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公开(公告)号：KR100158759B1
公开(公告)日：1998-11-16
申请号：KR1019950038384
申请日：1995-10-31
Applicant: 한국화학연구원
Abstract: 본 발명은 중기공성(Mesoporous) 구조를 갖는 결정화합물의 제조방법에 관한 것으로서, 더욱 성세하게는 불화수소용액에 실리카 등을 녹여 상온, 상압조건에서 반응시킴으로써 모든 종류의 실리카를 이용할 수 있으며 단시간내에 반응을 진행시킬 수 있는 중기공성 구조를 갖는 결정화합물의 새로운 제조방법에 관한 것이다.
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Patent Agency Ranking
公开(公告)号：KR1019970058773A
公开(公告)日：1997-08-12
申请号：KR1019960001085
申请日：1996-01-19
Applicant: 한국화학연구원
IPC: B01J29/06
Abstract: 본 발명은 친수 및 친유성 흡착특성을 지닌 복합분자체 제조방법에 관한 것으로서, 더욱 상세하게는 친수성 제올라이트를 제조하는 과정 초기에 친유성이고 산과 알칼리에 높은 안정성을 갖는 활성탄을 첨가하여 활성탕의 기공내에서 3차원적인 다공성 제올라이트를 결정화시켜 친수성 특성과 친유성 특성을 함께 갖고 있어 폭넓은 흡착특성을 갖는 복합분자체의 제조방법에 관한 것이다.
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公开(公告)号：KR1019970007021B1
公开(公告)日：1997-05-02
申请号：KR1019930014239
申请日：1993-07-26
Applicant: 한국화학연구원
IPC: C07C309/28 , C07C309/29 , C07C309/30
Abstract: The preparation relates to a chemical reaction (I), R+H2SO4 RSO3H+H2O (wherein R is benzene, toluene, ethylbenzene, xylene, crezole, xylenol, chlorophenol, methoxybenzene, dihydroxy benzene, naphthalene, methyl naphthalene, chloronaphthol, naphthol, anthracene, aniline, naphthylamine, aminophenol, toluidine, nitrobenzene, diethylbenzene, dibuthylamine, quinoline, triarylamine, methylnathphalene, docecane and dihexylamine. The preparing method includes reacting an aromatic carbohydrate compound with sulfuric acid to sulfonylate the aromatic carbohydrate compound and produce aromatic sulfonic acid. Specifically, the method includes continuously supplying sulfuric acid through a plurality of feeding inlets, sulfonylating the excessive aromatic carbohydrate compound with insufficient sulforic acid to lower the concentration of the product, aromatic sulfonic acid, condensing the gas emitted from a tower of the reactor to remove water from the phase separator, refluxing the gas to the reaction tower, and purifying the aromatic sulfonic acid in a purification area provided under the reaction tower.
Abstract translation: 该制备涉及化学反应（I），R + H 2 SO 4→RSO 3 H + H 2 O（其中R为苯，甲苯，乙苯，二甲苯，克z唑，二甲苯酚，氯酚，甲氧基苯，二羟基苯，萘，甲基萘，氯萘酚 萘酚，蒽，苯胺，萘胺，氨基苯酚，甲苯胺，硝基苯，二乙苯，二丁胺，喹啉，三芳胺，甲基萘，二十烷和二己胺，其制备方法包括使芳族碳水化合物与硫酸反应，使芳族碳水化合物化合物磺酰化， 具体地说，该方法包括：通过多个进料口连续供给硫酸，用过量的磺酸磺酰化过量的芳族碳水化合物，以降低产物的浓度，芳香族磺酸，冷凝从塔 反应器从相分离器中除去水分，将气体回流至 反应塔，并在反应塔下提供的净化区域中纯化芳族磺酸。
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公开(公告)号：KR1019960012711B1
公开(公告)日：1996-09-24
申请号：KR1019940004466
申请日：1994-03-08
Applicant: 한국화학연구원
IPC: C01B33/32
Abstract: The layered sodium silicate is prepared by making anhydrous sodium silicate powder(X) with below 100 um avg. particle size that mole ratio of SiO2 to Na2O is 1.8-3.5, and making amorphous sodium silicate by heating and dehydrating sodium silicate solution that mole ratio of SiO2 to Na2O and H2O to Na2O controlled into 1.2-2.5 and 5.0-15.0 by adding sodium hydroxide to water glass at 150-400 deg.C for 0.002-10.0 hrs, and mixing 90-10 wt.% X and 10-90 wt.% Y and aging mixed powder for 0.1-5.0 hrs at 550-800 deg.C.
Abstract translation: 层状硅酸钠通过制备低于100平方米的无水硅酸钠粉末（X）制备。 SiO 2与Na 2 O的摩尔比为1.8-3.5的粒径，通过加热和脱水硅酸钠溶液制备无定形硅酸钠，通过加入氢氧化钠将SiO 2与Na 2 O和H 2 O的摩尔比与Na 2 O控制在1.2-2.5和5.0-15.0 在150-400℃的水玻璃中进行0.002-10.0小时，并在550-800℃下混合90-10重量％的X和10-90重量％的Y和时效的混合粉末0.1-5.0小时。
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