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    111.
    发明专利
    未知

    公开(公告)号：DE4425794A1

    公开(公告)日：1996-01-25

    申请号：DE4425794

    申请日：1994-07-21

    Applicant: BASF AG

    Inventor： LAMM GUNTHER DR ,  REICHELT HELMUT DR ,  GRUND CLEMENS DR

    IPC: C07D271/06 ,  C09B51/00 ,  D06P1/19 ,  C07C205/45

    Abstract: Nitro dyes of formula (I), in which X and X are hydrogen, C1-C6 alkyl, C1-C6 alkoxy or pyrrolidine-2-one-1-yl, X is hydrogen or C1-C6 alkyl and X is a radical of formula (a), (b) or (c), in which R is hydrogen, possibly substituted C1-C12 alkyl, possibly substituted C3-C7 cycloalkyl or possibly substituted phenyl, R and R are hydrogen, C1-C6 alkyl or C1-C6 alkoxy, R is hydrogen, methyl, ethyl, methoxy or ethoxy and R is hydrogen or C1-C6 alkyl and process for their production and their use in dyeing or printing textiles.

    Multicomponent dye mixt for textiles e.g. polyester dyeing - contg six or more di:amino-pyridine deriv mono:azo dyes, giving temp-independent exhaustion properties for fabrics of cellulose ester] or polyamide
    115.
    发明专利
    Multicomponent dye mixt for textiles e.g. polyester dyeing - contg six or more di:amino-pyridine deriv mono:azo dyes, giving temp-independent exhaustion properties for fabrics of cellulose ester] or polyamide 未知

    公开(公告)号：DE4241116A1

    公开(公告)日：1994-06-09

    申请号：DE4241116

    申请日：1992-12-07

    Applicant: BASF AG

    Inventor： LOEFFLER HERMANN ,  LAMM GUNTHER DR

    IPC: C09B67/22 ,  D06P1/18

    Abstract: The mixts. contain at least six (6-12) similarly coloured 2,6-diamino-3-azo-5-cyano-6-methylpyridine deriv. dyes of formula (I), D = residue of a diazo component of the aniline, aminothiophene, amino(iso)thiazole or aminobenzisothiazole series; one of X1, X2 = NH2, and the other = -NR1-L-O-R2; L = 2-8C alkylene (opt. interrupted by 1 or 2 ether O functions); R1 = H or 1-4C alkyl (opt. substd. by OH, 1-4C alkoxy or 1-8C alkanoyloxy); R2 = H, 1-4C alkyl, benzyl, phenyl or 1-8C alkanoyl. More specifically, D = gp. of formula (IIa)-(IIe), esp. (IIb)-(IId), where Z1 = H, NO2, CN, 1-9C alkoxycarbonyl or 1-9C alkylamino carbonyl (both opt. interrupted by 1 or 2 ether O functions), CF3, 1-4C alkylsulphonyl, 3-(1-4C alkyl)-1,2,4-oxadiazol-5-yl or 3-phenyl-1,2,4-oxadiazol-5-yl; Z2 = H, Cl, Br, CN, Me, OMe, OEt, phenylazo or benzoyl (opt. substd. by Me, OMe or Cl); Z3 = H, CN, Cl, Br or 1-9C alkoxycarbonyl (opt. interrupted by 1 or 2 ether O); or Z2+Z3 = -CO-NA'-CO-; A' = H or 1-4C alkyl; Z4 = CN, CHO, NO2, 1-9C alkoxycarbonyl (opt. interrupted by 1 or 2 ether O), phenylazo (opt. substd. by CN) or A2-C(CN)=CH-; A2 = CN, CHO, 1-9C alkoxycarbonyl (opt. interrupted by 1 or 2 ether O); Z5 = H, 1-4C alkyl, 1-4C alkoxy, phenyl or benzyl (both opt. substd. by Me, OMe or Cl), 1-4C alkylsulphonyl, Cl, Br or 1-9C alkoxycarbonyl (opt. interrupted by 1 or 2 ether O; Z6 = 1-4C alkyl, phenyl or benzyl (both opt. substd. by Me, OMe or Cl), CN, NO2, 1-9C alkoxycarbonyl (opt. interrupted by 1 or 2 ether O) or 1-4C alkylsulphonyl; Z7 = 1-4C alkyl, phenyl or benzyl (both opt. substd. by Me, OMe or Cl) or 1-4C alkylsulphonyl; Z8 = NO2, CN or 1-4C alkylsulphonyl; R2 = 1-5C alkanoyl (esp. acetyl); L = 4-8C alkylene interrupted by 1 or 2 ether O. The mixts. are prepd. e.g. by: (1) reacting 2,6-dichloro-3-cyano-4-methyl pyridine with NH3 to give a mixt. of 2-chloro-3-cyano-4-methyl-6-aminopyridine and the corresp. 2-amino-6-chloro cpd. in molar ratio 3:17 to 2:3; (2) reacting the mixt. with amines of formula R1-NH-L-OR3 (R3 = H, 1-4C alkyl, benzyl or phenyl, R3 is H in the amine(s) to give a mixt. of 2-(NR-L-OH)-3-cyano-4-methyl-6-aminopyridines and the corresp. 2-amino-6-(NR'-L-OH) cpds.; (3) O-acylating with a 1-8C alkanoic acid (opt. in presence of mineral acid); and (4) coupling with a diazonium salt derived from DNH2. USE/ADVANTAGE - Use of the mixt. for dyeing or printing textiles is claimed. Typically they are used with fibres or fabrics of cellulose ester, polyamide, polyester-cellulose or -wool blends or esp. polyester, e.g. giving blue, violet, red, orange, brown or yellow shades. Unlike the individual dyes (I) or known mixts. of up to 4 cpds. (I) (see US4855412/3, EP-201896), the exhaustion behaviour of the present mixts. is virtually independent of temp. the mixts. also have high exhaustion and very low tendency to recrystallise in dispersed form.

    116.
    发明专利
    未知

    公开(公告)号：DE59005501D1

    公开(公告)日：1994-06-01

    申请号：DE59005501

    申请日：1990-03-26

    Applicant: BASF AG

    Inventor： LAMM GUNTHER DR ,  ETZBACH KARL HEINZ DR ,  WIESENFELDT MATTHIAS DR ,  HANSEN GUENTER DR ,  REICHELT HELMUT DR

    IPC: C09B29/00 ,  C09B29/042 ,  C09B29/36 ,  D06P1/18

    Abstract: Thiazole azo-dyes of the formula … … in which… R denotes C1-C12-alkyl which is optionally interrupted by oxygen atoms, or phenyl, halogen, cyano or C1-C4-alkoxycarbonyl,… R denotes formyl, cyano, C1-C4-alkoxycarbonyl or a radical of the formula -CH=CH X , in which X and X independently of one another stand for cyano or C1-C4-alkoxycarbonyl,… R denotes C1-C12-alkyl which is optionally interrupted or substituted by oxygen atoms, C5-C7-cycloalkyl, optionally substituted phenyl, furyl, thienyl, C1-C4-alkylthienyl or pyridyl and… R and R independently of one another denote C1-C12-alkyl which is optionally interrupted and/or substituted by oxygen atoms,… with the proviso that the alkyl chain is interrupted by oxygen atoms in at least one of the radicals R , R and R , and their use for dyeing textile fibres.

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