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    Process for Manufacturing 4-Propargylated Amino-Benzoxazinones
    1.
    发明申请
    Process for Manufacturing 4-Propargylated Amino-Benzoxazinones 有权
    制备4-炔丙基化氨基苯并嗪酮的方法

    公开(公告)号：US20160137615A1

    公开(公告)日：2016-05-19

    申请号：US14899755

    申请日：2014-06-17

    Applicant: BASF SE

    Inventor： Timo FRASSETTO ,  Maximilian DOCHNAHL ,  Michael RACK ,  Volker MAYWALD ,  Bernd WOLF ,  Roland GOETZ ,  Philip MUELHEIMS ,  Rudolf HAEBERLE

    IPC: C07D265/36

    CPC classification number: C07D265/36 ,  C07C17/16 ,  C07D413/04 ,  C07C21/22

    Abstract: The present invention relates to a process for manufacturing 4-propargylated amino-benzoxazinones of formula (I), comprising the following steps: step a) preparing propargyl chloride by reacting propargyl alcohol with thionyl chloride optionally in the presence of a catalyst; and step b) reacting the propargyl chloride prepared in step (a) with a NH-benzoxazinone of formula (II); wherein the variables are defined according to the description.

    Abstract translation: 本发明涉及制备式（I）的4-炔丙基化苯并恶嗪酮的方法，包括以下步骤：步骤a）任选地在催化剂存在下，通过炔丙醇与亚硫酰氯反应制备炔丙基氯; 和步骤b）使步骤（a）中制备的炔丙基氯与式（II）的NH-苯并嗪酮反应; 其中根据描述定义变量。

    Process for Preparing Sulfimines and Their in-situ Conversion into N-(1-Amino-Benzoyl)-Sulfimines
    2.
    发明申请
    Process for Preparing Sulfimines and Their in-situ Conversion into N-(1-Amino-Benzoyl)-Sulfimines 审中-公开
    制备亚磺酰亚胺及其原位转化成N-（1-氨基 - 苯甲酰基） - 亚磺酰胺的方法

    公开(公告)号：US20160046572A1

    公开(公告)日：2016-02-18

    申请号：US14778771

    申请日：2014-03-27

    Applicant: BASF SE

    Inventor： Timo FRASSETTO ,  Harald JOCKERS ,  Christopher KORADIN ,  Thomas ZIERKE ,  Karsten KOERBER

    IPC: C07C381/10 ,  C07D401/04

    CPC classification number: C07C381/10 ,  A01N37/28 ,  A01N43/56 ,  C07C2601/02 ,  C07D401/04 ,  C07D409/14

    Abstract: The present invention relates to a process for preparing a compound of the formulae (Ia) or (Ib), or a mixture thereof, wherein R1 and R2 independently of one another are hydrogen, C1-C10-alkyl, C1-C10-haloalkyl, C3-C10-cycloalkyl, C3-C10-halocycloalkyl, C2-C10-alkenyl, C2-C10-haloalkenyl or together represent an aliphatic chain, or the like; A− is HSO4− or 1/2 SO42−; the process comprising the reaction of a sulfide of formula SR1R2 with hydroxylamineO-sulfonic acid of formula; wherein the reaction is carried out in an aqueous medium in the presence of a base. The present invention also relates to a process for preparing a compound of the formula (IV), wherein R3 is halogen, cyano, C1-C8-alkyl, C1-C8-haloalkyl, C3-C8-cycloalkyl, C3-C8-halocycloalkyl, C2-C8-alkenyl, C2-C8-haloalkenyl, C1-C8-alkoxy, phenyl, or the like; R4 is hydrogen, C1-C10-alkyl, C1-C10-haloalkyl, C3-C8-cycloalkyl, C3-C8-halocycloalkyl, C2-C10-alkenyl, C2-C10-haloalkenyl, phenyl, or the like; p is 0, 1, 2, 3 or 4; the process comprising: (i) providing the compound of the formulae (Ia) or (Ib), or a mixture thereof, (ii) reacting a compound of the formulae (Ia) or (Ib), or a mixture thereof, obtained in step (i) with a compound of the formula (V) in the presence of a base,

    Abstract translation: 本发明涉及制备式（Ia）或（Ib）化合物或其混合物的方法，其中R 1和R 2彼此独立地是氢，C 1 -C 10 - 烷基，C 1 -C 10 - 卤代烷基， C 3 -C 10 - 环烷基，C 3 -C 10 - 卤代环烷基，C 2 -C 10 - 烯基，C 2 -C 10 - 卤代烯基或一起代表脂族链等; A-是HSO4-或1/2 SO42-; 该方法包括式SR 1 R 2的硫化物与式的羟胺O-磺酸的反应; 其中反应在碱的存在下在水性介质中进行。 本发明还涉及制备式（IV）化合物的方法，其中R 3是卤素，氰基，C 1 -C 8 - 烷基，C 1 -C 8 - 卤代烷基，C 3 -C 8 - 环烷基，C 3 -C 8 - 卤代环烷基， C 2 -C 8 - 烯基，C 2 -C 8 - 卤代烯基，C 1 -C 8 - 烷氧基，苯基等; R4是氢，C1-C10-烷基，C1-C10-卤代烷基，C3-C8-环烷基，C3-C8-卤代环烷基，C2-C10-烯基，C2-C10-卤代烯基，苯基等; p是0，1，2，3或4; 该方法包括：（i）提供式（Ia）或（Ib）化合物或其混合物，（ii）使式（Ia）或（Ib）化合物或其混合物 步骤（i）与式（Ⅴ）化合物在碱的存在下反应，

    CARBAMAT-BENZOXAZINONES
    4.
    发明申请
    CARBAMAT-BENZOXAZINONES 有权
    卡巴胺 - 苯并恶唑酮

    公开(公告)号：US20150299148A1

    公开(公告)日：2015-10-22

    申请号：US14421348

    申请日：2013-08-07

    Applicant: BASF SE

    Inventor： Maximilian DOCHNAHL ,  Roland GÖTZ ,  Joachim GEBHARDT ,  Uwe Josef VOGELBACHER ,  Timo FRASSETTO ,  Michael RACK ,  Volker MAYWALD ,  Bernd WOLF

    IPC: C07D265/36 ,  C07D413/04

    CPC classification number: C07D265/36 ,  C07D413/04

    Abstract: The present invention relates to carbamat-benzoxazinones of formula (I), wherein the variables are defined according to the description, as well as to a process for manufacturing carbamat-benzoxazinones of formula (I), and to the use of carbamat-benzoxazinones of formula (I) in manufacturing benzoxazinones of formula (X).

    Abstract translation: 本发明涉及式（I）的氨基甲酰 - 苯并恶嗪酮，其中根据描述定义变量，以及制备式（I）的氨基甲酰 - 苯并恶嗪酮的方法，以及使用式（I）的氨基甲酰 - 苯并恶嗪酮 式（I）在制备式（X）的苯并恶嗪酮时。

    Process for Manufacturing Haloacetamides
    6.
    发明申请
    Process for Manufacturing Haloacetamides 有权
    制备卤代乙酰胺的方法

    公开(公告)号：US20160176805A1

    公开(公告)日：2016-06-23

    申请号：US14902890

    申请日：2014-06-04

    Applicant: BASF SE

    Inventor： Timo FRASSETTO ,  Volker MAYWALD ,  Michael RACK ,  Maximilian DOCHNAHL ,  Bernd WOLF

    IPC: C07C231/02 ,  C07C51/58

    CPC classification number: C07C231/02 ,  C07C51/58 ,  C07C231/00 ,  C07C233/05 ,  C07C53/48

    Abstract: The present invention relates to a process for manufacturing haloacetamides of formula (I), comprising sub-step (a): reacting halones of formula (II) with oleum; followed by sub-step (b): reacting the reaction mixture obtained in sub-step(a) with an amine of formula (IV) optionally in the presence of a base; wherein the variables are defined according to the description.

    Abstract translation: 本发明涉及一种制备式（I）的卤代乙酰胺的方法，其包括以下步骤（a）：使式（II）的卤酮与发烟硫酸反应; 然后是亚步骤（b）：使在步骤（a）中获得的反应混合物与式（IV）的胺任选地在碱的存在下反应; 其中根据描述定义变量。

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