion where the lower portion is between the upper portion and the base surface, and the upper and lower portions have differing compositions. The nanostructured article includes a second layer disposed over the plurality of pillars and extending continuously to the base surface.
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公开(公告)号：US10213993B2
公开(公告)日：2019-02-26
申请号：US15105913
申请日：2014-12-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Kui Chen-Ho , Caroline M. Ylitalo , Yu Yang , Yongshang Lu , Alan L. Levin , Hyacinth L. Lechuga , Steven H. Kong , Suresh S. Iyer , Ingrid N. Haugan , Mahfuza B. Ali
IPC: C08K3/22 , C09D127/12 , C09D143/04 , B32B27/08 , B32B7/02 , B32B27/28 , B32B27/30 , B32B37/14 , C09D133/10 , B32B27/36 , B32B1/00 , C09D7/61
Abstract: Described herein is composite article comprising a substrate; and on at least one face of the substrate a multilayered coating disposed thereon. The multilayered coating comprises (i) an abrasion-resistant layer adjacent to the substrate, wherein the abrasion-resistant layer comprises inorganic oxide nanoparticles and a polymer binder; and (ii) an antireflection layer adjacent to the abrasion-resistant layer opposite the substrate, wherein the antireflection layer comprises a fluorosilane polymer, wherein the fluorosilane polymer comprises: at least one monomeric unit A represented by the formula (I) wherein R1 represents H or methyl, L1 represents a covalent bond or a divalent aliphatic group having from 1 to 10 carbon atoms, each Y1 independently represents a hydrocarbyl group having from 1 to 6 carbon atoms, each Y2 independently represents a hydrolyzable group, g is 0, 1, or 2; and at least one divalent monomeric unit B represented by the formula (I) wherein R2, R3, and R4 represent H, methyl, trifluoromethyl, or F, wherein at least one of R2, R3, and R4 is F, Rf1 represents a covalent bond or a divalent group selected from the group consisting of —(CF2O)a—, —(CF2CF2O)b—, —(CF2CF2CF2O)c—, —(CF2CF2CF2CF2O)d—, —(CF2CF(CF3)O)e—, and combinations thereof, wherein a, b, c, d, and e represent integers in the range of from 0 to 130, and wherein 1≤a+b+c+d+e≤130, and Rf2 is a perfluoroalkyl group.
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公开(公告)号：US20160318287A1
公开(公告)日：2016-11-03
申请号：US15105913
申请日：2014-12-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Kui Chen-Ho , Caroline M. Ylitalo , Yu Yang , Yongshang Lu , Alan L. Levin , Hyacinth L. Lechuga , Steven H. Kong , Suresh I. Iyer , Ingrid N. Haugan , Mahfuza B. Ali
IPC: B32B27/08 , B32B7/02 , C09D133/10 , B32B27/30 , C09D7/12 , C09D143/04 , B32B37/14 , B32B27/28
CPC classification number: B32B27/08 , B32B1/00 , B32B7/02 , B32B27/28 , B32B27/308 , B32B27/365 , B32B37/14 , B32B2255/10 , B32B2255/20 , B32B2255/24 , B32B2255/28 , B32B2264/102 , B32B2307/554 , B32B2457/20 , B32B2551/00 , C08K3/22 , C09D7/61 , C09D127/12 , C09D133/10 , C09D143/04
Abstract: Described herein is composite article comprising a substrate; and on at least one face of the substrate a multilayered coating disposed thereon. The multilayered coating comprises (i) an abrasion-resistant layer adjacent to the substrate, wherein the abrasion-resistant layer comprises inorganic oxide nanoparticles and a polymer binder; and (ii) an antireflection layer adjacent to the abrasion-resistant layer opposite the substrate, wherein the antireflection layer comprises a fluorosilane polymer, wherein the fluorosilane polymer comprises: at least one monomeric unit A represented by the formula (I) wherein R1 represents H or methyl, L1 represents a covalent bond or a divalent aliphatic group having from 1 to 10 carbon atoms, each Y1 independently represents a hydrocarbyl group having from 1 to 6 carbon atoms, each Y2 independently represents a hydrolyzable group, g is 0, 1, or 2; and at least one divalent monomeric unit B represented by the formula (I) wherein R2, R3, and R4 represent H, methyl, trifluoromethyl, or F, wherein at least one of R2, R3, and R4 is F, Rf1 represents a covalent bond or a divalent group selected from the group consisting of —(CF2O)a—, —(CF2CF2O)b—, —(CF2CF2CF2O)c—, —(CF2CF2CF2CF2O)d—, —(CF2CF(CF3)O)e—, and combinations thereof, wherein a, b, c, d, and e represent integers in the range of from 0 to 130, and wherein 1≦a+b+c+d+e≦130, and Rf2 is a perfluoroalkyl group.
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4.发明公开公开(公告)号：US20240066473A1
公开(公告)日：2024-02-29
申请号：US17766395
申请日：2020-12-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Clinton P. Waller, Jr. , Michelle M. Mok , Lucas D. McIntosh , Timothy M. Gillard , Carl A. Laskowski , Hyacinth L. Lechuga
CPC classification number: B01D69/02 , B01D71/80 , B01D71/26 , B01D71/281 , B01D71/521 , B01D71/5211 , B01D71/283 , B01D69/12 , B01D67/0013 , B01D2325/0212 , B01D2325/04 , B01D2325/02832 , B01D2325/02833
Abstract: The present disclosure provides an article including an isoporous membrane disposed on a porous substrate. The iso-porous membrane includes a triblock copolymer or a pentablock copolymer. The isoporous membrane has a thickness and is isoporous throughout its thickness. A method of making an article is also provided, which does not require a solvent exchange process. The method includes depositing a composition on a porous substrate, thereby forming a fdm, and removing at least a portion of the solvent from the film, thereby forming an isoporous membrane having numerous pores. The composition contains a solvent and solids including a triblock copolymer or a pentablock copolymer. The article advantageously can be hydrophilic and provides sharp molecular weight cut-offs and high flux.
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5.发明公开公开(公告)号：US20240001415A1
公开(公告)日：2024-01-04
申请号：US18253989
申请日：2022-01-25
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Jodi L. Connell , Raymond P. Johnston , John J. Sullivan , Karl J.L. Geisler , Vivian W. Jones , Gordon A. Kuhnley , Patrick G. Zimmerman , Bradley W. Eaton , Kurt J. Halverson , Brian W. Lueck , Alexandr C. Eldredge , Hyacinth L. Lechuga , Lynn E. Lorimor , Diane R. Wolk , Junia M. Pereira , Caroline M. Yitalo , Linda W. Suszko , Daniel J. Rogers , Bryon A. Mrrill
CPC classification number: B08B17/065 , B29C2059/023 , B08B17/04
Abstract: Films and articles are described comprising a microstructured surface having an array of peak structures and adjacent valleys. For improved cleanability, the valleys preferably have a maximum width ranging from 10 microns to 250 microns and the peak structures have a side wall angle greater than 10 degrees. The peak structures may comprise two or more facets such as in the case of a linear array of prisms or an array of cube-corners elements. The facets form continuous or semi-continuous surfaces in the same direction. The valleys typically lack intersecting walls. Also described are methods of making and methods of use. The microstructured surface of the article can be prepared by various microreplication techniques such as coating, injection molding, embossing, laser etching, extrusion, casting and curing a polymerizable resin; and bonding microstructured film to a surface or article with an adhesive.
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Patent Agency Ranking
公开(公告)号：US20190386251A1
公开(公告)日：2019-12-19
申请号：US16340472
申请日：2017-10-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Nicholas C. Erickson , Moses M. David , Xiaoguang Sun , Manoj Nirmal , Haeen Sykora , Hui Luo , Samuel J. Carpenter , Jilliann M. Nelson , Justin P. Meyer , Bert T. Chien , David J. Rowe , Robert L. Brott , David G. Freier , Hyacinth L. Lechuga
Abstract: A nanostructured article having a first layer with a nanostructured surface is described. The nanostructured surface includes a plurality of pillars extending from a base surface of the first layer. The pillars have an average height greater than an average lateral dimension of the pillars. An average center-to-center spacing between pillars is no more than 2000 nm. The average lateral dimension is no less than 50 nm. Each pillar in the plurality of pillars has at least a lower portion and an upper portion where the lower portion is between the upper portion and the base surface, and the upper and lower portions have differing compositions. The nanostructured article includes a second layer disposed over the plurality of pillars and extending continuously to the base surface.
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公开(公告)号：US20230158557A1
公开(公告)日：2023-05-25
申请号：US17917704
申请日：2021-05-14
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Jodi L. Connell , Raymond P. Johnston , Daniel J. Rogers , John J. Sullivan , Gordon A. Kuhnley , Brian W. Lueck , Alexander C. Eldredge , Kurt J. Halverson , Hyacinth L. Lechuga
CPC classification number: B08B17/065 , A61B7/02
Abstract: Medical diagnostic devices or components thereof are described that comprise a microstructured surface that comprises peak structures and adjacent valleys wherein the valleys have a maximum width ranging from 1 to 1000 microns and the peak structures. In some embodiments (e.g.
for improved cleanability) the peak structures of the microstructured surface have a side wall angle of greater than 10 degrees. The peak structures may comprise two or more facets such as in the case of a linear array of prisms or an array of cube-comers elements. The microstructured surface of the medical diagnostic device typically comes in contact with multiple patients during normal use of the device, such as a stethoscope diaphragm. The microstructured surface exhibits better microorganism (e.g. bacteria) removal when cleaned and/or provides a reduction in microbial touch transfer. Also described are methods of making and methods of use.-
公开(公告)号：US20220088546A1
公开(公告)日：2022-03-24
申请号：US17425409
申请日：2020-03-24
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Michelle M. Mok , Timothy M. Gillard , Carl A. Laskowski , Lucas D. McIntosh , Hyacinth L. Lechuga
Abstract: A porous membrane, The porous membrane includes a triblock copolymer of the formula ABC, the porous membrane comprising a plurality of pores; wherein the A block has a Tg of 90 degrees Celsius or greater and is present in an amount ranging from 30% to 80% by weight, inclusive, of the total block copolymer; wherein the B block has a Tg of 25 degrees Celsius or less and is present in an amount ranging from 10% to 40% by weight, inclusive, of the total block copolymer and wherein the C block is a water miscible hydrogen-bonding block immiscible with each of the A block and the B block; wherein the porous membrane comprising a first major surface and an opposed second major surface, wherein the first major surface is a nanostructured surface.
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公开(公告)号：US20200047135A1
公开(公告)日：2020-02-13
申请号：US16339832
申请日：2017-11-14
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Michelle M. Mok , Carl A. Laskowski , Lucas D. McIntosh , Hyacinth L. Lechuga , Timothy M. Gillard , Clinton P. Waller, JR.
Abstract: The present disclosure provides a porous membrane made of pentablock copolymer. The porous membrane includes an ABCBA block copolymer and has a number of pores. The A block is immiscible with each of the B block and the C block, the B block has a glass transition temperature (Tg) of 90 degrees Celsius or greater, and the C block has a Tg of 25 degrees Celsius or less. The A block comprises a poly(alkylene oxide), a substituted epoxide, a polylactam, or a substituted carbonate; B block comprises a vinyl aromatic monomer or a polyalkylmethacrylate and C block comprises a polyacrylate, a polysiloxane or a polyisoprene. A method of making a porous membrane is also provided. The method includes forming a film or a hollow fiber from a solution including a solvent and solids containing an ABCBA block copolymer. The method further includes removing at least a portion of the solvent from the film or the hollow fiber and contacting the film or the hollow fiber with a nonsolvent.
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10.发明申请公开(公告)号：US20150076106A1
公开(公告)日：2015-03-19
申请号：US14384100
申请日：2013-05-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Mark J. Pellerite , Seth M. Kirk , Hyacinth L. Lechuga
IPC: H01B13/00
CPC classification number: H01B13/003 , H01B1/22 , H01L27/3239 , H01L51/0021 , H01L51/102 , H01L51/442 , H01L51/5206 , H01L51/5215 , H05K9/009 , H05K9/0094 , Y02E10/549
Abstract: A method comprising: providing a transparent electrically conductive film comprising: a transparent substrate (14); a composite layer (18) comprising: an electrically conductive layer disposed on at least a portion of a major surface of the transparent substrate (14) and comprising a plurality of interconnecting metallic nanowires (12); and a polymeric overcoat layer disposed on a portion of the electrically conductive layer, to provide a coated area of the electrically conductive layer; and patternwise exposing the coated area of the electrically conductive layer to a corona discharge to provide a patternwise exposed electrically conductive film comprising (1) an un exposed region (122) of the coated region having a first electrical resistivity, and (2) an exposed region (121) having a second electrical resistivity; wherein the exposed region is less electrically conductive than the unexposed region, and wherein there is a ratio of the second electrical resistivity over the first electrical resistivity of at least 1000:1.
Abstract translation: 一种方法，包括：提供透明导电膜，包括：透明基板（14）; 复合层（18），包括：导电层，设置在所述透明基板（14）的主表面的至少一部分上并且包括多个互连金属纳米线（12）; 以及设置在所述导电层的一部分上的聚合物外涂层，以提供所述导电层的涂覆区域; 以及将所述导电层的涂覆区域图案化地暴露于电晕放电以提供图案化的暴露的导电膜，所述导电膜包括（1）所述涂覆区域的未曝光区域（122）具有第一电阻率，和（2） 具有第二电阻率的区域（121）; 其中所述暴露区域比所述未曝光区域导电性差，并且其中所述第一电阻率与所述第一电阻率之比至少为1000:1。
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