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公开(公告)号：KR101886321B1
公开(公告)日：2018-08-09
申请号：KR1020160074404
申请日：2016-06-15
Applicant: 한국과학기술연구원
IPC: H01M8/1246 , H01M4/90 , H01M8/124
CPC classification number: H01M4/8867 , C04B35/453 , C04B35/50 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3279 , C04B2235/3298 , C04B2235/405 , C04B2235/407 , C04B2235/408 , H01M4/8885 , H01M4/9066 , H01M4/9075 , H01M2004/8684 , H01M2008/1293
Abstract: 본발명은금속-세라믹복합체에관한것으로, 보다상세하게는금속함량은현저히줄이면서도, 금속입자간의간격은일정하게유지하여, 활성및 전도성이향상된금속-세라믹복합체및 이를제조하는방법에관한것이다. 상기연료전지의연료극용금속-세라믹복합체는저함량의금속촉매원료물질과혼합전도성세라믹을포함함으로써, 상기금속-세라믹복합체내에존재하는금속촉매나노입자의함량을종래보다현저히낮추어금속촉매의부피변화로인해발생하던응력을최소화하고, 결함발생문제를해결하여, 수명특성을향상시킬수 있다.
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公开(公告)号：KR101788553B1
公开(公告)日：2017-10-23
申请号：KR1020100089687
申请日：2010-09-13
Applicant: 한국과학기술연구원
CPC classification number: Y02P70/56
Abstract: 본발명은소결첨가물및 동시소결기술을이용하여연료극지지형세라믹연료전지용음극지지체및 전해질을포함하는전극소자를제조하는방법에관한것으로서, 본발명의음극지지체및 전해질을포함하는연료전지음극소자의제조방법은, 음극지지체, 전해질또는이 둘모두에소결첨가물을첨가하고소결하는단계를포함하고, 하기화학식 1의 ABO계수소이온전도성세라믹을포함하는음극지지체및 전해질을포함하는연료전지음극소자의제조방법이다. 상기화학식은 Ba(ZrYM)O이고, 여기서, M은전이금속, Cu 및 Zn으로이루어진군 중에서선택되는적어도어느하나이고, x는 0
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公开(公告)号：KR1020160011472A
公开(公告)日：2016-02-01
申请号：KR1020140092601
申请日：2014-07-22
Applicant: 한국과학기술연구원
CPC classification number: Y02P70/56 , H01M8/1253 , H01M4/86 , H01M8/02 , H01M8/1226 , H01M2008/1095 , H01M2008/1293 , Y02E60/525
Abstract: 본발명은소결수축률이큰 연료극기판층과층간응력차이를완화시켜주는혼합층을포함하는적층체를동시소결하여전해질층의치밀도를향상시킨것을특징으로하는연료극지지형고체산화물셀 및그 제조방법에관한것으로서, 본발명에따르면, 저온에서동시에소결이이루어져단전지제조공정을단순화시킬수 있고, 연료극조성의유연성을확보하여수축률이높은연료극기판의사용이가능하도록함으로써, 전해질층의치밀도를향상시킬수 있으며, 혼합층의도입으로계면의열응력집중현상을완화시켜동시소결후 셀의휨현상, 균열및 셀의파괴를방지할수 있으므로, 전기화학적성능향상및 장기안정성이확보된연료극지지형고체산화물셀의제공및 상용화를가능하게한다.
Abstract translation: 本发明涉及通过共烧烧包括具有高烧结收缩率的阳极基底层的层叠体和减轻层之间的应力差的混合层来提高电解质层的密度的阳极支撑固体氧化物电池，以及 其制造方法。 根据本发明，由于在低温下进行共烧结，因此能够简化端电池制造工序，通过确保阳极组成的柔软性，可以使用具有高收缩率的阳极基板，从而增加 电解质层的密度。 通过引入混合层可以缓解界面的热应力集中现象。 因此，可以防止在共烧结之后电池弯曲，并且也避免了电池的破裂和断裂。 因此，可提供改善电化学性能并确保长期稳定性的负极固体氧化物电池的提供和商业化。
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公开(公告)号：KR1020150081928A
公开(公告)日：2015-07-15
申请号：KR1020140001931
申请日：2014-01-07
Applicant: 한국과학기술연구원
Abstract: 본발명은수소이온전도성고체산화물연료전지및 이의제조방법에관한것으로서, 본발명에따른수소이온전도성고체산화물연료전지의제조방법은연료극을준비하는단계, 상기연료극상에이트륨도프된바륨지르코네이트계(BZY) 고체산화물을포함하는제1 전해질층을형성하는단계, 상기제1 전해질층상에이트륨도프된바륨세레이트계(BCY) 고체산화물을포함하는제2 전해질층을형성하여반전지를제조하는단계, 상기연료극, 제1 전해질층및 제2 전해질층을동시에소결하는단계및 상기제2 전해질층상에공기극을형성하는단계를포함한다.
Abstract translation: 本发明涉及氢离子传导固体氧化物燃料电池及其制造方法。 根据本发明，氢离子导电固体氧化物燃料电池的制造方法包括以下步骤：制备燃料电极; 在所述燃料电极上形成包含掺钇锆酸钡（BZY）的固体氧化物的第一电解质层; 在所述第一电解质层上形成包含掺钇锆酸钡（BZY）的固体氧化物的第二电解质层的半电池; 同时烧结燃料电极，第一电解质层和第二电解质层; 以及在所述第二电解质层上形成阴极。
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Patent Agency Ranking
公开(公告)号：KR1020140107892A
公开(公告)日：2014-09-05
申请号：KR1020130022068
申请日：2013-02-28
Applicant: 한국과학기술연구원
CPC classification number: Y02P70/56 , C03C8/24 , C03C3/064 , C03C3/078 , C03C3/089 , C03C8/02 , C03C8/14 , H01M8/0282 , Y02E60/525
Abstract: The present invention relates to a sealant for a low temperature operation solid oxide fuel cell and a manufacturing method thereof and, more specifically, to a sealant for plate-shaped solid oxide fuel cell stack which is operated at low operation temperatures of 700°C or less. The composite sealant according to the present invention exhibits excellent compression resistance and long term endurance at 700 °C, prevents a softening point from being increased while maintaining low nucleation rate, maintains stable states and has excellent thermal cycle sealing stability since leakage and deterioration are not generated, thereby being able to be usefully used as a sealant for a low temperature plate-shaped solid oxide fuel cell stack and being able to usefully used in a plate-shaped solid oxide fuel cell stack module, a plate-shaped solid oxide fuel cell system, a plate-shaped solid oxide fuel cell single cell including the composite sealant of the present invention and the like.
Abstract translation: 本发明涉及用于低温操作的固体氧化物燃料电池的密封剂及其制造方法，更具体地说，涉及在700℃的低工作温度下操作的板状固体氧化物燃料电池堆的密封剂， 减。 根据本发明的复合密封剂在700℃下表现出优异的耐压缩性和长期耐久性，防止软化点增加，同时保持低成核速率，保持稳定状态并具有优异的热循环密封稳定性，因为渗漏和劣化不是 从而能够有效地用作低温板状固体氧化物燃料电池堆的密封剂，并且能够有效地用于板状固体氧化物燃料电池堆组件，板状固体氧化物燃料电池 系统，包括本发明的复合密封剂的板状固体氧化物型燃料电池单电池等。
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公开(公告)号：KR101307560B1
公开(公告)日：2013-09-12
申请号：KR1020110117652
申请日：2011-11-11
Applicant: 한국과학기술연구원
CPC classification number: Y02P70/56
Abstract: 본 발명은 용액공정에 기반한 스핀 코팅 공정에 의한 구성요소 형성과 이의 저온 소결을 이용한 중저온 온도영역에서 작동하는 고체 산화물 연료 전지(Solid Oxide Fuel Cell, SOFC)의 구조 및 제조 방법에 관한 것이다.본 발명에서는 저온 공정으로 고가의 장비나 출발 물질을 필요로 하지 않고, 기판 형태 및 크기에 따른 제약을 받지 않으며, 기판의 인장응력에 기인하는 결함 및 전극과 전해질 사이의 계면 반응을 억제할 수 있고 계면강도가 강화된 고체 산화물 연료 전지를 제조할 수 있으므로, SOFC의 수율 향상, 대면적화 및 실용화에 크게 이바지할 것으로 기대된다.
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98.发明公开소결 첨가물 및 동시소결을 이용하는 연료극 지지형 세라믹 연료전지용 음극 지지체 및 전해질을 포함하는 전극 소자의 제조방법 有权通过使用烧结添加剂和共烧技术，将包含阳极支持体和阳极支持的SOFC的电解质的ELETRODE装置的制造方法
公开(公告)号：KR1020120027875A
公开(公告)日：2012-03-22
申请号：KR1020100089687
申请日：2010-09-13
Applicant: 한국과학기술연구원
CPC classification number: Y02P70/56 , H01M8/1246 , H01B1/08 , H01M4/86 , H01M8/0206 , Y02E60/525
Abstract: PURPOSE: A manufacturing method of an electrode device is provided to restrain structural defect of each composing layer, the delamination between the composing layers or interface defect. CONSTITUTION: A manufacturing method of an electrode device comprises a step of adding sintering additive to an anode supporter and/or an electrolyte, and sintering the mixture. The electrode device comprises anode supporter including ABO_3 based proton conducting ceramic in chemical formula: Ba(Zr_(1-x-y)Y_xM_y)O_(3-δ), and electrolyte. In chemical formula, M is one selected from a group consisting of transition metals, Cu and Zn, 0
Abstract translation: 目的：提供电极装置的制造方法，以抑制每个构成层的结构缺陷，构成层之间的分层或界面缺陷。 构成：电极装置的制造方法包括将烧结添加剂添加到阳极支撑体和/或电解质中并烧结混合物的步骤。 电极装置包括具有化学式为Ba（Zr_（1-x-y）Y_xM_y）O_（3-＆amp;）和电解质的ABO_3基质子传导陶瓷的阳极支持体。 在化学式中，M是选自过渡金属Cu和Zn，0
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公开(公告)号：KR1020100104761A
公开(公告)日：2010-09-29
申请号：KR1020090023390
申请日：2009-03-19
Applicant: 한국과학기술연구원
Abstract: PURPOSE: A solid oxide fuel cell and a manufacturing method thereof are provided to prevent the defect occurrence by the sintering difference at a multi-layered structure by controlling the pore size distribution, and the surface roughness. CONSTITUTION: A solid oxide fuel cell comprises the following: a porous supporter; a dense electrolyte thin film; and a nanoporous layer smaller including a pore on the surface where contacting with the dense electrolyte thin film with the size smaller than the thickness of the dense electrolyte thin film and the pore size of the porous supporter. The nanoporous layer is formed in between the porous supporter and the dense electrolyte thin film. The nanoporous layer is a coating film of a metal oxide sol dispersed with nanopowder.
Abstract translation: 目的：提供固体氧化物燃料电池及其制造方法，以通过控制孔径分布和表面粗糙度来防止多层结构中的烧结差异的缺陷发生。 构成：固体氧化物燃料电池包括：多孔支持体; 致密电解质薄膜; 以及更小的纳米多孔层，其具有与致密电解质薄膜的密度接触的表面上的孔，其尺寸小于致密电解质薄膜的厚度和多孔载体的孔径。 纳米多孔层形成在多孔载体和致密电解质薄膜之间。 纳米多孔层是用纳米粉末分散的金属氧化物溶胶的涂膜。
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公开(公告)号：KR1020090078660A
公开(公告)日：2009-07-20
申请号：KR1020080004597
申请日：2008-01-15
Applicant: 한국과학기술연구원
CPC classification number: H01M8/1286 , C25D11/045 , C25D11/24 , C25D11/26 , C25D11/30 , C25D11/32 , C25D11/34 , H01M4/8878 , Y02P70/56
Abstract: A micro fuel cell, its manufacturing method, and a micro fuel cell stack using it are provided to inhibit the coherence of an electrode material due to the heat energy at a high temperature, thereby maintaining the structural stability even at a high temperature. A micro fuel cell comprises a solid electrolyte(50), and first and second electrodes(40,60) which are separately formed on the electrolyte, wherein at least one of the first and second electrodes is supported by a template(35) where a plurality of nanopores(47) are formed by anodizing and etching after the evaporation deposition of thin film, and is a porous electrode having the nanopore formed at the position corresponding to the entire or some part of the plurality of nanopores formed at the template.
Abstract translation: 提供一种微型燃料电池及其制造方法以及使用该微型燃料电池的微型燃料电池堆来抑制由于高温下的热能导致的电极材料的一致性，从而即使在高温下也能够保持结构稳定性。 微型燃料电池包括固体电解质（50）以及在电解质上分开形成的第一和第二电极（40,60），其中第一和第二电极中的至少一个由模板（35）支撑，其中 在薄膜的蒸发沉积之后通过阳极氧化和蚀刻形成多个纳米孔（47），并且是在对应于在模板形成的多个纳米孔的全部或部分的位置处形成的纳米孔的多孔电极。
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