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公开(公告)号：US09084977B2
公开(公告)日：2015-07-21
申请号：US13340569
申请日：2011-12-29
Applicant: Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
Inventor： Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
CPC classification number: B01J8/1827 , B01J8/002 , B01J8/0278 , B01J8/44 , Y10T137/0318 , Y10T137/8593
Abstract: A method, system, and apparatus for lift gas distribution are disclosed. According to one embodiment, a lift gas distributor comprises a plate having a surface and an underside, the plate having a first diameter; a center section of the plate having a second diameter, wherein the first diameter is larger than the second diameter; a predetermined number of holes having a third diameter drilled into the surface of the plate, the holes drilled at an angle, the holes evenly distributed in the center section; and a plurality of tubes welded onto the underside of the plate, each tube having a predetermined length, wherein each tube is welded onto each hole. Lift gas passes through the tubes and holes into a reactor.
Abstract translation: 公开了用于提升气体分配的方法，系统和装置。 根据一个实施例，提升气体分配器包括具有表面和下侧的板，该板具有第一直径; 所述板的中心部分具有第二直径，其中所述第一直径大于所述第二直径; 预定数量的孔具有钻进板的表面的第三直径，孔以一定角度钻出，孔均匀地分布在中心部分中; 以及焊接在板的下侧上的多个管，每个管具有预定的长度，其中每个管被焊接到每个孔上。 提升气体通过管和孔进入反应堆。
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公开(公告)号：US06046125A
公开(公告)日：2000-04-04
申请号：US55690
申请日：1998-04-06
Applicant: Stephen K. Pavel
Inventor： Stephen K. Pavel
Abstract: The present invention discloses aqueous methods for enhancing the acid sites of fluid catalytic cracking (FCC) catalysts. The methods comprise the steps of contacting an FCC catalyst, either spent or fresh, with an aqueous solution comprising water, an inorganic acid substantially free of chloride and aluminum. The acid is preferably sulfurous or sulfuric acid. The aluminum is provided by an aluminum source selected from the group consisting of the alumina trihydrates and aluminum oxide. Chloride contamination of the aluminum source should be minimal, preferably less than about 1000 ppm chloride, more preferably less than about 200 ppm chloride. The pH of the aqueous solution is adjusted to about 3-12 by the addition of a sufficient quantity of ammonium hydroxide. The FCC catalyst is added to this solution, preferably with stirring, in a weight ratio of about 1 part catalyst to about 1-10 parts water to prepare an aqueous slurry. Upon stabilization of the pH of the aqueous slurry, enhancement of the acid sites of the catalyst is achieved and the catalyst may be separated from the slurry and, if desired, washed. This simple, aqueous process reduces the level of many metal poisons on the FCC catalyst and produces a catalyst having an enhanced number of acid reaction sites.
Abstract translation: 本发明公开了用于增强流化催化裂化（FCC）催化剂的酸性位点的水性方法。 所述方法包括以下步骤：将消耗或新鲜的FCC催化剂与包含水，基本上不含氯化物和铝的无机酸的水溶液接触。 酸优选为亚硫酸或硫酸。 铝由选自三水合氧化铝和氧化铝的铝源提供。 铝源的氯化物污染应该是最小的，优选小于约1000ppm氯化物，更优选小于约200ppm氯化物。 通过加入足够量的氢氧化铵将水溶液的pH调节至约3-12。 将FCC催化剂优选在搅拌下加入到该溶液中，重量比为约1份催化剂至约1-10份水以制备含水浆料。 在稳定水性浆料的pH后，实现催化剂的酸性位置的增强，并且催化剂可以与浆料分离，并且如果需要，可以洗涤。 这种简单的含水方法降低了FCC催化剂上的许多金属毒素的水平，并产生了具有增加数量的酸反应位点的催化剂。
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Patent Agency Ranking
3.发明授权公开(公告)号：US09162171B2
公开(公告)日：2015-10-20
申请号：US13341854
申请日：2011-12-30
Applicant: Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
Inventor： Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
CPC classification number: B04C5/04 , B01D45/12 , B01D45/16 , B01D50/002 , B04C5/15 , C10B49/22 , C10B55/10 , C10G2300/40
Abstract: A method, system, and apparatus for separation in processing of feedstocks are disclosed. According to one embodiment, an apparatus comprises a tubular vessel having a square pipe entry and a vapor outlet, wherein the vapor outlet is positioned at the top of the tubular vessel, and wherein the square pipe entry is tangential to an inner diameter of the tubular vessel; a barrel positioned below the tubular vessel; and a double isolation knife valve positioned between the tubular vessel and the barrel, wherein a stream of gas and solids enters the tubular vessel through the square pipe entry, and wherein the gas and solids are separated by using centrifugal force, and wherein the gas exits the vapor outlet and the solids are collected in the barrel.
Abstract translation: 公开了一种在原料加工中分离的方法，系统和装置。 根据一个实施例，一种装置包括具有方形管入口和蒸汽出口的管状容器，其中蒸汽出口位于管状容器的顶部，并且其中方形管入口与管状物的内径相切 船只; 位于管状容器下方的桶; 以及位于管状容器和桶之间的双隔离刀阀，其中气体和固体物流通过方形管入口进入管状容器，并且其中气体和固体通过离心力分离，并且其中气体离开 蒸汽出口和固体被收集在桶中。
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公开(公告)号：US20120168537A1
公开(公告)日：2012-07-05
申请号：US13340487
申请日：2011-12-29
Applicant: Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
Inventor： Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
IPC: A62C31/02
CPC classification number: B01J4/002 , B01J19/26 , B01J2204/002 , B01J2219/00247 , B01J2219/00252
Abstract: Improved reactor feed nozzles are disclosed. According to one embodiment, a feed nozzle comprises an inner tubing encased within an outer heat shield tubing, a first circular hole fabricated in the inner tubing, the first circular hole having a first diameter and serving as a discharge hole, a second circular hole fabricated in the outer heat shield tubing, the second circular hole having a second diameter, wherein the second diameter is larger than the first diameter; and a welded tip for extending a flow path at a declining angle, the welded tip having a section extending at a predetermined angle from the inner tubing to the discharge hole.
Abstract translation: 公开了改进的反应器进料喷嘴。 根据一个实施例，进料喷嘴包括封装在外部热屏蔽管内的内管，在内管中制造的第一圆形孔，第一圆孔具有第一直径并用作排出孔，第二圆孔制造 在所述外部隔热管中，所述第二圆形孔具有第二直径，其中所述第二直径大于所述第一直径; 以及用于以下降角度延伸流动路径的焊接尖端，所述焊接尖端具有从内管延伸到排出孔的预定角度的部分。
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5.发明申请公开(公告)号：US20120167767A1
公开(公告)日：2012-07-05
申请号：US13341854
申请日：2011-12-30
Applicant: Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
Inventor： Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
IPC: B01D45/16
CPC classification number: B04C5/04 , B01D45/12 , B01D45/16 , B01D50/002 , B04C5/15 , C10B49/22 , C10B55/10 , C10G2300/40
Abstract: A method, system, and apparatus for separation in processing of feedstocks are disclosed. According to one embodiment, an apparatus comprises a tubular vessel having a square pipe entry and a vapor outlet, wherein the vapor outlet is positioned at the top of the tubular vessel, and wherein the square pipe entry is tangential to an inner diameter of the tubular vessel; a barrel positioned below the tubular vessel; and a double isolation knife valve positioned between the tubular vessel and the barrel, wherein a stream of gas and solids enters the tubular vessel through the square pipe entry, and wherein the gas and solids are separated by using centrifugal force, and wherein the gas exits the vapor outlet and the solids are collected in the barrel.
Abstract translation: 公开了一种在原料加工中分离的方法，系统和装置。 根据一个实施例，一种装置包括具有方形管入口和蒸汽出口的管状容器，其中蒸汽出口位于管状容器的顶部，并且其中方形管入口与管状物的内径相切 船只; 位于管状容器下方的桶; 以及位于管状容器和桶之间的双隔离刀阀，其中气体和固体物流通过方形管入口进入管状容器，并且其中气体和固体通过离心力分离，并且其中气体离开 蒸汽出口和固体被收集在桶中。
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公开(公告)号：US20120167989A1
公开(公告)日：2012-07-05
申请号：US13340569
申请日：2011-12-29
Applicant: Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
Inventor： Stephen K. Pavel , Michael A. Silverman , Steven A. Kalota
IPC: F17D1/00
CPC classification number: B01J8/1827 , B01J8/002 , B01J8/0278 , B01J8/44 , Y10T137/0318 , Y10T137/8593
Abstract: A method, system, and apparatus for lift gas distribution are disclosed. According to one embodiment, a lift gas distributor comprises a plate having a surface and an underside, the plate having a first diameter; a center section of the plate having a second diameter, wherein the first diameter is larger than the second diameter; a predetermined number of holes having a third diameter drilled into the surface of the plate, the holes drilled at an angle, the holes evenly distributed in the center section; and a plurality of tubes welded onto the underside of the plate, each tube having a predetermined length, wherein each tube is welded onto each hole. Lift gas passes through the tubes and holes into a reactor.
Abstract translation: 公开了用于提升气体分配的方法，系统和装置。 根据一个实施例，提升气体分配器包括具有表面和下侧的板，该板具有第一直径; 所述板的中心部分具有第二直径，其中所述第一直径大于所述第二直径; 预定数量的孔，其具有在板的表面钻出的第三直径，以一定角度钻出的孔，均匀分布在中心部分中的孔; 以及焊接在板的下侧上的多个管，每个管具有预定的长度，其中每个管被焊接到每个孔上。 提升气体通过管和孔进入反应堆。
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公开(公告)号：US6034017A
公开(公告)日：2000-03-07
申请号：US79100
申请日：1998-05-14
Applicant: Stephen K. Pavel
Inventor： Stephen K. Pavel
Abstract: The present invention discloses aqueous methods for enhancing the acid sites of fluid catalytic cracking (FCC) catalysts. The methods comprise the steps of contacting an FCC catalyst, either spent or fresh, with an aqueous solution comprising water, and a source of both phosphorus and aluminum. Optionally the solution includes sulfurous or sulfuric acid. The phosphorus is provided by phosphoric acid, phosphorous acid or ammonium dihydrogen phosphate. The aluminum is provided by an aluminum source selected from the group consisting of the alumina trihydrates and aluminum oxide. Chloride contamination of the aluminum source should be minimal, preferably less than about 1000 ppm chloride, more preferably less than about 200 ppm chloride. The pH of the aqueous solution is adjusted to about 3-12 by the addition of a sufficient quantity of an aqueous ammonium solution. The FCC catalyst is added to this solution, preferably with stirring, in a weight ratio of about 1 part catalyst to about 1-10 parts water to prepare an aqueous slurry. Upon stabilization of the pH of the aqueous slurry, enhancement of the acid sites of the catalyst is achieved and the catalyst may be separated from the slurry and, if desired, washed. This simple, aqueous process reduces the level of many metal poisons, including nickel and vanadium, on the FCC catalyst and produces a catalyst having an enhanced number of acid reaction sites.
Abstract translation: 本发明公开了用于增强流化催化裂化（FCC）催化剂的酸性位点的水性方法。 所述方法包括使FCC催化剂（废弃或新鲜的）与包含水的水溶液以及磷和铝的来源接触的步骤。 任选地，溶液包括亚硫酸或硫酸。 磷由磷酸，亚磷酸或磷酸二氢铵提供。 铝由选自三水合氧化铝和氧化铝的铝源提供。 铝源的氯化物污染应该是最小的，优选小于约1000ppm氯化物，更优选小于约200ppm氯化物。 通过加入足够量的铵水溶液将水溶液的pH调节至约3-12。 将FCC催化剂优选在搅拌下加入到该溶液中，重量比为约1份催化剂至约1-10份水以制备含水浆料。 在稳定水性浆料的pH后，实现催化剂的酸性位置的增强，并且催化剂可以与浆料分离，并且如果需要，可以洗涤。 这种简单的含水方法在FCC催化剂上降低许多金属毒素（包括镍和钒）的水平，并产生具有增加数量的酸反应位点的催化剂。
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