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公开(公告)号：US20140097391A1
公开(公告)日：2014-04-10
申请号：US14050184
申请日：2013-10-09
Applicant: California Institute of Technology
Inventor： Jean-Pierre Fleurial , Sabah K. Bux
IPC: H01L35/22
Abstract: The present invention provides a method of preparing a nanocomposite thermoelectric material. The method includes heating a reaction mixture of a semiconductor material and a metal complex to a temperature greater than the decomposition temperature of the metal complex. The heating forms metallic inclusions having a size less than about 100 nm that are substantially evenly distributed throughout the semiconductor material forming the nanocomposite thermoelectric material. The present invention also provides a nanocomposite thermoelectric material prepared by this method.
Abstract translation: 本发明提供一种制备纳米复合热电材料的方法。 该方法包括将半导体材料和金属络合物的反应混合物加热至大于金属络合物的分解温度的温度。 加热形成尺寸小于约100nm的金属夹杂物，其基本均匀地分布在形成纳米复合热电材料的整个半导体材料中。 本发明还提供了一种通过该方法制备的纳米复合热电材料。
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公开(公告)号：US20170066962A1
公开(公告)日：2017-03-09
申请号：US15261764
申请日：2016-09-09
Inventor： Vilupanur A. Ravi , Samad A. Firdosy , Sabah K. Bux , Jean-Pierre Fleurial , Shiao-Pin S. Yen , Andrew Kindler , Su C. Chi , Margie L. Homer , Bryan W. McEnerney , Pandurang Kulkarni , Desikan Sundararajan
CPC classification number: C09K8/80 , B01J2/04 , C04B33/1352 , C04B33/138 , C04B35/587 , C04B35/597 , C04B35/62204 , C04B35/62655 , C04B2235/3208 , C04B2235/528 , C04B2235/5427 , C04B2235/6562 , C04B2235/6565 , C04B2235/77 , C04B2235/94 , C04B2235/96 , C09K8/805 , Y02P40/69
Abstract: The disclosure herein includes methods of preparing ceramic beads, useful as proppant materials, by mixing ceramic precursors, such as slag, fly ash, or aluminum dross, forming bead precursors from the mixture, and heating the bead precursors to drive a chemical reaction between the ceramic precursors to form the ceramic beads. The resultant ceramic beads may be generally spherical particles that are characterized by diameters of about 0.1 to 2 mm, a diametral strength of at least about 100 MPa, and a specific gravity of about 1.0 to 3.0. A coating process may optionally be used to increase a diametral strength of a proppant material. A sieving process may optionally be used to obtain a smaller range of sizes of proppant materials.
Abstract translation: 本文的公开内容包括通过混合陶瓷前体，例如炉渣，飞灰或铝渣，制备陶瓷珠，用作支撑剂材料的方法，从混合物形成珠粒前体，以及加热珠粒前体以驱动 陶瓷前体形成陶瓷珠。 得到的陶瓷珠可以是通常为球形颗粒，其特征在于直径为约0.1至2mm，直径强度为至少约100MPa，比重为约1.0至3.0。 涂覆方法可以任选地用于增加支撑剂材料的直径强度。 筛选方法可以任选地用于获得较小范围的支撑剂材料的尺寸。
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Patent Agency Ranking
公开(公告)号：US10017687B2
公开(公告)日：2018-07-10
申请号：US14712888
申请日：2015-05-14
Applicant: CALIFORNIA INSTITUTE OF TECHNOLOGY
Inventor： Vilupanur A. Ravi , Samad A. Firdosy , Jean-Pierre Fleurial , Sabah K. Bux , Andrew Kindler
IPC: C09K8/80 , C04B35/622 , C04B35/653 , C04B35/628 , C04B33/135 , C04B33/138 , C04B33/32 , C04B35/04 , C04B35/58 , C04B35/626 , C04B35/645 , C04B38/00
CPC classification number: C09K8/805 , C04B33/1352 , C04B33/138 , C04B33/32 , C04B33/323 , C04B35/04 , C04B35/58007 , C04B35/62204 , C04B35/62655 , C04B35/628 , C04B35/645 , C04B35/653 , C04B38/009 , C04B2235/3217 , C04B2235/5427 , C04B2235/6562 , C04B2235/6565 , C04B2235/6586 , C04B2235/77 , C04B2235/80 , C04B2235/94 , C04B2235/96 , C09K8/80 , Y02P40/69 , C04B38/0074
Abstract: The present invention provides a method of preparing a proppant material by heating a reaction mixture comprising a plurality of oxides in a reactive atmosphere to a temperature above the melting point of the reaction mixture to form a melt, and then allowing the melt to solidify in a mold in the form of spherical particles. The present invention also provides a method of preparing a proppant material by heating a reaction mixture comprising a plurality of oxides and one or more additives in a reactive atmosphere to a temperature below the melting point of the reaction mixture to form a powder including one or more reaction products, and then processing the powder to form spherical particles. The present invention also provides a proppant material including spherical particles characterized by a specific gravity of about 1.0 to 3.0 and a crush strength of at least about 10,000 psi.
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公开(公告)号：US20150329769A1
公开(公告)日：2015-11-19
申请号：US14712888
申请日：2015-05-14
Applicant: CALIFORNIA INSTITUTE OF TECHNOLOGY
Inventor： Vilupanur A. Ravi , Samad A. Firdosy , Jean-Pierre Fleurial , Sabah K. Bux , Andrew Kindler
IPC: C09K8/80 , C04B35/653 , C04B35/628 , C04B35/622
CPC classification number: C09K8/805 , C04B33/1352 , C04B33/138 , C04B33/32 , C04B33/323 , C04B35/04 , C04B35/58007 , C04B35/62204 , C04B35/62655 , C04B35/628 , C04B35/645 , C04B35/653 , C04B38/009 , C04B2235/3217 , C04B2235/5427 , C04B2235/6562 , C04B2235/6565 , C04B2235/6586 , C04B2235/77 , C04B2235/80 , C04B2235/94 , C04B2235/96 , C09K8/80 , Y02P40/69 , C04B38/0074
Abstract: The present invention provides a method of preparing a proppant material by heating a reaction mixture comprising a plurality of oxides in a reactive atmosphere to a temperature above the melting point of the reaction mixture to form a melt, and then allowing the melt to solidify in a mold in the form of spherical particles. The present invention also provides a method of preparing a proppant material by heating a reaction mixture comprising a plurality of oxides and one or more additives in a reactive atmosphere to a temperature below the melting point of the reaction mixture to form a powder including one or more reaction products, and then processing the powder to form spherical particles. The present invention also provides a proppant material including spherical particles characterized by a specific gravity of about 1.0 to 3.0 and a crush strength of at least about 10,000 psi.
Abstract translation: 本发明提供了一种制备支撑剂材料的方法，该方法是将包含反应性气氛中的多种氧化物的反应混合物加热到高于反应混合物熔点的温度以形成熔体，然后使熔体固化 模具以球形颗粒的形式。 本发明还提供了一种通过在反应性气氛中将包含多种氧化物和一种或多种添加剂的反应混合物加热到低于反应混合物的熔点的温度来制备支撑剂材料的方法，以形成包含一种或多种 反应产物，然后加工粉末形成球形颗粒。 本发明还提供了包含球形颗粒的支撑剂材料，其特征在于比重为约1.0至3.0，压碎强度为至少约10,000psi。
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公开(公告)号：US09640746B2
公开(公告)日：2017-05-02
申请号：US14161641
申请日：2014-01-22
Applicant: CALIFORNIA INSTITUTE OF TECHNOLOGY
Inventor： James M. Ma , Sabah K. Bux , Jean-Pierre Fleurial , Vilupanur A. Ravi , Samad A. Firdosy , Kurt Star , Richard B. Kaner
Abstract: The present invention provides a composite thermoelectric material. The composite thermoelectric material can include a semiconductor material comprising a rare earth metal. The atomic percent of the rare earth metal in the semiconductor material can be at least about 20%. The composite thermoelectric material can further include a metal forming metallic inclusions distributed throughout the semiconductor material. The present invention also provides a method of forming this composite thermoelectric material.
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公开(公告)号：US09231180B2
公开(公告)日：2016-01-05
申请号：US14050184
申请日：2013-10-09
Applicant: California Institute of Technology
Inventor： Jean-Pierre Fleurial , Sabah K. Bux
Abstract: The present invention provides a method of preparing a nanocomposite thermoelectric material. The method includes heating a reaction mixture of a semiconductor material and a metal complex to a temperature greater than the decomposition temperature of the metal complex. The heating forms metallic inclusions having a size less than about 100 nm that are substantially evenly distributed throughout the semiconductor material forming the nanocomposite thermoelectric material. The present invention also provides a nanocomposite thermoelectric material prepared by this method.
Abstract translation: 本发明提供一种制备纳米复合热电材料的方法。 该方法包括将半导体材料和金属络合物的反应混合物加热至大于金属络合物的分解温度的温度。 加热形成尺寸小于约100nm的金属夹杂物，其基本均匀地分布在形成纳米复合热电材料的整个半导体材料中。 本发明还提供了一种通过该方法制备的纳米复合热电材料。
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7.发明申请HIGH PERFORMANCE HIGH TEMPERATURE THERMOELECTRIC COMPOSITES WITH METALLIC INCLUSIONS 有权具有金属含量的高性能高温热电复合材料公开(公告)号：US20160111619A1
公开(公告)日：2016-04-21
申请号：US14161641
申请日：2014-01-22
Applicant: CALIFORNIA INSTITUTE OF TECHNOLOGY
Inventor： James M. Ma , Sabah K. Bux , Jean-Pierre Fleurial , Vilupanur A. Ravi , Samad A. Firdosy , Kurt Star , Richard B. Kaner
Abstract: The present invention provides a composite thermoelectric material. The composite thermoelectric material can include a semiconductor material comprising a rare earth metal. The atomic percent of the rare earth metal in the semiconductor material can be at least about 20%. The composite thermoelectric material can further include a metal forming metallic inclusions distributed throughout the semiconductor material. The present invention also provides a method of forming this composite thermoelectric material.
Abstract translation: 本发明提供一种复合热电材料。 复合热电材料可以包括包含稀土金属的半导体材料。 半导体材料中的稀土金属的原子百分数可以为至少约20％。 复合热电材料还可以包括分布在整个半导体材料中的金属形成金属夹杂物。 本发明还提供了形成该复合热电材料的方法。
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