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    91.
    发明专利
    未知

    公开(公告)号：BRPI0506587A

    公开(公告)日：2007-05-02

    申请号：BRPI0506587

    申请日：2005-01-27

    Applicant: BASF AG

    Inventor： SCHEIDEL JENS ,  JUNGKAMP TIM ,  BARTSCH MICHAEL ,  HADERLEIN GERD ,  BAUMANN ROBERT ,  LUYKEN HERMANN

    IPC: C07C253/10 ,  C07C253/34 ,  C07C255/07

    Abstract: A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) reacting 1,3-butadiene with hydrogen cyanide over at least one catalyst to obtain a stream 1 which comprises 3-pentenenitrile, 2-methyl-3-butenenitrile, the at least one catalyst and 1,3-butadiene, (b) distilling stream 1 in a column to obtain a high-1,3-butadiene stream 2 as the top product and a low-1,3-butadiene stream 3 as the bottom product which comprises 3-pentenenitrile, the at least one catalyst and 2-methyl-3-butenenitrile, (c) distilling stream 3 in a column to obtain a stream 4 as the top product which comprises 1,3-butadiene, a stream 5 which comprises 3-pentenenitrile and 2-methyl-3-butenenitrile at a side draw of the column, and a stream 6 as the bottom product which comprises the at least one catalyst, (d) distilling stream 5 to obtain a stream 7 as the top product which comprises 2-methyl-3-butenenitrile, and a stream 8 as the bottom product which comprises 3-pentenenitrile.

    92.
    发明专利
    未知

    公开(公告)号：DE502004003136D1

    公开(公告)日：2007-04-19

    申请号：DE502004003136

    申请日：2004-03-24

    Applicant: BASF AG

    Inventor： BARTSCH MICHAEL ,  BAUMANN ROBERT ,  HADERLEIN GERD ,  FLORES MIGUEL ANGEL ,  JUNGKAMP TIM ,  LUYKEN HERMANN ,  SCHEIDEL JENS ,  SIEGEL WOLFGANG ,  MOLNAR FERENC

    IPC: B01J27/14 ,  B01J23/755 ,  B01J31/02 ,  B01J31/14 ,  B01J31/18 ,  C07C253/10 ,  C07C255/04

    Abstract: A system which is suitable as a catalyst for the hydrocyanation of olefinically unsaturated compounds and comprises a) Ni(0) b) a compound which complexes Ni(0) as a ligand and contains trivalent phosphorus, c) a Lewis acid and d) a compound of the formula M Rn where M: Al or Ti R: identical or different monovalent alkoxy radicals, in which case a plurality of alkoxy radicals may be bonded together, and additionally, in the case that M=Al, R may be identical or different monovalent alkyl radicals, in which case a plurality of alkyl radicals may be bonded together or one or more alkyl radicals may be bonded to one or more of the abovementioned alkoxy radicals, n: valency of M, and processes for hydrocyanating an olefinically unsaturated compound in the presence of such a system.

    93.
    发明专利
    未知

    公开(公告)号：BRPI0506581A

    公开(公告)日：2007-04-10

    申请号：BRPI0506581

    申请日：2005-01-27

    Applicant: BASF AG

    Inventor： JUNGKAMP TIM ,  BAUMANN ROBERT ,  BARTSCH MICHAEL ,  HADERLEIN GERD ,  LUYKEN HERMANN ,  SCHEIDEL JENS

    IPC: C07C253/10 ,  C07C255/04

    Abstract: An adiponitrile/methylglutaronitrile preparation process includes distilling a reaction stream to obtain stream 3 depleted in pentenenitriles (bottom product) and stream 4 enriched in pentenenitriles (top product); extracting stream 3 obtaining stream 6 enriched with extractant (top product) and stream 7 depleted in extractant (bottom product); distilling stream 6 obtaining stream 8 comprising the catalyst (bottom product) and stream 9 comprising the extractant (top product); distilling stream 7 obtaining stream 10 (bottom product) and stream 11 comprising the extractant (top product); distilling stream 10 obtaining stream 12 comprising catalyst degradation products, at least one promotor, adiponitrile and methylglutaronitrile (bottom product) and stream 13 comprising pentenenitriles (top product); distilling stream 12 obtaining stream 14 comprising catalyst degradation products and the promotor(s) (bottom product) and stream 15 comprising adiponitrile and methylglutaronitrile (top product); distilling stream 15 obtaining stream 16 comprising adiponitrile (bottom product) and stream 17 comprising methylglutaronitrile (top product).

    PHOSPHITE
    96.
    发明专利
    PHOSPHITE 未知

    公开(公告)号：DE50012997D1

    公开(公告)日：2006-07-27

    申请号：DE50012997

    申请日：2000-10-25

    Applicant: BASF AG

    Inventor： BAUMANN ROBERT ,  FISCHER JAKOB ,  JUNGKAMP TIM ,  KUNSMANN-KEITEL PASCALE ,  SIEGEL WOLFGANG

    IPC: B01J31/22 ,  C07F9/145 ,  B01J31/02 ,  B01J31/18 ,  C07B61/00 ,  C07C253/10 ,  C07C253/30 ,  C07C255/03 ,  C07C255/07 ,  C07C255/19 ,  C07F15/04

    Abstract: New phosphites (I), with alkylaryl, arylaryl and/or condensed aryl groups, have 1, 2 or 3 o-substituted and optionally 1 or 2 m- and/or p-substituted aryl groups. New phosphites of formula (I), with alkylaryl, arylaryl and/or condensed aryl groups, have 1, 2 or 3 o-substituted and optionally 1 or 2 m- and/or p-substituted aryl groups; P(O-R 1>)(O-R 2>) y(O-R 3>) z(O-R 4>) p (I) R 1>an aromatic group with a 1-18 carbon (C) alkyl, an aromatic substituent or a condensed aromatic system in the o-position to the oxygen (O) atom linking the phosphorus (P) atoms to the aromatic system; R 2>a similar aromatic group substituted in the m-position; R 3>a similar aromatic group substituted in the p-position; R 4>an aromatic group with a different substituent in the o-, m- or p-position and a hydrogen (H) atom in the o-position; x : 1 or 2; y, z, p : 0, 1 or 2; (x+y+z+p) : 3 Independent claims are also included for: (a) new transition metal complexes (II) with (I) as ligand; (b) the preparation of (I); (c) the preparation of (II); (d) the addition of hydrogen cyanide to an olefinic double bond in the presence of (II) as catalyst; and (e) the isomerization of organic nitriles in the presence of (II) as catalyst.

    PROCEDIMIENTO PARA LA PREPARACION DE PENTENONITRILO LINEAL
    98.
    发明专利
    PROCEDIMIENTO PARA LA PREPARACION DE PENTENONITRILO LINEAL 未知

    公开(公告)号：AR048221A1

    公开(公告)日：2006-04-12

    申请号：ARP050100304

    申请日：2005-01-28

    Applicant: BASF AG

    Inventor： JUNGKAMP TIM ,  BAUMANN ROBERT ,  BARTSCH MICHAEL ,  HADERLEIN GERD ,  LUYKEN HERMANN ,  SCHEIDEL JENS

    IPC: C07C255/07 ,  C07B35/08 ,  C07C253/10 ,  C07C255/03

    Abstract: Se describe un procedimiento para la produccion de 3-pentenonitrilo, caracteriado porque los siguientes pasos del, procedimiento: (a) isomerizacion de una corriente de eductos que contiene 2-metil-3-butenonitrilo, por lo menos un catalizador de isomerizacion, disuelto o disperso, de manera de obtener una corriente 1, que contiene por lo menos un catalizador de isomerizacion, 2-metil-3-butenonitrilo, 3-pentenonitrilo y (Z)-2-metil-2-butenonitrilo; (b) destilacion de la corriente 1 con lo cual se obtiene una corriente 2 como producto de cabeza, que contiene 2-metil-3-butenonitrilo, 3-pentenonitrilo y (Z)-2-metil-2-butenonitrilo, y una corriente 3 como producto de descarga, que contiene por lo menos un catalizador de isomerizacion; (c) destilacion de la corriente 2, con lo cual se obtiene una corriente 4 como producto de cabeza que con respecto a la corriente 2 se ha enriquecido en (Z)-2-metil-2-butenonitrilo, referido a la suma de todos los pentenonitrilos en la corriente 2, y una corriente 5 como producto de descarga que con respecto a la corriente 2 se ha enriquecido en 3-pentenonitrilo y 2-metil-3-butenonitrilo, referido a la suma de todos los pentenonitrilos en la corriente 2; (d) destilacion de la corriente 5, con lo cual se obtiene una corriente 6 como producto de descarga que contiene 3-pentenonitrilo, y una corriente 7 como producto de cabeza que contiene 2-metil-3-butenonitrilo.

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