Methods and Systems for Concentrating a Gas Sample

    公开(公告)号:US20240094101A1

    公开(公告)日:2024-03-21

    申请号:US18273561

    申请日:2022-01-28

    CPC classification number: G01N1/4022 G01N30/12 G01N2001/4033 G01N2030/025

    Abstract: The present techniques, including methods and systems, relate to obtaining or producing a concentrated gas sample from a non-concentrated gas sample with a trap that is not inline with (or indirectly connected to) a chromatographic method, and injecting a controlled volume of the concentrated gas sample in a sample loop including a valve or similar chromatographic component through a sample line. The method includes preparing the concentrated gas sample from the non-concentrated gas sample with a trap; controlling a temperature of an internal volume of the trap to reach a release temperature; injecting the concentrated gas sample in a sample line towards a sample loop, the sample line and sample loop being at a sub-atmospheric pressure; and operating the sample loop to release the concentrated gas sample contained in the sample loop in a chromatographic method, wherein the trap is not inline with the chromatographic method.

    Discharge-based photo ionisation detector for use with a gas chromatography system

    公开(公告)号:US10761059B2

    公开(公告)日:2020-09-01

    申请号:US15555610

    申请日:2016-03-07

    Inventor: Yves Gamache

    Abstract: A discharge-based photo ionisation detector (PID) for use with gas chromatography systems is provided. The PID includes a discharge zone in which a plasma can be generated, resulting in the emission of energetic photons. The PID further includes an ionisation zone in which the gas sample to be analysed is bombarded by the photons created in the discharge zone, photo ionising the impurities in the gas sample. The generated current is measured in order to measure the concentration of impurities in the gas sample. Plasma localizing of the plasma in the discharge zone and optical monitoring of the emission from the plasma in the discharge zone may be provided. Methods using such a PID with a split input from a chromatography column or with inputs from two different chromatography columns are provided.

    Method and apparatus for analysing a gas chromatography elution peak

    公开(公告)号:US11467140B2

    公开(公告)日:2022-10-11

    申请号:US16764529

    申请日:2018-11-14

    Abstract: Methods and systems for measuring, in a gas stream, an analyte concentration level from a gas chromatography elution peak outputted by a gas chromatography system are provided. The method includes receiving an analyte signal representative of the gas chromatography elution peak in the time domain, converting the analyte signal from the time-domain to the frequency domain, in the frequency domain, preprocessing the analyte signal to distinguish frequencies of the analyte signal, integrating the analyte signal after preprocessing to obtain a redressed analyte signal in the time domain, the redressed analyte signal having a substantially Gaussian shape, and processing the redressed analyte signal to obtain the analyte concentration level. The system includes a detector operable for generating the analyte signal and one or more processors configured for preprocessing and integrating the analyte signal to obtain the redressed analyte signal and processing the redressed analyte signal to obtain the analyte concentration level.

    Actuator
    5.
    发明授权
    Actuator 有权
    执行器

    公开(公告)号:US09145977B2

    公开(公告)日:2015-09-29

    申请号:US14487374

    申请日:2014-09-16

    Inventor: Yves Gamache

    Abstract: An actuator for actuating a plunger of a valve is provided. The actuator has an inlet and includes first and second hollow caps. A main actuation assembly is provided between the caps. The main actuation assembly includes a deformable diaphragm; first and second chambers, static sealing elements and a main piston movable between actuated and unactuated positions. A biasing mechanism biases the piston in the unactuated position. When pressurized gas is flown through the inlet and/or drawn from the outlet of the actuator, the first chamber expands, moving the main piston from the unactuated position to the actuated position, an actuating stem connected to the main piston thereby sliding within a channel provided in the bottom cap. Stackable actuating assemblies can also be used between the caps. Using static sealing elements advantageously avoids friction between moving parts.

    Abstract translation: 提供了用于致动阀的柱塞的致动器。 致动器具有入口并包括第一和第二中空盖。 主驱动组件设置在盖之间。 主致动组件包括可变形隔膜; 第一和第二腔室,静密封元件和可在致动位置和未致动位置之间移动的主活塞。 偏压机构将活塞偏压在未致动位置。 当压缩气体流过入口和/或从​​致动器的出口抽出时,第一室膨胀,将主活塞从未致动位置移动到致动位置,连接到主活塞的致动杆由此在通道内滑动 提供在底盖。 也可以在盖之间使用可堆叠的致动组件。 使用静态密封元件有利地避免了运动部件之间的摩擦。

    METHODS AND SYSTEMS FOR CHROMATOGRAPHICALLY ANALYZING A TEST SAMPLE

    公开(公告)号:US20240060943A1

    公开(公告)日:2024-02-22

    申请号:US18267547

    申请日:2021-12-16

    Inventor: Yves Gamache

    Abstract: There are provided techniques, including methods and systems, for chromatographically analyzing a test sample. The techniques include obtaining a sample chromatogram of the test sample with a chromatography system, the chromatography system including a detector having an adjustable response factor. The techniques also include adjusting, while obtaining the sample chromatogram, the response factor of the detector based on a compensation signal for compensating expected chromatographic artefacts to obtain an artefact-compensated sample chromatogram. The disclosed techniques allow compensating for chromatographic artefacts, which include baseline drift(s) and/or peak tailing(s), during acquisition of chromatograms.

    Diaphragm-Sealed Valve with Improved Actuator Design
    7.
    发明申请
    Diaphragm-Sealed Valve with Improved Actuator Design 有权
    具有改进的致动器设计的隔膜密封阀

    公开(公告)号:US20150083259A1

    公开(公告)日:2015-03-26

    申请号:US14377670

    申请日:2013-02-18

    Inventor: Yves Gamache

    Abstract: A valve comprising a valve cap, a valve body and a diaphragm positioned between the valve cap and the valve body. The valve further has a plurality of plungers movable, by an actuation system, between a closed position where the plunger engages the diaphragm, and an open position where the plunger is disengaged from the diaphragm. Each plunger comprises a base section connected to the actuation system and having a head projecting away therefrom; a top section extending between the base section and the diaphragm, the top section having a foot in contact with the head of the base section; and a biasing mechanism biasing the top section away from the diaphragm when the plunger is in the open position. Tangential contact points may also be provided between components of the actuation and the biasing mechanism for preventing a misalignment of the actuation system within the valve body.

    Abstract translation: 一种阀,包括阀盖,阀体和位于阀盖和阀体之间的隔膜。 阀还具有多个柱塞,其可通过致动系统在柱塞与隔膜接合的关闭位置和柱塞与隔膜分离的打开位置之间移动。 每个柱塞包括连接到致动系统并且具有从其突出的头部的基部; 在所述基部和所述隔膜之间延伸的顶部,所述顶部具有与所述基部的头部接触的脚; 以及当所述柱塞处于打开位置时偏置所述顶部远离所述隔膜的偏置机构。 也可以在致动部件和偏置机构之间提供切向接触点,以防止致动系统在阀体内的不对准。

    Emission-based detector for capillary gas chromatography

    公开(公告)号:US11879849B2

    公开(公告)日:2024-01-23

    申请号:US17732248

    申请日:2022-04-28

    Inventor: Yves Gamache

    Abstract: An emission-based detector for use in conjunction with capillary chromatography or other applications involving a gas sample having a small volume is provided. The detector is based on optical emission from a plasma medium. An optical cartridge or other detection and/or processing means may be provided to receive and analyse the emitted radiation and thereby obtain information on the gas to be analysed. The emission-based detector includes a gas inlet, a gas outlet and a capillary channel which is in fluid communication with the gas inlet and gas outlet. The capillary channel acts as the plasma chamber. Preferably, the capillary channel has transversal dimensions of the same order as the cross-section of typical chromatography capillary columns and defines a winding path within the detection area. A multi-cell emission-based detector and a method of analysing a gas sample using multiple detection cells are also provided.

    Emission-based detector for capillary gas chromatography

    公开(公告)号:US11340173B2

    公开(公告)日:2022-05-24

    申请号:US15737354

    申请日:2016-06-23

    Inventor: Yves Gamache

    Abstract: An emission-based detector for use in conjunction with capillary chromatography or other applications involving a gas sample having a small volume is provided. The detector is based on optical emission from a plasma medium. An optical cartridge or other detection and/or processing means may be provided to receive and analyse the emitted radiation and thereby obtain information on the gas to be analysed. The emission-based detector includes a gas inlet, a gas outlet and a capillary channel which is in fluid communication with the gas inlet and gas outlet. The capillary channel acts as the plasma chamber. Preferably, the capillary channel has transversal dimensions of the same order as the cross-section of typical chromatography capillary columns and defines a winding path within the detection area. A multi-cell emission-based detector and a method of analysing a gas sample using multiple detection cells are also provided.

    EMISSION-BASED DETECTOR FOR CAPILLARY GAS CHROMATOGRAPHY

    公开(公告)号:US20180164219A1

    公开(公告)日:2018-06-14

    申请号:US15737354

    申请日:2016-06-23

    Inventor: Yves Gamache

    Abstract: An emission-based detector for use in conjunction with capillary chromatography or other applications involving a gas sample having a small volume is provided. The detector is based on optical emission from a plasma medium. An optical cartridge or other detection and/or processing means may be provided to receive and analyse the emitted radiation and thereby obtain information on the gas to be analysed. The emission-based detector includes a gas inlet, a gas outlet and a capillary channel which is in fluid communication with the gas inlet and gas outlet. The capillary channel acts as the plasma chamber. Preferably, the capillary channel has transversal dimensions of the same order as the cross-section of typical chromatography capillary columns and defines a winding path within the detection area. A multi-cell emission-based detector and a method of analysing a gas sample using multiple detection cells are also provided.

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