Kontinuální zpusob sušení a následné kondenzace polykondenzovaného granulátu, systém k provádení zpusobu a použití systému

    公开(公告)号:CZ301886B6

    公开(公告)日:2010-07-21

    申请号:CZ20021885

    申请日:2000-11-29

    Applicant: BASF AG

    Abstract: Zarízení (1) pro sušení a tepelné zpracování granulátu proudem netecného plynu obsahuje hranolovitou základní jednotku (2) se vstupem (3) pro privádení granulátu v její horní cásti a výstupem (4) granulátu v její spodní cásti, s prívodem (5) proudu netecného plynu na jedné bocní ploše a s odtahem (6) proudu netecného plynu na protilehlé bocní ploše hranolovité základní jednotky (2). Zarízení (1) dále obsahuje distribucní a zadržovací príslušenství (7, 8), usporádané v uvedeném poradí, v oblasti prívodu (5) proudu netecného plynu a v oblasti odtahu (6) proudu netecného plynu, pricemž se každé z uvedených príslušenství rozkládá pres v podstate celý úcinný prurez hranolovité základní jednotky (2) ve vertikálním smeru. Sušení probíhá pri teplote 105 až 120 .degree.C s následným ochlazováním a je vhodné zejména pro granuláty polyesteru nebo polyamidu.

    METHOD FOR THE CONTINUOUS PRODUCTION OF COPOLYAMIDES BASED ON A LACTAME (I), A DIAMINE (II) AND A DICARBOXYLIC ACID (III)

    公开(公告)号:CA2392736C

    公开(公告)日:2007-10-09

    申请号:CA2392736

    申请日:2000-11-15

    Applicant: BASF AG

    Abstract: The invention relates to a method for the continuous production of copolyamides which are based on a lactame (I), a diamine (II) and a dicarboxylic acid (III). The inventive method is characterised in that a mixture (IV) containing a diamine (II), a dicarboxylic acid (III) and water is converted to a polymer in a first reaction area at a pressure of 1,3*10 5 to 2,5*10 5 Pa in the entry part of the reaction area, at a temperature above the melting point of the polymer (V) and with a degree of conversion of at least 80 % in relation to the molar quantities of diamine (II) and dicarboxylic acid (III), in that a mixture (VI) containing lactame (I) and water is converted to a polymer (VII) in a second reaction area at a pressure of 5*10 5 to 40*10 5 Pa, at a temperature above the melting point of the polymer (VII) and with a degree of conversion of at least 80 % in relation to the molar quantity of lactame (I), in that polymer (V) and polymer (VII) are then reacted with each other in a third reaction area at a pressure of 1*10 5 to 1,5*10 5 Pa in the entry part of the reaction area, at temperatures above the melting temperature of the polymer (VIII), to produce the polymer (VIII). Polymer (VIII) contains a maximum of 10 wt. % constituents that are extractable with water at a temperature of 95.degree.C, in relation to lactame (I), diamine (II) and dicarboxylic acid (III). The polymer (VIII) is then extracted with water so as to obtain the copolyamide. The invention also relates to copolyamides obtained using this method and to the ir use in the production of fibres, sheet structures and moulded bodies which are based on these copolyamides.

    PROCESS FOR PRODUCING POLYAMIDES FROM AMINONITRILES

    公开(公告)号:CA2264023C

    公开(公告)日:2007-03-27

    申请号:CA2264023

    申请日:1997-08-26

    Applicant: BASF AG

    Abstract: A process for producing a polyamide by reacting at least one aminonitrile wi th water has the following steps: (1) at least one aminonitrile is reacted with water at a temperature from 100 to 360 .degree. C and pressure from 0.1 to 35..times. 10 6 Pa, yielding a reaction mixture; (2) the reaction mixture is further reacted at a temperature from 150 to 400 .degree.C and pressure lower than the pressure in step 1. The temperature and pressure are selected to yield a first gaseous phase and a first liquid or solid phase or a mixture of a first solid and a first liquid phase. The first gaseous phase is separated from the first liquid or solid phase or the mixture of a first liquid and a first solid phase is separated; and (3) the first liquid or solid phase or the mixture of a first liquid and first solid phase is mixed with a water-containing gaseous or liquid phase at a temperature from 150 to 360 .degree.C and pressure from 0.1 to 30 .times. 10 6 Pa, yielding a product mixture. Also disclosed are other embodiments of this process and the thus produced polyamides.

    DISPOSITIVO PARA SECAR Y TRATAR TERMICAMENTE UN GRANULADO CON UNA CORRIENTE DE GAS INERTE

    公开(公告)号:CO5290281A1

    公开(公告)日:2003-06-27

    申请号:CO00091437

    申请日:2000-11-29

    Applicant: BASF AG

    Abstract: Un aparato (1) para secar y tratar térmicamente pellets con una corriente de gas inerte, caracterizado porque el aparato tiene una unidad de base cuboide (2) con una alimentación (3) para los pellets en su parte superior y una salida (4) en su parte inferior, con una alimentación (5) en una superficie lateral y con una descarga (6) en la superficie lateral opuesta de la unidad de base cuboide (2) para la corriente de gas inerte, y también con un equipo de distribución y retención (7,8) en al región de la alimentación (5) y respectivamente, de la descarga (6) para la corriente de gas inerte, en donde cada una de estas piezas del equipo se extiende esencialmente sobre toda la sección transversal vertical de la unidad de base cuboide (2).

    100.
    发明专利
    未知

    公开(公告)号:DE59708777D1

    公开(公告)日:2003-01-02

    申请号:DE59708777

    申请日:1997-08-26

    Applicant: BASF AG

    Abstract: A process for preparing a polyamide by reacting at least one aminonitrile with water comprises:(1) reacting at least one aminonitrile with water at a temperature from 100 to 360° C. and a pressure from 0.1 to 35x106 Pa to obtain a reaction mixture,(2) further reacting the reaction mixture at a temperature from 150 to 400° C. and a pressure which is lower than the pressure in step 1, the temperature and the pressure being selected so as to obtain a first gas phase and a first liquid or a first solid phase or a mixture of first solid and first liquid phase, and the first gas phase is separated from the first liquid or the first solid phase or from the mixture of first liquid and first solid phase, and(3) admixing the first liquid or the first solid phase or the mixture of first liquid and first solid phase with a gaseous or liquid phase comprising water at a temperature from 150 to 360° C. and a pressure from 0.1 to 30x106 Pa to obtain a product mixture.

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