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公开(公告)号：WO2013012201A2
公开(公告)日：2013-01-24
申请号：PCT/KR2012/005524
申请日：2012-07-12
CPC classification number: C01F7/30 , B01J20/08 , B01J20/28004 , B01J20/28076 , B01J21/04 , B01J35/1019 , B01J35/1042 , B01J35/1047 , B01J35/1061 , B01J37/0009 , B01J37/036 , B01J37/10 , B82Y30/00 , C01F7/34 , C01F7/448 , C01P2002/60 , C01P2004/04 , C01P2004/52 , C01P2004/64 , C01P2006/14
Abstract: 본 발명은 촉매 담체, 흡착제 및 각종 표면 코팅제로 적합하게 사용될 수 있는 미세하고 균일한 입도 분포와 큰 기공 부피를 가지는 뵈마이트(boehmite) 또는 의사뵈마이트(pseudoboehmite) 구조의 다공성 알루미나의 제조방법에 관한 것이다.
Abstract translation:
本发明的勃姆石（勃姆石）或假（假勃姆石），其具有适度微细孔和大孔体积和均匀的粒度分布，其可以被用作催化剂载体，吸附剂和其它表面涂层结构 在这种情况下，
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公开(公告)号：KR101286108B1
公开(公告)日：2013-07-15
申请号：KR1020110033420
申请日：2011-04-11
Applicant: 한국화학연구원
Abstract: 본 발명은 고비점 유기 용매에 커플링제 및 텔륨 산화물을 혼합, 반응시켜 Te 나노와이어를 제조하고, 이를 비스무스(Bi) 화합물과 혼합함으로써 비스무스 이온의 환원에 의하여 Bi
2 Te
3 나노튜브를 제조하는 방법에 관한 것이다.
본 발명에 의하여 Bi
2 Te
3 나노튜브를 제조하는 경우 간단하면서도, 대량 제조가 가능하므로, 용액상에서 균일한 1차원 나노튜브를 제조에 광범위하게 적용될 수 있을 것으로 기대된다.-
公开(公告)号：KR1020120115851A
公开(公告)日：2012-10-19
申请号：KR1020110033420
申请日：2011-04-11
Applicant: 한국화학연구원
CPC classification number: C01B19/02 , C01G29/00 , C01P2002/70 , C01P2004/03 , C01P2004/04 , C01P2004/16
Abstract: PURPOSE: A manufacturing method of tellurium-based nano-wires and bismuth telluride nano-tubes is provided to obtain the tellurium-based nano-wires by mixing a coupling agent and tellurium oxides with organic solvents of high boiling points. CONSTITUTION: A manufacturing method of tellurium-based nano-wires includes the following: one or more organic solvents are mixed with a coupling agent to become a mixed solution; and a tellurium oxide selected from a group including TeO_2, TeO, TeO_3, Te_2O_5, and Te_4O_9 to be reacted. The organic solvents are selected from a group including ethylene glycol, oleic acid, oleylamine, hexadecane, ethylene diamine, dimethyl formamide, pyridine, and acetone. The coupling agent is made of trialkyl phosphine, trialkyl phosphine oxide, alkyl amine, alkyl thiol, phenyl sulfone, or aminophenyl sulfone. The pH value of the mixed solution is adjusted in a range between 8 and 13.
Abstract translation: 目的：提供碲基纳米线和碲化铋纳米管的制备方法，通过将偶联剂和氧化碲与高沸点有机溶剂混合来获得碲基纳米线。 构成：碲系纳米线的制造方法如下：将一种或多种有机溶剂与偶联剂混合成为混合溶液; 和选自TeO_2，TeO，TeO_3，Te_2O_5和Te_O4的基团中的氧化碲进行反应。 有机溶剂选自乙二醇，油酸，油胺，十六烷，乙二胺，二甲基甲酰胺，吡啶，丙酮等。 偶联剂由三烷基膦，三烷基氧化膦，烷基胺，烷基硫醇，苯基砜或氨基苯基砜制成。 将混合溶液的pH值调节在8和13之间的范围内。
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公开(公告)号：KR1020120070740A
公开(公告)日：2012-07-02
申请号：KR1020100132175
申请日：2010-12-22
Applicant: 한국화학연구원
CPC classification number: C01B19/04 , B82Y40/00 , C01G29/00 , C01P2004/13
Abstract: PURPOSE: A tellurium nanotube of solvothermal synthesis and a manufacturing method of bismuth telluride are provided to manufacture Te nano-tube by reacting a high-boiling point organic solvent, coupling agent, and Tellurium compound and to mass produce Bi2Te3 nano-tubes. CONSTITUTION: A tellurium nanotube of solvothermal synthesis comprises the following steps: manufacturing a mixed solution by mixing organic solvent with a coupling agent; and reacting tellurium compound in the mixture. The organic solvent is one or more kinds which are selected from ethylene glycol, oleic acid, oleylamine, hexadecane, ethylenediamine, dimethylformamide, pyridine, and acetone. The coupling agent is selected from polyviny pyrrolidone, polyvinylalcohol, cetyl-trimethyl-ammonium-bromide, ethylenediaminotetraacetic acid disodium salt, and sodium dodecyl-benzene-sulfonate. A manufacturing method of the Bi2Te3 nanotubes comprises a step of reacting a solution including bismuth compound and reducing agent with a solution which includes Te nano-tubes.
Abstract translation: 目的：提供溶剂热合成的碲纳米管和碲化铋的制备方法，通过使高沸点有机溶剂，偶联剂和碲化合物反应制备Te纳米管，并大量生产Bi2Te3纳米管。 构成：溶剂热合成碲纳米管包括以下步骤：通过将有机溶剂与偶联剂混合制备混合溶液; 并使碲化合物在混合物中反应。 有机溶剂是选自乙二醇，油酸，油胺，十六烷，乙二胺，二甲基甲酰胺，吡啶和丙酮中的一种或多种。 偶联剂选自聚乙烯吡咯烷酮，聚乙烯醇，十六烷基 - 三甲基溴化铵，乙二胺四乙酸二钠盐和十二烷基苯磺酸钠。 Bi2Te3纳米管的制造方法包括使包含铋化合物和还原剂的溶液与包含Te纳米管的溶液反应的步骤。
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公开(公告)号：KR1020110093395A
公开(公告)日：2011-08-18
申请号：KR1020100013423
申请日：2010-02-12
CPC classification number: C04B28/08 , C04B14/02 , C04B20/0096 , C04B40/0032 , C04B2103/10 , C04B2103/302 , C04B24/10 , C04B24/18 , C04B24/223
Abstract: PURPOSE: Cementless concrete using blast slag and a method for manufacturing the same are provided to adequately control the mobility and a time for a coagulating process by coating a water-reducing agent mixed with sugar to the blast slag and adding an activator. CONSTITUTION: Blast slag, fine aggregate, and a water reducing agent mixed with sugar are mixed in a mixer. An activator, coarse aggregate, and water are additionally introduced into the mixer and are mixed. The water reducing agent mixed with super is composed of the combination of sugar and at least one of a melamine-based material or a lignin-based material. The content of the water reducing agent mixed with sugar is 1.5 to 4.5 parts by weight, based on 100 parts by weight of the blast slag. The activator includes at least one of sodium hydroxide or sodium silicate.
Abstract translation: 目的：提供使用鼓风炉渣的无水泥混凝土及其制造方法，以通过将与糖混合的减水剂涂布在高炉渣中并加入活化剂来充分控制凝结过程的流动性和时间。 构成：将混合有高炉渣，细骨料和与糖混合的减水剂混合在混合器中。 将活化剂，粗骨料和水另外引入混合器中并混合。 与超级混合的减水剂由糖和三聚氰胺类材料或木质素类材料中的至少一种组合构成。 与糖混合的减水剂的含量相对于100重量份的炉渣为1.5〜4.5重量份。 活化剂包括氢氧化钠或硅酸钠中的至少一种。
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Patent Agency Ranking
公开(公告)号：KR100787191B1
公开(公告)日：2007-12-21
申请号：KR1020060081601
申请日：2006-08-28
CPC classification number: C01F7/441 , C01F7/34 , C01P2002/72 , C01P2004/20 , C01P2004/54 , C01P2004/61 , C01P2006/80 , C09C1/407 , Y10T428/2982
Abstract: A method for preparing flaky alpha-alumina crystals is provided to allow easy control of the thickness and size of the crystals, to maintain an aspect ratio of at least 100, and to realize the use of the alpha-alumina crystals as a matrix for a high-quality pearl pigment, ceramic material or filler. A method for preparing flaky alpha-alumina crystals comprises the steps of: mixing an aqueous aluminum precursor solution containing an aqueous solvent with an aqueous precursor solution containing 0.05-5 parts by weight of a zinc precursor and 0.01-0.5 parts by weigh of a tin precursor based on 100 parts by weight of the aluminum precursor to provide an aqueous metal precursor solution; titrating the aqueous metal precursor solution with an aqueous sodium salt solution to a pH of 6.0-7.5 and carrying out hydrolysis to obtain a mixed gel; pretreating the mixed gel by aging the mixed gel at 60-100 deg.C for 5-30 hours, followed by drying; drying the pretreated gel at 60-200 deg.C for 5-30 hours; crystallizing the dried gel at 850-1300 deg.C for 1-8 hours to obtain crystallized cake; and cooling the crystallized cake to room temperature, dissolving the cake into water at 20-90 deg.C, followed by filtering to remove the solvent, and dispersing the resultant product into 0.1-30% sulfuric acid solution at 20-90 deg.C, followed by filtering, washing with water and drying to obtain alpha-alumina crystals. Further, the aluminum precursor is selected from acid salts of an aluminum, a halide and an oxide.
Abstract translation: 提供了制备片状α-氧化铝晶体的方法，以便容易地控制晶体的厚度和尺寸，以保持至少100的纵横比，并且实现使用α-氧化铝晶体作为基体的 高品质珍珠颜料，陶瓷材料或填料。 制备片状α-氧化铝晶体的方法包括以下步骤：将含有水性溶剂的含水铝前体溶液与含有0.05-5重量份锌前体的水性前体溶液和0.01-0.5重量份锡 基于100重量份的铝前体的前体，以提供金属前体溶液; 用钠盐水溶液滴定含水金属前体溶液至pH 6.0-7.5，并进行水解得到混合凝胶; 通过将混合凝胶在60-100℃下老化5-30小时来预处理混合凝胶，然后干燥; 将预处理的凝胶在60-200℃干燥5-30小时; 将干燥的凝胶在850-1300℃下结晶1-8小时，得到结晶饼; 并将结晶的滤饼冷却至室温，将滤饼溶解在20-90℃的水中，然后过滤除去溶剂，并将所得产物分散在20-30℃的0.1-30％硫酸溶液中 ，然后过滤，用水洗涤并干燥，得到α-氧化铝晶体。 此外，铝前体选自铝，卤化物和氧化物的酸式盐。
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公开(公告)号：KR1020010056165A
公开(公告)日：2001-07-04
申请号：KR1019990057602
申请日：1999-12-14
Applicant: 한국화학연구원
IPC: B01J20/00
CPC classification number: B01J20/3078 , B01J20/20 , B01J2220/42
Abstract: PURPOSE: A method for manufacturing a multi-functional granular adsorptive material is provided to fundamentally improve demerits of an existing manufacturing method which is artificially combined simply using zeolite, activated carbon and binder by directly manufacturing zeolite and an activated carbon composite material using raw materials of bran and sodium aluminate aqueous solution. CONSTITUTION: The method for manufacturing a multi-functional granular adsorptive material comprises the processes of granulating the blended material by blending bran powder and sodium aluminate aqueous solution; and performing hydrothermal treatment using a sodium hydroxide aqueous solution after passing the granulated materials through carbonization and activation processes, wherein the carbonization process is performed under the temperature condition of 400 to 700 deg.C, or 750 to 950 deg.C under the infusion of steam, wherein the hydrothermal treatment comprises the processes of adding 3 to 8 wt.% of alkaline aqueous solution, aging at a temperature of 10 to 60 deg.C, and crystallization at a temperature of 80 to 110 deg.C, and wherein the adsorptive material is characterized in that a content of A, X or Y type zeolite is 55 to 70 wt.%, and a content of an activated carbon is 30 to 45 wt.%.
Abstract translation: 目的：提供一种多功能颗粒状吸附材料的制造方法，从根本上改善现有的制造方法的缺点，即现有的制造方法，简单地使用沸石，活性炭和粘合剂通过直接制造沸石和活性炭复合材料，人造组合使用原料 麸皮和铝酸钠水溶液。 构成：多功能颗粒状吸附材料的制造方法包括通过混合麸粉和铝酸钠水溶液对混合材料进行造粒的方法; 并且在通过碳化和活化方法使造粒材料通过之后，使用氢氧化钠水溶液进行水热处理，其中碳化过程在400-700℃或750-950℃的温度条件下进行， 蒸汽，其中水热处理包括加入3至8重量％的碱性水溶液，在10至60℃的温度下老化并在80至110℃的温度下结晶的方法，其中 吸附材料的特征在于，A，X或Y型沸石的含量为55〜70重量％，活性炭的含量为30〜45重量％。
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公开(公告)号：KR1019950031902A
公开(公告)日：1995-12-20
申请号：KR1019950013679
申请日：1995-05-29
Applicant: 한국화학연구원
IPC: C01B33/32
Abstract: 본 발명은 층상결정성 이규산나트륨의 제조방법에 관한 것으로서, 더욱 상세하게는 SiO
2 /Na
2 O이 몰비가 1.80~2.20 범위로 저정되어 생산된 컬릴(cullet)분말을 출발물질로 하여 여기에 소량의 물을 가하여 조립입상물을 먼저 제조하고 이 조립입상물을 소성로에 투입한 다음 소성공정만을 거치는 간단한 방법으로 층상결정성 이규산나트륨을 제조함으로써, 기존방법에 비하여 제품의 순도를 높이고 제조공정을 단순화 하는 한편, 에너지 소모를 획기적으로 줄일 수 있어 원가절감은 물론 장치내에 반응물이 침적되는 현상을 개선하여 물 연화제(water softmer) 또는 세제조성물의 빌더(builder)로서 유용한 층상결정성 이규산나트륨의 새로운 제조방법에 관한 것이다.-
公开(公告)号：KR101451302B1
公开(公告)日：2014-10-16
申请号：KR1020120091694
申请日：2012-08-22
Applicant: 한국화학연구원
Abstract: 본 발명은 비스무트 텔루라이드(Bi
2 Te
3 ) 나노튜브의 제조방법 및 이에 따라 제조되는 열전특성이 향상된 비스무트 텔루라이드(Bi
2 Te
3 ) 나노튜브를 제공하는데 있다. 이를 위하여 본 발명은 트리옥틸포스핀옥사이드(tri-octylphosphineoxide, TOPO), 제 3 인산소다(Na
3 PO
4 ·12H
2 O), 소듐도데실벤젠설퍼네이트(sodium dodecyl-benzene-sulfonate, SDBS) 및 세틸트리메틸암모늄브로마이드(cetyl-trimethyl-ammonium-bromide)로 이루어진 군으로부터 선택되는 1종과 폴리비닐피롤리돈(Polyvinylpyrrolidone, PVP), 폴리비닐알콜(polyvinylalcohol) 및 에틸렌다이아미노테트라아세트산 염(sodium dodecyl-benzene-sulfonate)으로 이루어진 군으로부터 선택되는 1종으로 이루어진 캡핑제(capping agent)를 포함하는 용매에 산화텔루륨(TeO
2 )을 용해하고 환원제를 첨가하여 텔루륨 나노와이어를 제조하는 단계(단계 1); 비스무트 전구체 용액을 상기 단계 1의 텔루륨 나노와이어와 혼합하고 환원제를 첨가하여 혼합용액을 제조하는 단계(단계 2); 및 상기 단계 2의 혼합용액을 열처리하여 비스무트 텔루라이드(Bi
2 Te
3 ) 나노튜브를 제조하는 단계(단계 3);를 포함하는 비스무트 텔루라이드(Bi
2 Te
3 ) 나노튜브의 제조방법을 제공한다.-
公开(公告)号：KR101420084B1
公开(公告)日：2014-07-21
申请号：KR1020130053316
申请日：2013-05-10
Applicant: 한국화학연구원
CPC classification number: D01F6/905 , D01D5/003 , D01D5/0046 , D01D5/0076 , D01D10/06 , D06M11/83
Abstract: The present invention relates to a method for manufacturing conductive long fiber and conductive long fiber manufactured thereby. More particularly, the present invention provides a method for manufacturing long fiber, comprising the steps of: manufacturing conductive long fiber by electrospinning a spinning solution including poly(amide-co-imide) and Poly(trimellitic anhydride chloride-co-4,4′-methylenedianiline), which are mixed in a weight ratio of 4.5:5.5 to 5.5:4.5 (step 1); and coating the surface of the long fiber with conductive particles by immersing the long fiber, which has been manufactured in the step 1, sequentially in aqueous solution of polyethyleneglycol (PEG), solution of conductive metal precursors and washing liquid (step 2), wherein step 2 is conducted continuously as the long fiber is moved to a recovery part for recovering long fiber. The method for manufacturing conductive long fiber according to the present invention does not require many devices or much time compared with existing surface treatment by alkali solution for electroless plating or a method using a precious metal catalyst. In addition, the present invention can be applied easily to industrial scenes as a single process for continuously coating can be developed, thus reducing electroless plating time and increasing productivity greatly.
Abstract translation: 本发明涉及一种用于制造由此制造的导电长纤维和导电长纤维的方法。 更具体地说，本发明提供一种长纤维的制造方法，包括以下步骤：通过静电纺丝包含聚（酰胺 - 酰亚胺）和聚（偏苯三酸酐氯化物 - 共-4,4' - 亚甲基二苯胺），其以4.5:5.5至5.5:4.5的重量比（步骤1）混合; 并且通过将步骤1中制造的长纤维依次浸渍在聚乙二醇（PEG），导电金属前体和洗涤液的溶液（步骤2）中，将导电颗粒的表面依次涂覆在导电颗粒的表面上，其中 当长纤维移动到用于回收长纤维的回收部分时，步骤2连续进行。 本发明的导电性长纤维的制造方法与现有的无电解电镀用碱溶液的表面处理或使用贵金属催化剂的方法相比，不需要许多器件或多个时间。 此外，本发明可以容易地应用于工业场景，因为可以开发连续涂布的单一工艺，从而大大减少无电镀时间并提高生产率。
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