公开(公告)号：US3729385A

公开(公告)日：1973-04-24

申请号：US3729385D

申请日：1971-07-29

Applicant: SUN RESEARCH DEVELOPMENT

Inventor： TUMOLO A

IPC: C07C41/06 ,  C07C41/12

CPC classification number: C07C41/06 ,  C07C41/42 ,  C07C41/46 ,  C07C43/04

Abstract: Propylene trimer methyl ether is of interest as a non-air polluting solvent; however, in the production of the ether, there is a major proportion of unreacted propylene trimer from which the ether must be separated. Distilling the propylene trimer methyl ether out of the ether-trimer mixture results in up to 30 percent degradation of the ether. By adding 0.1-10 weight percent quinoline to the distillation mixture, however, reduces degradation loss to less than 5 percent.

Abstract translation: 丙烯三聚甲醚作为非空气污染溶剂是有意义的; 然而，在醚的生产中，存在主要比例的未反应的丙烯三聚体，其中乙醚必须从其中分离出来。 将丙烯三聚体甲醚从乙醚 - 三聚体混合物中蒸馏，导致乙醚降解高达30％。 然而，通过向蒸馏混合物中加入0.1-10重量％的喹啉，将降解损失降低到小于5％。