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    METHOD FOR PRODUCTION OF ALKALI METAL DIALKYLAMIDES
    4.
    发明申请
    METHOD FOR PRODUCTION OF ALKALI METAL DIALKYLAMIDES 审中-公开
    用于生产碱金属 - 烷基酰胺

    公开(公告)号：WO03042154A3

    公开(公告)日：2003-09-25

    申请号：PCT/EP0212528

    申请日：2002-11-08

    Applicant: BASF AG ,  STEINBRENNER ULRICH ,  BOEHLING RALF ,  FUNKE FRANK ,  HARDER WOLFGANG

    Inventor： STEINBRENNER ULRICH ,  BOEHLING RALF ,  FUNKE FRANK ,  HARDER WOLFGANG

    IPC: B01J31/26 ,  B01J31/02 ,  C07B61/00 ,  C07C209/00 ,  C07C209/60 ,  C07C211/03 ,  C07C211/35 ,  C07C211/65 ,  C07F1/00 ,  C07F1/02 ,  C07F1/04 ,  C07F1/06

    CPC classification number: C07C209/00 ,  C07C211/65

    Abstract: The present invention relates to a method for producing dialkylamides of the alkali metals by reacting the corresponding dialkylamine with the corresponding alkali metal in the presence of an electron donor substance of the group 1,3-butadiene, isoprene, naphthalene and/or styrene with the formation of low quantities of butenyl dialkylamine. According to said method, the corresponding alkali metal is introduced and suspended in a solvent and the dialkylamine and the electron donor substance are added, such that the dialkylamine is present in an amount up to 45 wt. %, preferably up to 25 wt. %, in particular up to 15 wt. % and the butadiene is present in an amount up to 5 wt. %, preferably up to 3 wt. %, in particular up to 1.5 wt. %.

    Abstract translation: 本发明涉及一种方法，用于通过与相应的碱金属的相应的二烷基胺在一种供电子物质的选自1,3-丁二烯，异戊二烯，萘和/或苯乙烯低的存在下反应形成butenyldialkylamine的量，其中，制备所述碱金属的二烷基酰胺 相应的碱金属悬浮在溶剂中并提交并随后加入二烷基胺和供电子物质以这样的方式，所述二烷基胺的存在量至45重量％，优选至25重量％，特别是15重量％到，并 的量存在于丁二烯至5重量％，优选为重量％至3，特别是至多1.5重量％，是存在的。

    PROCESS FOR PRODUCING POLYAMIDES FROM AMINONITRILES
    7.
    发明申请
    PROCESS FOR PRODUCING POLYAMIDES FROM AMINONITRILES 审中-公开
    一种从氨基腈PRODUCING聚酰胺

    公开(公告)号：WO9808889A2

    公开(公告)日：1998-03-05

    申请号：PCT/EP9704640

    申请日：1997-08-26

    Applicant: BASF AG ,  WEISS ROBERT ,  KRAUSS DIETER ,  KELLER DIETER ,  PIPPER GUNTER ,  HARDER WOLFGANG ,  LUDWIG ALFONS ,  MOHRSCHLADT RALF

    Inventor： WEISS ROBERT ,  KRAUSS DIETER ,  KELLER DIETER ,  PIPPER GUNTER ,  HARDER WOLFGANG ,  LUDWIG ALFONS ,  MOHRSCHLADT RALF

    IPC: C08G69/00 ,  C08G69/04 ,  C08G69/08 ,  C08G69/28 ,  C08G69/36

    CPC classification number: C08G69/04 ,  C08G69/08 ,  C08G69/28 ,  C08G69/36

    Abstract: A process for producing a polyamide by reacting at least one aminonitrile with water has the following steps: (1) at least one aminonitrile is reacted with water at a temperature from 100 to 360 DEG C and pressure from 0.1 to 35.x 10 Pa, yielding a reaction mixture; (2) the reaction mixture is further reacted at a temperature from 150 to 400 DEG C and pressure lower than the pressure in step 1. The temperature and pressure are selected to yield a first gaseous phase and a first liquid or solid phase or a mixture of a first solid and a first liquid phase. The first gaseous phase is separated from the first liquid or solid phase or the mixture of a first liquid and a first solid phase is separated; and (3) the first liquid or solid phase or the mixture of a first liquid and first solid phase is mixed with a water-containing gaseous or liquid phase at a temperature from 150 to 360 DEG C and pressure from 0.1 to 30 x 10 Pa, yielding a product mixture. Also disclosed are other embodiments of this process and the thus produced polyamides.

    Abstract translation: 一种用于通过至少一个氨基腈与水反应，包括下列步骤制备聚酰胺过程：（1）在100至360摄氏度的温度和0.1〜35×10的压力<至少一个氨基腈与水反应 6> Pa至获得得到的反应混合物，（2）进一步在150〜400℃和压力是比在步骤1中的压力更低的温度下的反应混合物反应，所述温度和压力被选择为使得 该第一气相和第一液体或第一固相或第一固体和第一液相的混合物获得，并从所述第一液体或第一固相或第一液体和第1固相的混合物中的第一气体相分离出 是，（3）将第一液体或第一固相或第一液体和第1固相的与气态或混合物 含有液体相包含水，在150〜360℃的温度和0.1〜30×10 <6> Pa的压力以获得产物混合物中获得，以及这样的方法的其它实施例中，将如此制备的 聚酰胺本身。

    PROCESS FOR PREPARING ALIPHATIC ALPHA, OMEGA-AMINONITRILES
    9.
    发明专利
    PROCESS FOR PREPARING ALIPHATIC ALPHA, OMEGA-AMINONITRILES 未知

    公开(公告)号：CA2208775C

    公开(公告)日：2005-07-05

    申请号：CA2208775

    申请日：1995-12-16

    Applicant: BASF AG

    Inventor： MELDER JOHANN-PETER ,  SCHNURR WERNER ,  FLICK KLEMENS ,  EBEL KLAUS ,  REHFINGER ALWIN ,  HARDER WOLFGANG ,  FISCHER ROLF ,  WITZEL TOM

    IPC: B01J23/89 ,  B01J23/76 ,  B01J23/889 ,  B01J27/18 ,  B01J37/02 ,  C07B61/00 ,  C07C253/30 ,  C07C255/24

    Abstract: Aliphatic alpha,omega-aminonitriles are prepared by partially hydrogenating aliphatic alpha,omega-dinitriles at an increased temperature and pressure in the presence of a solvent and a catalyst. The catalyst contains (a) a compound based on a metal selected from the group made up of nickel, cobalt, iron, ruthenium and rhodium; (b) 0.01 to 25 % by weight in relation to (a) of a promoter based on a metal selected from the group comprising of palladium, platinum, iridiu m, osmium, copper, silver, gold, chromium, molybdenum. tungsten, manganese, rhenium, zinc, cadmium, lead, aluminium, tin, phosphoru s, arsenic, antimony, bismuth, silicium, titanium, zirconium and rare earth metals; and (c) 0 to 5 % by weight in relation to (a) of a compound based on an alkaline or alkaline-earth metal, provided that component (a) not be based on iron or iron and a metal selected from th e group comprising cobalt, ruthenium and rhodium when (b) is a promoter based on a metal selected from the group comprising titanium, manganese, chromium and molybdenum. Moreover, when component (a) is a compound based only on ruthenium or on rhodium, ruthenium and rhodium, or nickel and rhodium, promoter (b) may be dispensed with.

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