公开(公告)号：DE19650107A1

公开(公告)日：1998-06-04

申请号：DE19650107

申请日：1996-12-03

Applicant: BASF AG

Inventor： OFTRING ALFRED DR ,  OETTER GUENTER DR ,  BAUR RICHARD DR ,  BORZYK OLIVER DR ,  BURKHART BERND DR ,  OTT CHRISTIAN DR ,  KAHMEN MARTIN AUS DEM DR

IPC: C07C231/02 ,  C07C231/24 ,  C07C233/05 ,  C07C233/09 ,  C07C233/18 ,  C07C233/20 ,  C11D19/00

Abstract: Separation of glycerol (I) from a reaction mixture containing (I) and fatty acid amides (II) comprises separation into an aqueous phase containing (I) and an organic phase containing (II) by adding aqueous acid solution to pH 1-7 and separating the aqueous phase. Also claimed is a method of preparing (II) by reacting fatty acid glycerides (III) with amines, in which the reaction mixture is treated in this way.

公开(公告)号：DE19751744A1

公开(公告)日：1999-05-27

申请号：DE19751744

申请日：1997-11-21

Applicant: BASF AG

Inventor： STOECKIGT DIETER ,  POTTHOFF-KARL BIRGIT DR ,  KAHMEN MARTIN AUS DEM DR ,  PERNER JOHANNES DR ,  BORZYK OLIVER DR ,  WOLFF ERWIN

IPC: C10M173/02 ,  C10M133/16 ,  B65G45/08 ,  C07C69/708 ,  C07C235/08 ,  C10M129/70 ,  C10M129/72 ,  C10M129/74 ,  C10M173/00

公开(公告)号：DE19650151A1

公开(公告)日：1998-06-04

申请号：DE19650151

申请日：1996-12-03

Applicant: BASF AG

Inventor： OFTRING ALFRED DR ,  OETTER GUENTER DR ,  BAUR RICHARD DR ,  BORZYK OLIVER DR ,  BURKHART BERND DR ,  OTT CHRISTIAN DR ,  KAHMEN MARTIN AUS DEM DR

IPC: C07C231/14 ,  C07C233/18 ,  C08G65/26 ,  C09K23/42 ,  C11D1/52 ,  C11D1/72 ,  A61K7/00 ,  A61K7/50 ,  A61K7/075 ,  B01F17/42

Abstract: Production of alkoxylated amides of formula R1CONR2CHR3CHR4O(CHR5CHR6O)nH (I) comprises: (a) reacting a glyceride of a fatty acid of formula R1COOH (II) with an amine of formula NHR2R7(III) to give an amide of formula R1CONR2R7 (IV) and glycerol; (b) adding aqueous acid solution to the reaction mixture to pH 1-7 and separating the aqueous glycerol-containing phase from the organic phase containing amide (IV); and (c) etherifying (IV) with ethylene oxide (EO), propylene oxide and/or butylene oxide to give (I). R1 = 5-25C aliphatic residue containing 0-5 double bonds; R2 = H or 1-20C alkyl optionally interrupted by 1-5 O; R3-R6 = H; or one of R3 and R4 and/or one of R5 and R6 = Me or Et; R7 = H or CHR3CHR4OH; n = 1-100; provided that R2 and R7 are not both H. (I) are new when R2 is Me or Et. Also claimed are (1) compounds (I) obtained as above; and (2) washing, cleaning and body care agents containing 0.1-50 wt.% (I).