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公开(公告)号：US20170253725A1
公开(公告)日：2017-09-07
申请号：US15510880
申请日：2015-09-25
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： William D. ARENDT , Emily MCBRIDE , Steven D. ROTH , Jerry ANDREWS
IPC: C08K5/101 , C09J123/08 , C09J131/04
CPC classification number: C08K5/101 , C08K5/0016 , C08K2201/019 , C09J11/06 , C09J123/0853 , C09J131/04 , C09J2205/102 , C09J2423/04 , C09J2431/00 , C08L27/06 , C08L33/00 , C08L31/04 , C08L23/0853
Abstract: Unique 3-PPB monobenzoate analogs useful as plasticizers in polymeric dispersions, such as plastisols, melt compounds, and adhesives among other applications. The analogs are structurally similar to and/or derived from 3-phenylpropyl benzoate and heretofore were not known for use in industrial applications, particularly not as a plasticizer in polymeric applications. Depending on the application, the advantages rendered by the use of the inventive monobenzoate analogs include, among other things, excellent solvating properties and rheology, low viscosity and significantly improved viscosity over time, comparable or improved Tg suppression, set and open times, as well as health, safety and environmental advantages, over traditional plasticizers.
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公开(公告)号：US20210269621A1
公开(公告)日：2021-09-02
申请号：US17254581
申请日：2019-06-28
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： Emily MCBRIDE , Julie O. VAUGHN-BIEGE , Jason R. BUTT , Kyle Jeffrey POSSELT , William D. ARENDT
IPC: C08K5/103 , C08G18/08 , C08G18/76 , C08G18/32 , C08G18/42 , C08G18/48 , C08G18/66 , C08J3/20 , C09J175/08 , C09J175/06 , C09J11/06 , C09K3/10
Abstract: Low hydroxyl value dibenzoate plasticizer for use in a reactive polyurethane composition, including but not limited to thermoplastic and thermoset polyurethanes, wherein the plasticizer is particularly useful in TPU's, a reactive polyurethane adhesive or sealant, or a tastable polyurethane article and achieves comparable or improved properties, including without limitation compatibility, color, exudation, optical properties, MVTR, hardness, tensile strength, tear strength, rebound, compression set, and solvent swell, when compared with that achieved with traditional plasticizers, including other benzoate esters, used in polyurethane compositions.
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Patent Agency Ranking
公开(公告)号：US20160053085A1
公开(公告)日：2016-02-25
申请号：US14928364
申请日：2015-10-30
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： William D. ARENDT , Emily MCBRIDE
CPC classification number: C08K5/12 , C08K5/0016 , C08K5/06 , C08K5/10 , C08K5/103 , C08K2201/014 , C09D7/63 , C09D11/03 , C09J11/06
Abstract: Plasticizer blends comprise a triblend of diethylene glycol dibenzoate, dipropylene glycol dibenzoate, and 1,2-propylene glycol dibenzoate, in specified ratios, useful in combination with a multitude of thermoplastic polymers, thermosetting polymers, and elastomeric polymers and numerous applications, including but not limited to plastisols, adhesives, sealants, caulks, architectural coatings, industrial coatings, OEM coatings, inks, overprint varnishes, polishes, and the like. The advantages rendered by the use of the triblend depend on the type of polymer and application in which it is utilized and include among other advantages higher solvating power and lower processing time, low VOC's, reduced plasticizer freeze point, improved gelation and fusion characteristics, higher tensile strength, superior stain and extraction resistance, and improved rheology over traditional diblends of diethylene glycol dibenzoate and dipropylene glycol dibenzoate.
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公开(公告)号：US20210340339A1
公开(公告)日：2021-11-04
申请号：US17254599
申请日：2019-06-28
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： Emily MCBRIDE , Karena Kaye LINKENHOGER , Bradley Les FARRELL , Kyle Jeffrey POSSELT , William D. ARENDT
Abstract: Modifiers for use in vinyl flooring applications reduce or eliminate the need for traditional, general-purpose plasticizers in applications that require increased hardness or rigidity. High solvating, fast fusing modifiers, such as dibenzoates, added to LVT formulations provide unexpectedly increased flexural strength, hardness, indentation resistance and deflection not heretofore known or recognized in luxury vinyl tile formulations.
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公开(公告)号：US20160326345A1
公开(公告)日：2016-11-10
申请号：US15109339
申请日：2015-01-02
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： William D. ARENDT , Emily MCBRIDE , Steven D. ROTH , Eric HATCHER
Abstract: Polyester plasticizer compositions for adhesives, caulk, sealants, vinyl and other polymeric compositions comprising low molecular weight oligomeric dibenzoates prepared by end-capping a polyester plasticizer, having alternating units of glycols or diols and dibasic acids, with benzoic acid. Methods for preparing oligomeric dibenzoates include steps to reduce or eliminate residual hydroxyl content and improve plasticizer performance by adding acetic anhydride are also disclosed. Propylene glycol adipate and propylene glycol succinate polyesters with benzoic acid end-caps are particularly useful, as are hybrid benzoate/acetate end-capped polyesters formed in the process with acetic anhydride. Caulks, adhesives, sealants, and vinyl compositions comprising the oligomeric end-capped polyesters of the invention are also contemplated.
Abstract translation: 用于粘合剂，填缝料，密封剂，乙烯基和其它聚合物组合物的聚酯增塑剂组合物，其包含通过用具有二醇或二元醇和二元酸的交替单元与苯甲酸封端的聚酯增塑剂制备的低分子量低聚二苯甲酸酯。 制备低聚二苯甲酸酯的方法包括通过加入乙酸酐降低或消除残余羟基含量并提高增塑剂性能的步骤。 丙二醇己二酸酯和具有苯甲酸端帽的丙二醇琥珀酸酯聚酯是特别有用的，以及在该方法中与乙酸酐形成的混合苯甲酸酯/乙酸酯封端的聚酯。 还考虑了包含本发明的低聚端封聚酯的填缝剂，粘合剂，密封剂和乙烯基组合物。
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6.发明申请公开(公告)号：US20160017119A1
公开(公告)日：2016-01-21
申请号：US14771347
申请日：2014-03-14
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： William D. ARENDT , Emily MCBRIDE , Rebecca HANES
CPC classification number: C08K5/103 , C08J3/18 , C08J2300/00 , C08K5/101 , C08K2201/014 , C08L27/06
Abstract: A novel plasticizer blend(s) useful for plastisol compositions, including organisols, having good solvating properties, good viscosity profiles and compatibility with other plasticizers and solvents traditionally used in plastisols, comprising benzoate ester plasticizer(s) and a compatibilizing plasticizer component. Methods for preparing a plastisol having low viscosity and good rheology characteristics and for rendering a benzoate ester plasticizer, or blends thereof, compatible with organic solvents traditionally used in plastisols, by incorporating the novel plasticizer blend(s), which do not require adjusting the solubility parameters of the solvents to accommodate the plasticizer, are disclosed.
Abstract translation: 包括苯甲酸酯增塑剂和增容增塑剂组分的可用于增塑溶胶组合物的新型增塑剂混合物，包括有机溶剂，具有良好的溶剂化性能，良好的粘度特性和与其它增塑剂和传统上用于增塑溶胶的溶剂的相容性。 通过掺入不需要调节溶解度的新型增塑剂共混物，制备具有低粘度和良好流变特性的增塑溶胶和用于使苯甲酸酯增塑剂或其混合物与传统上用于增塑溶胶中的有机溶剂相容的增塑剂的方法， 公开了用于容纳增塑剂的溶剂的参数。
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7.发明申请公开(公告)号：US20140275376A1
公开(公告)日：2014-09-18
申请号：US14291660
申请日：2014-05-30
Applicant: EMERALD KALAMA CHEMICAL, LLC
Inventor： William D. ARENDT , Emily MCBRIDE
CPC classification number: C08K5/101 , C08K5/0008 , C08K5/0016 , C08K5/12 , C08L91/00 , C09D7/63 , C09D11/00 , C09J131/04 , C08L27/06 , C08L33/06
Abstract: A unique monobenzoate useful as a plasticizer in polymeric dispersions, such as plastisols and melt compounds. The monobenzoate comprises 3-phenyl propyl benzoate, a benzoate ester heretofore known as a flavoring and fragrance agent, but not previously utilized as a plasticizer in polymeric applications. Depending on the application, the advantages rendered by the use of the inventive monobenzoate include, among other things, excellent solvating properties, low viscosity, viscosity stability, and improved rheology, as well as health, safety and environmental advantages over traditional plasticizers. The monobenzoate may be used alone or in combination with a variety of plasticizers, including but not limited to phthalates, terephthalates, dibenzoates, other monobenzoates, or 1,2-cyclohexane dicarboxylate esters, and mixtures thereof.
Abstract translation: 一种独特的单苯甲酸酯，可用作聚合物分散体中的增塑剂，如增塑溶胶和熔融化合物。 单苯甲酸酯包括苯甲酸3-苯基酯，迄今为止称为调味剂和香料的苯甲酸酯酯，但以前不用作聚合物应用中的增塑剂。 根据应用，通过使用本发明的单苯甲酸酯所带来的优点包括与传统的增塑剂相比优异的溶剂化性能，低粘度，粘度稳定性和改进的流变学以及健康，安全性和环境优点。 单苯甲酸酯可以单独使用或与各种增塑剂组合使用，包括但不限于邻苯二甲酸酯，对苯二甲酸酯，二苯甲酸酯，其它单苯甲酸酯或1,2-环己烷二羧酸酯，及其混合物。
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