Method for the purification of a crude acrylic acid melt

    公开(公告)号:AU4652801A

    公开(公告)日:2001-10-23

    申请号:AU4652801

    申请日:2001-04-04

    Applicant: BASF AG

    Abstract: In a process for the purification of a crude acrylic acid melt, the crude acrylic acid melt is converted, under the action of low temperatures, into a crude acrylic acid suspension consisting of acrylic acid crystals and residual melt, and the acrylic acid crystals of the crude acrylic acid suspension are freed from remaining residual melt in a wash column, the production of the acrylic acid crystals of the crude acrylic acid suspension being carried out in the presence of water, the wash column being a wash column with forced transport of the acrylic acid crystals and the wash liquid used being the melt of acrylic acid crystals purified in the wash column.

    5.
    发明专利
    未知

    公开(公告)号:NO20075631L

    公开(公告)日:2008-02-01

    申请号:NO20075631

    申请日:2007-11-06

    Applicant: BASF AG

    Abstract: The calculation of the above balance shows that the division of stream (5) into the streams (5a) and (5b) used here leads to the fact that in the neutralization stage no excess sodium formate is produced, so that any ejection can be omitted. Furthermore, the water content of the stream (14) comprising sodium formate recirculated to the first crystallization stage in this case can be set to a very low value.

    تحضير حمض أكريليك ACRYLIC ACID

    公开(公告)号:SA1510B1

    公开(公告)日:2006-11-04

    申请号:SA03240323

    申请日:2003-10-08

    Applicant: BASF AG

    Abstract: الملخص: فىطريقةلتحضيرحمضاكريليك preparing acrylic acid،يتمتكثيفالخليطالغازىالمحتوىعلىحمضاكريليك acrylic acid الناتجمنالاكسدةالجزئيةذاتالطورالغازىالحفازةلمركب C3 اولىمنحمضالاكريليك acrylic acid،وبعدالتبريدالمباشربسائلإطفاء،تجزيئيافىعمودفصلمزودبمساحاتفاصلةداخلية،ويتصاعدداخلةبتيارجانبيمنحمضاكريليكخام crude acrylic acid،ويتمتفككاوليجوميرات oligomers حمضالاكريليك acrylic acid المتكونة،وتعريضغازالتفككالناتجالىتقويممتعاكسالاتجاهقبلاعادةتدويره.

    Purification process of raw acrylic acid melts

    公开(公告)号:CZ20023376A3

    公开(公告)日:2003-05-14

    申请号:CZ20023376

    申请日:2001-04-04

    Applicant: BASF AG

    Abstract: In a process for the purification of a crude acrylic acid melt, the crude acrylic acid melt is converted, under the action of low temperatures, into a crude acrylic acid suspension consisting of acrylic acid crystals and residual melt, and the acrylic acid crystals of the crude acrylic acid suspension are freed from remaining residual melt in a wash column, the production of the acrylic acid crystals of the crude acrylic acid suspension being carried out in the presence of water, the wash column being a wash column with forced transport of the acrylic acid crystals and the wash liquid used being the melt of acrylic acid crystals purified in the wash column.

    PRODUCTION OF SODIUM DIFORMATE
    10.
    发明专利

    公开(公告)号:CA2607099C

    公开(公告)日:2013-07-09

    申请号:CA2607099

    申请日:2006-05-02

    Applicant: BASF AG

    Abstract: The invention relates to a method for producing a solid sodium diformate preparation having a minimum formic acid concentration of 35 percent by weight relative to the total weight of the sodium diformate preparation. According to said method, an aqueous solution having a molar ratio HCOOH: HCOONa of more than 1.5:1 and a molar ratio HCOOH: H2O of at least 1.1:1 is produced from sodium formate and at least 74 percent by weight of formic acid at an elevated temperature, the aqueous solution is crystallized, and the solid phase is separated from the mother liquor. (i) A partial amount (A) of the mother liquor is used during the production of the aqueous solution while (ii) a partial amount (B) of the mother liquor is mixed with a sodium-containing base and the obtained sodium formate-containing mixture is also used during the production of the aqueous solution, optionally after separating a portion of the same and optionally after concentrating the same, the partial amounts (A) and (B) of the mother liquor amounting to 100 percent by weight.

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