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    METHOD FOR PRODUCING ALKYLARYL COMPOUNDS
    3.
    发明申请
    METHOD FOR PRODUCING ALKYLARYL COMPOUNDS 审中-公开
    用于生产烷CONNECTIONS

    公开(公告)号：WO2005061447A3

    公开(公告)日：2007-01-04

    申请号：PCT/EP2004014444

    申请日：2004-12-17

    Applicant: BASF AG ,  BOTTKE NILS ,  TROPSCH JUERGEN ,  NARBESHUBER THOMAS ,  STEPHAN JUERGEN ,  ROEPER MICHAEL ,  HEIDEMANN THOMAS ,  STEINBRENNER ULRICH ,  BENFER REGINA

    Inventor： BOTTKE NILS ,  TROPSCH JUERGEN ,  NARBESHUBER THOMAS ,  STEPHAN JUERGEN ,  ROEPER MICHAEL ,  HEIDEMANN THOMAS ,  STEINBRENNER ULRICH ,  BENFER REGINA

    IPC: C07C2/66 ,  C07C303/06 ,  C07C309/31 ,  C11D1/22 ,  C11D11/04

    CPC classification number: C07C6/04 ,  C07C2/08 ,  C07C2/66 ,  C07C5/2506 ,  C07C303/06 ,  C11D1/22 ,  C11D11/04 ,  C07C309/31 ,  C07C11/02 ,  C07C11/10 ,  C07C15/107

    Abstract: The production of alkylaryl compounds comprises the following stages: a) reaction of a C4/C5 olefin mixture on a metathesis catalyst to produce a C 4-8 olefin mixture containing 2-pentene and the optional isolation of the C 4-8 olefin mixture; b) isolation of between 5 and 100 % of the 2-pentene obtained in step a) and subsequent reaction on an isomerisation catalyst to form a mixture of 2-pentene and 1-pentene, which is returned to stage a); c) dimerisation of the C 4-8 olefin mixture obtained in stage b) after the isolation process, to form a mixture containing C 8-16 olefins, isolation of the C 8-16 olefins and optional isolation of a partial stream of the latter; d) reaction of the C 8-16 olefin mixtures obtained in stage c) or the partial stream with an aromatic hydrocarbon in the presence of an alkylation catalyst, to form alkyl aromatic compounds, whereby prior to the reaction an additional 0 to 60 wt. % linear olefins, in relation to the C 8-16 olefin mixtures obtained in stage c), can be added; e) optional sulphonation of the alkyl aromatic compounds obtained in stage d) and neutralisation to form alkylaryl sulphonates, whereby prior to the sulphonation an additional 0 to 60 wt. % linear alkyl benzols, in relation to the alkyl aromatic compounds obtained in stage d), can be added, provided that there were no admixtures in stage d); f) optional mixing of the alkylaryl sulphonates obtained in stage e) with between 0 and 60 wt. %, linear alkylaryl sulphonates, in relation to the alkylaryl sulphonates obtained in stage e), provided that there were no admixtures in stages d) and e).

    Abstract translation: 烷基芳基化合物通过C4 / C5烯烃混合物的超过一个C含有2-戊烯 4-8 烯烃混合物的制备复分解催化剂的C 的）反应，和可选地移除该制剂 4-8 烯烃混合物，b）中的5％至100％的分离在步骤a）所得2-戊烯和异构化催化剂的2-戊烯与1-戊烯的混合物随后的反应，在阶段a） 再循环，C）C的分离之后，在步骤b中得到的二聚） 4-8 在二聚催化剂存在下烯烃混合物，得到含烯烃-C 8-16 混合物， 的C 8-16 烯烃，和任选除去一个部分流体，D）在步骤C中获得的化合物反应）C 8-16 烯烃混合物或所述部分与芳族料流的分离 在烷基化催化剂的存在下烃以形成烷基芳香族Ve的 rbindungen，其中烯烃，e）可以反应，0〜60重量％之前添加到直链烯烃，基于在步骤c得到的）C在磺化 8-16，任选地 获得步骤d）的烷基芳族化合物中和以得到烷基芳基磺酸盐，其中之前的磺化，0至60重量％，基于在步骤d）中获得的烷基，可被加入到直链烷基苯的芳族化合物中，如果在步骤d没有掺合）下进行 中，f）如果到60重量％）的0）在步骤e中得到的烷基芳基磺酸盐的适当的混合，基于在步骤e烷芳基磺酸盐所获得的），线性烷基芳基磺酸盐，如果在步骤没有外加剂d）和e被执行。

    METHOD FOR PRODUCING PHTHALIC ACID ANHYDRIDE
    4.
    发明申请
    METHOD FOR PRODUCING PHTHALIC ACID ANHYDRIDE 审中-公开
    用于生产苯酐

    公开(公告)号：WO0155072A3

    公开(公告)日：2001-12-20

    申请号：PCT/EP0100303

    申请日：2001-01-11

    Applicant: BASF AG ,  WALCH ANDREAS ,  KAMMEL ULRICH ,  HEIDEMANN THOMAS

    Inventor： WALCH ANDREAS ,  KAMMEL ULRICH ,  HEIDEMANN THOMAS

    IPC: C07C51/265 ,  C07C51/46 ,  C07C63/16

    CPC classification number: C07C51/265 ,  B01D3/141 ,  C07C51/46 ,  C07C63/16

    Abstract: The invention relates to a method for producing phthalic acid anhydride. In a first step, o-xylol is partially oxidized with oxygen in a reactor in the liquid phase and in the presence of an added catalyst, said oxygen being optionally mixed with an inert gas. A fraction containing unreacted xylol is distilled off from the partially oxidized mixture and returned to the first step. In a second step, the partially oxidized mixture enriched with xylol is oxidized in the gas phase to produce phthalic acid anhydride. According to the invention, toluol is separated from the fraction containing the unreacted xylol that was distilled off, preferably in the form of an azeotrope with water. By separating off the toluol, it is possible to prevent the formation of hot spots in the second step of the reaction, which improves the selectivity of the reaction overall.

    Abstract translation: 本发明涉及一种用于在反应器中通过加入与氧的催化剂的液相中混合有惰性气体制备邻苯二甲酸酐，在第一步骤中邻二甲苯，可选地，被部分氧化，将含有未反应的二甲苯的级分 包含来自部分氧化的混合物中蒸出，并且所述第一阶段被反馈，且在二甲苯中的气相中邻苯二甲酸酐的第二步骤贫化部分氧化的混合物中被氧化。 根据本发明，从含有甲苯蒸馏，未反应的邻二甲苯级分，优选分离为与水的共沸物。 甲苯的除去，热点的形成防止了在反应，由此实现的总体反应的更好的选择性的第二阶段。

    7.
    发明专利
    未知

    公开(公告)号：AT382591T

    公开(公告)日：2008-01-15

    申请号：AT03762535

    申请日：2003-06-27

    Applicant: BASF AG

    Inventor： HEIDEMANN THOMAS ,  SIEBENHAAR URSULA

    IPC: C07C11/08 ,  C07C2/08 ,  C07C2/10

    Abstract: Process for oligomerizing an alkene stream over a solid catalyst comprising sulfur and nickel, in which the oligomerization is carried out in two or more successive catalyst zones and the molar ratio of sulfur to nickel in the first catalyst zone is less than 0.5 and that in the last catalyst zone is 0.5 or more and, in the case of further catalyst zones between the first and last catalyst zones, the molar ratio of sulfur to nickel in each catalyst zone is not less than that in the immediately preceding catalyst zone, based on the main flow direction of the feed stream.

    10.
    发明专利
    未知

    公开(公告)号：DE102005016152A1

    公开(公告)日：2006-10-12

    申请号：DE102005016152

    申请日：2005-04-07

    Applicant: BASF AG

    Inventor： STEPHAN JUERGEN ,  ROEPER MICHAEL ,  HEIDEMANN THOMAS ,  TRILLER MICHAEL ,  TROPSCH JUERGEN

    IPC: C08G65/34 ,  C11D1/72

    Abstract: The present invention relates to a process for preparing polyol alkyl ethers by reacting compounds comprising at least three hydroxyl functionalities with olefins in the presence of acidic catalysts at temperatures of from 20 to 250° C. and pressures of from 0.5 to 10 bar, wherein the olefins correspond to the general formula (I) in which R1 is hydrogen and R2 is a linear or branched carbon radical having from 7 to 28 carbon atoms, or R1 and R2 are each linear or branched carbon radicals having from 1 to 27 carbon atoms, the sum of the carbon number of R1 and R2 being at most 28, to polyol alkyl ethers derived from compounds having at least three hydroxyl functionalities, not more than all but one hydroxyl functionality being replaced by a moiety of the general formula (VIII) to the use of these polyol alkyl ethers as surfactants and to laundry detergents and cleaning compositions comprising these polyol alkyl ethers.

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