HYDRATED CRYSTALLINE FORM OF 2-ACRYLAMIDO-2-METHYLPROPANE SULFONIC ACID

    公开(公告)号:US20220332680A1

    公开(公告)日:2022-10-20

    申请号:US17664208

    申请日:2022-05-19

    Applicant: SPCM SA

    Abstract: The present invention relates to a hydrated crystalline form of 2-acrylamido-2-methylpropane sulfonic acid having a 2-theta powder X-ray diffraction diagram comprising peaks at 10.58°, 11.2°, 12.65°, 13.66°, 16.28°, 18.45°, 20°, 20.4°, 22.5°, 25.5°, 25.88°, 26.47°, 28.52°, 30.28°, 30.8°, 34.09°, 38.19°, 40.69°, 41.82°, 43.74°, 46.04° degrees (+/−0.1°).
    The present invention also relates to a production method for this form of 2-acrylamido-2-methylpropane sulfonic acid and a preparation method for an aqueous solution A of a salt of this form of 2-acrylamido-2-methylpropane sulfonic acid, and the (co)polymer of this form of -acrylamido-2-methylpropane sulfonic acid.

    HYDRATED CRYSTALLINE FORM OF 2-ACRYLAMIDO-2-METHYLPROPANE SULFONIC ACID

    公开(公告)号:US20220289672A1

    公开(公告)日:2022-09-15

    申请号:US17664209

    申请日:2022-05-19

    Applicant: SPCM SA

    Abstract: The present invention relates to a hydrated crystalline form of 2-acrylamido-2-methylpropane sulfonic acid having a 2-theta powder X-ray diffraction diagram comprising peaks at 10.58°, 11.2°, 12.65°, 13.66°, 16.28°, 18.45°, 20°, 20.4°, 22.5°, 25.5°, 25.88°, 26.47°, 28.52°, 30.28°, 30.8°, 34.09°, 38.19°, 40.69°, 41.82°, 43.74°, 46.04° degrees (+/−0.1°).
    The present invention also relates to a production method for this form of 2-acrylamido-2-methylpropane sulfonic acid and a preparation method for an aqueous solution A of a salt of this form of 2-acrylamido-2-methylpropane sulfonic acid, and the (co)polymer of this form of -acrylamido-2-methylpropane sulfonic acid.

    METHOD FOR THE PURIFICATION OF ACRYLAMIDO-2-METHYL-2-PROPANESULPHONIC ACID

    公开(公告)号:US20220089530A1

    公开(公告)日:2022-03-24

    申请号:US17447754

    申请日:2021-09-15

    Applicant: SPCM SA

    Abstract: The invention relates to a method for the purification of acrylamido-2-methyl-2-propanesulphonic acid comprising the following successive steps:
    1) preparation of a suspension of acrylamido-2-methyl-2-propanesulphonic acid crystals by distillation of an aqueous solution of acrylamido-2-methyl-2-propanesulphonic acid in order to obtain a suspension of acrylamido-2-methyl-2-propanesulphonic acid crystals, 2) isolation of the acrylamido-2-methyl-2-propanesulphonic acid crystals generally by solid/liquid separation from said suspension in order to isolate said acrylamido-2-methyl-2-propanesulphonic acid crystals, characterised in that the distillation step is carried out continuously and at a pressure below atmospheric pressure. The invention also relates to a polymer obtained from acrylamido-2-methyl-2-propanesulphonic acid crystals or its salts, obtained according to such a method, and to the use of said polymer in oil and gas recovery, in water treatment, in sludge treatment, in manufacturing paper, in construction, in mining, in cosmetic formulation, in detergent formulation, in textile making, or in agriculture.

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