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公开(公告)号：US07495043B2
公开(公告)日：2009-02-24
申请号：US11147761
申请日：2005-06-08
Applicant: Jiang-Jen Lin , Chung-Ming Tsai
Inventor： Jiang-Jen Lin , Chung-Ming Tsai
CPC classification number: B82Y30/00 , C01B33/126 , C01B33/44 , Y10T428/2982
Abstract: The present invention discloses a method for producing a clay/AMO complex by modifying layered inorganic silicate clay with the intercalating agent AMO (amine-terminated Mannich oligomer). The AMO is prepared by polymerizing polyoxyalkylene amine having molecular weight over 1000, p-cresol and formaldehyde. The present invention also discloses a method for producing nanosilicate plates by extracting the AMO from the above complex with a hydroxide or a chloride of alkali metal or alkaline-earth metal. The extracted AMO can be recycled for reusing.
Abstract translation: 本发明公开了一种用嵌入剂AMO（胺封端的曼尼式低聚物）改性层状无机硅酸盐粘土制备粘土/ AMO配合物的方法。 通过聚合分子量大于1000的聚氧化烯胺，对甲酚和甲醛来制备AMO。 本发明还公开了一种通过用碱金属或碱土金属的氢氧化物或氯化物从上述配合物中提取AMO来制备纳米硅酸盐板的方法。 提取的AMO可以回收再利用。
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2.发明授权公开(公告)号：US07094815B2
公开(公告)日：2006-08-22
申请号：US10270227
申请日：2002-10-15
Applicant: Jiang-Jen Lin , Chung-Ming Tsai
Inventor： Jiang-Jen Lin , Chung-Ming Tsai
CPC classification number: B82Y30/00 , C01B33/126 , C01B33/44 , Y10T428/2982
Abstract: The present invention discloses a clay/amine complex which is an excellent surfactant and a good reinforcing agent of polymers. The complex of the present invention can be produced by modifying layered inorganic silicate clay such as montomorillonite, with an intercalating agent, AMO (amine terminal-mannich oligomer). The AMO can be obtained by polymerizing polyoxyalkylene amine having molecular weight over 1000, p-cresol and formaldehyde. The present invention further discloses a nanosilica plate, which can be obtained by extracting the above complex with a hydroxide or a chloride of alkali metal or alkaline-earth metal, and consequently, the AMO intercalating agent can be recycled for reusing.
Abstract translation: 本发明公开了一种粘土/胺络合物，它是优异的表面活性剂和聚合物的良好增强剂。 本发明的复合物可以通过用嵌层剂AMO（胺末端 - 甘露糖低聚物）改性层状无机硅酸盐粘土如蒙脱石来制备。 AMO可以通过聚合分子量大于1000的聚氧化烯胺，对甲酚和甲醛来获得。 本发明还公开了一种纳米二氧化硅板，其可以通过用碱金属或碱土金属的氢氧化物或氯化物萃取上述配合物而获得，因此可以将AMO嵌入剂再循环使用。
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公开(公告)号：US20050239943A1
公开(公告)日：2005-10-27
申请号：US11147761
申请日：2005-06-08
Applicant: Jiang-Jen Lin , Chung-Ming Tsai
Inventor： Jiang-Jen Lin , Chung-Ming Tsai
CPC classification number: B82Y30/00 , C01B33/126 , C01B33/44 , Y10T428/2982
Abstract: The present invention discloses a method for producing a clay/AMO complex by modifying layered inorganic silicate clay with the intercalating agent AMO (amine terminal-mannich oligomer). The AMO is prepared by polymerizing polyoxyalkylene amine having molecular weight over 1000, p-cresol and formaldehyde. The present invention also discloses a method for producing nanosilica plates by extracting the AMO from the above complex with a hydroxide or a chloride of alkali metal or alkaline-earth metal. The extracted AMO can be recycled for reusing.
Abstract translation: 本发明公开了一种通过用嵌入剂AMO（胺末端 - 甘露糖低聚物）改性层状无机硅酸盐粘土制备粘土/ AMO配合物的方法。 通过聚合分子量大于1000的聚氧化烯胺，对甲酚和甲醛来制备AMO。 本发明还公开了一种通过用碱金属或碱土金属的氢氧化物或氯化物从上述配合物中提取AMO来制备纳米二氧化硅板的方法。 提取的AMO可以回收再利用。
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4.发明授权Method for reducing metal ion with nanosilicate platelets and dispersing metal nanoparticle and product thereof 有权用纳米硅酸盐血小板还原金属离子并分散金属纳米粒子及其产物的方法公开(公告)号：US08952087B2
公开(公告)日：2015-02-10
申请号：US12258402
申请日：2008-10-25
Applicant: Jiang-Jen Lin , Yi-Lin Liao , Chien-Chia Chu , Chih-Wei Chiu
Inventor： Jiang-Jen Lin , Yi-Lin Liao , Chien-Chia Chu , Chih-Wei Chiu
CPC classification number: B22F9/24 , B22F1/0022 , B22F2999/00 , B82Y30/00 , B22F1/0059
Abstract: The present invention provides a method for reducing metal ions (for example, silver ions) and stably dispersing metal nanoparticles by nanosilicate platelets. An organic dispersant, nanosilicate platelets and a metal ionic solution are mixed to perform a reductive reaction, wherein the organic dispersant is tri-sodium citrate dihydrate (SCD), chitosan or polyvinyl pyrrolidone (PVP), to produce a mixture of stably dispersed metal nanoparticles.
Abstract translation: 本发明提供了还原金属离子（例如银离子）并通过纳米硅酸盐片稳定分散金属纳米粒子的方法。 将有机分散剂，纳米硅酸盐片和金属离子溶液混合以进行还原反应，其中有机分散剂是柠檬酸三钠二水合物（SCD），壳聚糖或聚乙烯吡咯烷酮（PVP）），以产生稳定分散的金属纳米颗粒 。
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公开(公告)号：US20130172447A1
公开(公告)日：2013-07-04
申请号：US13561072
申请日：2012-07-29
Applicant: Jiang-Jen Lin , Ying-Nan Chan , Jau-Yu Chiou
Inventor： Jiang-Jen Lin , Ying-Nan Chan , Jau-Yu Chiou
CPC classification number: C08K5/5399 , B82Y30/00 , C07F9/65815 , C08K9/04 , C08L63/00 , C09K21/12
Abstract: A phosphorous flame retardant including nanosilicate platelets (NSP) is made by first reacting hexachlorotriphosphazene (HCP) with poly(oxyalkylene)amine, then mixing the HCP product with nano silicate platelets (NSP) to obtain the phosphorous flame retardant including NSP. The phosphorous flame retardant can be further applied to an epoxy resin as a curing agent.
Abstract translation: 通过首先使六氯三磷腈（HCP）与聚（氧化烯）胺反应，然后将HCP产物与纳米硅酸盐血小板（NSP）混合以获得包括NSP的磷阻燃剂，制备包括纳米硅酸盐血小板（NSP）的磷阻燃剂。 磷阻燃剂可以进一步用作环氧树脂作为固化剂。
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Patent Agency Ranking
公开(公告)号：US20130005918A1
公开(公告)日：2013-01-03
申请号：US13612052
申请日：2012-09-12
Applicant: Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
Inventor： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC: C07C231/02 , C08F8/32
CPC classification number: C08F26/00
Abstract: Polymeric polyamine is produced by polymerizing polyoxyalkylene-amine and a linker. The polyoxyalkylene-amine has a structural formula H2N—R—NH2, wherein R is selected from the group consisting of dianhydride, diacid, epoxy, diisocyanate and poly(styrene-co-maleic anhydride) copolymers (SMA). The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The polymeric polyamine so produced can be used as a stabilizer or dispersant of the Ag nanoparticles.
Abstract translation: 聚合多胺通过聚合聚氧亚烷基 - 胺和接头来制备。 聚氧化烯胺具有结构式H2N-R-NH2，其中R选自二酐，二酸，环氧，二异氰酸酯和聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。 接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。 如此生产的聚合多胺可用作Ag纳米颗粒的稳定剂或分散剂。
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7.发明申请METHOD FOR PREPARING SILVER NANOPARTICLES BY EMPLOYING ETHANOLAMINE AND POLY(STYRENE-CO-MALEIC ANHYDRIDE) COPOLYMERS 有权通过使用乙醇胺和聚（苯乙烯 - 马来酸酐）共聚物制备银纳米粒子的方法公开(公告)号：US20120279352A1
公开(公告)日：2012-11-08
申请号：US13549417
申请日：2012-07-14
Applicant: Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
Inventor： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
CPC classification number: B22F9/24 , B22F1/0018 , B82Y30/00 , Y10S977/896
Abstract: The present invention provides a method for producing silver nanoparticles by employing ethanolamine. The method of this invention can be easily operated and no organic solvent is required. Ethanolamine first reacts with copolymers of poly(styrene-co-maleic anhydride) (abbreviated as SMA) to generate polymeric polymers. The polymeric polymers then reduce silver ions to silver atoms which are dispersed in the form of silver nanoparticles. Functional groups of the polymeric polymers can chelate with silver ions and be stably compatible with water or organic solvents, whereby the silver nanoparticles can be stably dispersed without aggregation and the produced silver nanoparticles.
Abstract translation: 本发明提供使用乙醇胺制造银纳米粒子的方法。 本发明的方法可以容易地操作，不需要有机溶剂。 乙醇胺首先与聚（苯乙烯 - 共 - 马来酸酐）（缩写为SMA）的共聚物反应生成聚合物聚合物。 聚合物聚合物然后将银离子还原成以银纳米颗粒形式分散的银原子。 聚合物聚合物的官能团可以与银离子螯合并与水或有机溶剂稳定地相容，由此可以稳定地分散银纳米颗粒而不会聚集，并且所制备的银纳米颗粒。
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公开(公告)号：US20120031846A1
公开(公告)日：2012-02-09
申请号：US13039335
申请日：2011-03-03
Applicant: Jiang-Jen Lin , Ru-Siou Hsu
Inventor： Jiang-Jen Lin , Ru-Siou Hsu
IPC: B01D59/30
CPC classification number: C02F1/281 , B01D17/0202 , B01J20/10 , B01J20/12 , B01J20/3204 , B01J20/3272 , C02F1/285 , C02F1/288 , C02F1/681 , C02F2001/425 , C02F2101/32 , C10G25/003 , C10G33/04
Abstract: The present invention provides a method for collecting oil with a modified clay. By mixing the modified clay and oil, the oil can be adsorbed to the clay. The modified clay is obtained by intercalating a hydrophobic polymer such as acidified poly(oxyalkylene)-amine into layered silicate clay, mica or talc to enlarge the interlayer space. The modified clay thus becomes hydrophobic and adsorption to the oil is promoted.
Abstract translation: 本发明提供一种用改性粘土收集油的方法。 通过混合改性粘土和油，油可以吸附到粘土上。 改性粘土是通过将层状硅酸盐粘土，云母或滑石中的疏水性聚合物如酸化的聚（氧化烯） - 胺嵌入而获得的，以扩大层间空间。 因此，改性粘土变得疏水，促进了对油的吸附。
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9.发明申请ORGANIC/INORGANIC COMPOSITIVE DISPERSANT INCLUDING INORGANIC CLAY AND ORGANIC SURFACTANT 有权有机/无机组合物分散剂，包括无机粘土和有机表面活性剂公开(公告)号：US20100274036A1
公开(公告)日：2010-10-28
申请号：US12765853
申请日：2010-04-22
Applicant: Jiang-Jen Lin , Wei-Ting Chen , Yen-Chi Hsu , Chih-Wei Chiu
Inventor： Jiang-Jen Lin , Wei-Ting Chen , Yen-Chi Hsu , Chih-Wei Chiu
IPC: C07F7/02
CPC classification number: C08K13/02 , B01F17/0007 , B01F17/0021 , B01F17/0042 , B01F17/0085
Abstract: The present invention provides an organic/inorganic compositive dispersant and a method for producing the same. The compositive dispersant comprises a complex of inorganic clay and an organic surfactant. The compositive dispersant is produced by reacting inorganic clay with the organic surfactant in a solvent to generate a complex. The inorganic clay is layered or platelet. The organic surfactant is an anionic surfactant such as alkyl sulfates, a nonionic surfactant such as octylphenol polyethoxylate and polyoxyethylene alkyl ether, or a cationic surfactant such as fatty (C12˜C32) quaternary ammonium salts and fatty (C12˜C32) quaternary ammonium chlorides.
Abstract translation: 本发明提供一种有机/无机复合分散剂及其制造方法。 复合分散剂包括无机粘土和有机表面活性剂的复合物。 复合分散剂通过无机粘土与有机表面活性剂在溶剂中反应生成复合物。 无机粘土是分层的或血小板的。 有机表面活性剂是阴离子表面活性剂，如烷基硫酸盐，非离子表面活性剂如辛基苯酚聚乙氧基化物和聚氧乙烯烷基醚，或阳离子表面活性剂如脂肪（C12〜C32）季铵盐和脂肪（C12〜C32）季铵氯化物。
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10.发明授权公开(公告)号：US07022299B2
公开(公告)日：2006-04-04
申请号：US10270209
申请日：2002-10-15
Applicant: Jiang-Jen Lin , Chin-Cheng Chou , Tzong-Yuan Juang
Inventor： Jiang-Jen Lin , Chin-Cheng Chou , Tzong-Yuan Juang
IPC: C01B33/12
CPC classification number: C01B33/44
Abstract: The present invention discloses an exfoliative clay and a derivative thereof and a method for producing the same. The exfoliative clay is formed by emulsion exfoliating an inorganic layered silicate clay with an amphibious intercalating agent by powerfully stirring at 60–180° C. and not less than 14.7 psig. The amphibious intercalating agent is obtained by copolymerizing polyoxyalkylene amine having molecular weight over 1,800 and polypropylene-grafting-maleic anhydride (PP-g-MA). Before emulsion exfoliation, the intercalating agent is acidified with an inorganic acid. The acidification is the key step for obtaining nanoscale of emulsifying particles less than 100 nm for the exfoliation. The exfoliative clay can be further extracted with a hydroxide or a chloride of alkali metal or alkaline-earth metal to obtain a derivative in the form of nanosilica plates which is free of organic portions.
Abstract translation: 本发明公开了一种剥离性粘土及其衍生物及其制造方法。 通过在60-180℃和不低于14.7psig的强力搅拌下将无机层状硅酸盐粘土与两栖嵌入剂乳化成剥离形成剥离性粘土。 通过共聚分子量超过1800的聚氧亚烷基胺和聚丙烯接枝 - 马来酸酐（PP-g-MA）获得两栖嵌入剂。 在乳液脱落之前，插入剂用无机酸酸化。 酸化是获得纳米级乳化颗粒小于100nm的剥落的关键步骤。 剥离性粘土可以用碱金属或碱土金属的氢氧化物或氯化物进一步提取，得到无机部分的纳米二氧化硅板形式的衍生物。
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