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    Method for producing material libraries by means of electrochemical deposition
    2.
    发明授权
    Method for producing material libraries by means of electrochemical deposition 失效
    通过电化学沉积法生产材料库的方法

    公开(公告)号：US06896783B2

    公开(公告)日：2005-05-24

    申请号：US10168099

    申请日：2000-12-12

    Applicant: Stephan A. Schunk ,  Dirk Demuth ,  Hartmut Hibst

    Inventor： Stephan A. Schunk ,  Dirk Demuth ,  Hartmut Hibst

    IPC: B01J19/00 ,  B01J35/00 ,  B01J37/34 ,  C40B40/18 ,  C40B60/14 ,  C25D5/00

    CPC classification number: B01J35/0006 ,  B01J19/0046 ,  B01J37/348 ,  B01J2219/00283 ,  B01J2219/00286 ,  B01J2219/00306 ,  B01J2219/00333 ,  B01J2219/00511 ,  B01J2219/0052 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00707 ,  B01J2219/00713 ,  B01J2219/00745 ,  B01J2219/00752 ,  C40B40/18 ,  C40B60/14

    Abstract: The invention relates to a method for combinatorially producing a library of materials by means of an electrochemical deposition in an array. The inventive library is made from an array of containers that consist of an electroconductive material, are open to the top and are electroconductively connected to a shared current supply device and is made from a corresponding array of auxiliary electrodes that are electroconductively connected to a shared current supply device and are arranged in such a way that an auxiliary electrode plunges into a container respectively or can be introduced therein without touching said container. The inventive method comprises the following steps: filling the containers with electrolytes having different compositions and containing electrolytically separable elements and applying an electric voltage between the current supply devices of the containers and auxiliary electrodes for obtaining an electrolytic deposition on the surfaces of the containers.

    Abstract translation: 本发明涉及通过阵列中的电化学沉积来组合地制备材料库的方法。 本发明的库由一组由导电材料构成的容器组成，该导电材料通向顶部，并且电导连接到共享电流供应装置，并且由相应的辅助电极阵列制成，所述辅助电极阵列电导连接到共享电流 供给装置并且以这样的方式布置，使得辅助电极分别插入容器中或可以在其中引入而不接触所述容器。 本发明的方法包括以下步骤：用不同组成的电解质填充容器并含有电解分离元件，并在容器的电流供应装置和辅助电极之间施加电压，以在容器的表面上获得电解沉积。

    Computer-aided optimization of substance libraries
    3.
    发明授权
    Computer-aided optimization of substance libraries 失效
    物质图书馆计算机辅助优化

    公开(公告)号：US06862533B2

    公开(公告)日：2005-03-01

    申请号：US09876142

    申请日：2001-06-08

    Applicant: Wolfgang Strehlau ,  John Michael Newsam ,  Dirk Demuth ,  Wolfram Stichert ,  Armin Brenner ,  Stephan A. Schunk ,  Jens Klein

    Inventor： Wolfgang Strehlau ,  John Michael Newsam ,  Dirk Demuth ,  Wolfram Stichert ,  Armin Brenner ,  Stephan A. Schunk ,  Jens Klein

    IPC: B01J19/00 ,  C07B61/00 ,  C40B30/08 ,  C40B40/18 ,  G06F19/16 ,  G01N31/00

    CPC classification number: B01J19/0046 ,  B01J2219/00689 ,  B01J2219/00695 ,  B01J2219/007 ,  B01J2219/00702 ,  B01J2219/0072 ,  B01J2219/00745 ,  B01J2219/00747 ,  B01J2219/00754 ,  C40B30/08 ,  C40B40/18 ,  G06F19/16

    Abstract: The invention relates to a method for the automated production and iterative automated optimization of a substance library and/or at least one reaction parameter relating to a performance characteristic comprising at least two substances comprising the steps of: a) defining at least one production parameter and at least one test parameter; b) automated preparation of a substance library by producing at least two substances on the basis of the at least one production parameter; c) automated testing of the at least two substances of the substance library with respect to at least one performance characteristic on the basis of the at least one test parameter; d) evaluating the test using electronic data analysis; e) varying the at least one production parameter and/or the at least one test parameter for optimizing the performance characteristics, and single or repeated repetition of steps b) to e) or c) to e); characterized in that the steps b) to e) are carried out in an integrated automated process.

    Abstract translation: 本发明涉及用于物质文库的自动生产和迭代自动优化的方法和/或与包括至少两种物质的性能特征相关的至少一个反应参数的方法，包括以下步骤：a）定义至少一个生产参数和 至少一个测试参数; b）通过基于至少一个生产参数生产至少两种物质来自动制备物质文库; c）基于所述至少一个测试参数，相对于至少一个性能特征自动测试所述物质文库的至少两种物质; d）使用电子数据分析评估测试; e）改变所述至少一个生产参数和/或所述至少一个测试参数以优化所述性能特征，以及步骤b）至e）或c）至e）的单个或重复重复; 其特征在于步骤b）至e）以综合自动化过程进行。

    Process and apparatus for transferring air-sensitive substances
    4.
    发明授权
    Process and apparatus for transferring air-sensitive substances 失效
    用于转移空气敏感物质的方法和设备

    公开(公告)号：US07250307B2

    公开(公告)日：2007-07-31

    申请号：US09997285

    申请日：2001-11-30

    Applicant: Stephan A. Schunk

    Inventor： Stephan A. Schunk

    IPC: G01N30/00

    CPC classification number: B01J4/02 ,  B01J19/0046 ,  B01J2219/00283 ,  B01J2219/00337 ,  B01J2219/00342 ,  B01J2219/00389 ,  B01J2219/00391 ,  B01J2219/00418 ,  B01J2219/00481 ,  B01J2219/00585 ,  B01J2219/00689 ,  B01J2219/00691 ,  B01J2219/0072 ,  B01J2219/00722 ,  B01J2219/00738 ,  C40B40/14 ,  C40B60/14 ,  Y10T436/25 ,  Y10T436/2575

    Abstract: A process is provided for transferring and releasing substances which are air-sensitive or moisture-sensitive or light-sensitive, or air-sensitive and moisture-sensitive, or air-sensitive and light-sensitive, or moisture-sensitive and light-sensitive, or air-sensitive, moisture-sensitive and light-sensitive, at least one substance (20) which is air-sensitive or moisture-sensitive or light-sensitive, or air-sensitive and moisture-sensitive, or air-sensitive and light-sensitive, or moisture-sensitive and light-sensitive, or air-sensitive, moisture-sensitive and light-sensitive. The process comprises removing the substances after preparation under a protective gas atmosphere, from a synthesis chamber, wherein, during said removing, the substances are surrounded by at least one means (32, 34) for protecting the substances and then transferring the substances to at least one test reactor (50, 60), wherein the transfer takes place in a protective-gas-free chamber and at least one substance (20) is freed in the test reactor (50, 60) from the means (32, 34) protecting it using at least one apparatus or by means of at least one process.

    Abstract translation: 提供了一种用于转移和释放空气敏感或湿度敏感或光敏感或对空气敏感和湿气敏感或对空气敏感和光敏感或湿度敏感和光敏感的物质的方法， 或空气敏感，湿气敏感和光敏感的至少一种物质（20），其对于空气敏感或湿度敏感或光敏感，或对空气敏感和湿气敏感，或空气敏感和光敏性， 敏感或湿度敏感和光敏感，或空气敏感，湿度敏感和光敏感。 该方法包括在保护气体气氛下从合成室中除去物质，其中在所述除去期间，物质被至少一个用于保护物质的装置（32,34）包围，然后将物质转移到 至少一个测试反应器（50,60），其中所述转移发生在无保护气体的室中，并且在所述测试反应器（50,60）中从所述装置（32,34）中释放出至少一种物质（20） 使用至少一个装置或通过至少一个处理来保护它。

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