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    METHOD FOR PRODUCING AZINE COMPOUND AND OXIME COMPOUND
    161.
    发明专利
    METHOD FOR PRODUCING AZINE COMPOUND AND OXIME COMPOUND 审中-公开

    公开(公告)号：JP2003261525A

    公开(公告)日：2003-09-19

    申请号：JP2002063232

    申请日：2002-03-08

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07B61/00 ,  C07C249/00 ,  C07C249/04 ,  C07C249/16 ,  C07C251/42 ,  C07C251/44 ,  C07C251/88

    Abstract: PROBLEM TO BE SOLVED: To easily and efficiently obtain an oxime or an azine useful as a raw material for the oxime synthesis from an inexpensive raw material. SOLUTION: The azine represented by formula (3) (wherein, R a , R b , R c and R d are same or different, and each a hydrogen atom or a hydrocarbon group; R a and R b , or R c and R d may form a ring with an adjacent carbon atom by bonding to each other), or the oxime compound represented by formulas (4a) and/or (4b) (wherein, R a , R b , R c and R d are the same as the above) is formed by reacting a peroxide compound represented by formula (2) (wherein, R a , R b , R c and R d are the same as the above) with ammonia and water in the presence of an imide compound having a cyclic imide skeleton represented by formula (1) [wherein, n is 0 or 1; X is an oxygen atom or an -OR group (R is a hydrogen atom or a protective group of a hydroxyl group)]. COPYRIGHT: (C)2003,JPO

    METHOD FOR PRODUCING AMIDE COMPOUND
    163.
    发明专利
    METHOD FOR PRODUCING AMIDE COMPOUND 失效

    公开(公告)号：JP2002275142A

    公开(公告)日：2002-09-25

    申请号：JP2001072916

    申请日：2001-03-14

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  TATSUMI JUNRO

    IPC: B01J31/02 ,  C07B61/00 ,  C07C231/06 ,  C07C233/06

    Abstract: PROBLEM TO BE SOLVED: To provide a method capable of efficiently producing an amide compound by simple operation and apparatus. SOLUTION: This method for producing an amide compound comprises reacting (A) a compound capable of producing a radical with (B) a nitrile compound represented by the following formula (2): R CN (wherein R denotes an organic group) in the presence of (i) an imide compound having a cyclic imide skeleton represented by the following formula (I) [wherein X denotes oxygen atom or OR group (R denotes hydrogen atom or a protecting group of hydroxy group)] and (ii) one electron oxidant to produce the corresponding amide compound in which NHCOR group (R is the same as described above) is bound to a radical-producing site of the above compound (A).

    METHOD FOR MANUFACTURING KETONE
    164.
    发明专利
    METHOD FOR MANUFACTURING KETONE 失效

    公开(公告)号：JP2002265410A

    公开(公告)日：2002-09-18

    申请号：JP2001070425

    申请日：2001-03-13

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  KITAYAMA KENJI

    IPC: B01J31/36 ,  C07B61/00 ,  C07C45/34 ,  C07C49/203

    Abstract: PROBLEM TO BE SOLVED: To provide a method for manufacturing a ketone by efficiently oxidizing a terpene olefin to produce a corresponding ketone through a catalytic reaction using oxygen as an oxidant. SOLUTION: The method for manufacturing ketone is carried out by oxidizing a terpene olefin in the presence of an oxidation catalyst constituted with (A) a palladium compound and (B) a heteropolyacid or its salt, with a molecular oxygen to produce the corresponding ketone. Further, an ionic compound containing (C) a halide ion may coexist in the system. It is preferable that, in the manufacturing method, the heteropolyacid or the salt of the acid (B) contains at least one element selected from P, V, Mo and W as constituting element.

    METHOD FOR PRODUCING KETONE USING IMIDE COMPOUND AS CATALYST
    166.
    发明专利
    METHOD FOR PRODUCING KETONE USING IMIDE COMPOUND AS CATALYST 失效

    公开(公告)号：JP2002226423A

    公开(公告)日：2002-08-14

    申请号：JP2001025655

    申请日：2001-02-01

    Applicant: DAICEL CHEM

    Inventor： NAKAI TORU ,  ISHII YASUTAKA

    IPC: B01J31/04 ,  B01J31/20 ,  C07B61/00 ,  C07C45/39 ,  C07C49/403

    Abstract: PROBLEM TO BE SOLVED: To provide a method by which a ketone can efficiently be produced from a secondary alcohol under milder conditions. SOLUTION: This method for producing the ketone is characterized by making (ii) at least one reactional accelerator selected from an aromatic carboxylic acid or its salt and an aromatic aldehyde coexist in the reactional system in the reaction of (A) the secondary alcohol with (B) oxygen using (i) an imide compound having a cyclic imide skeleton represented by the following formula (I) [wherein, X denotes oxygen atom or an -OR group (R denotes hydrogen atom or a protecting group of hydroxy group)] as a catalyst.

    METHOD FOR PRODUCING ORGANIC PEROXIDE
    167.
    发明专利
    METHOD FOR PRODUCING ORGANIC PEROXIDE 失效

    公开(公告)号：JP2002155047A

    公开(公告)日：2002-05-28

    申请号：JP2000345824

    申请日：2000-11-13

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  TATSUMI JUNRO

    IPC: C07C407/00 ,  C07B61/00 ,  C07C409/20

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an organic peroxide, by which bis(1-hydroxycyclohexyl)peroxide can simply be produced from inexpensive raw materials. SOLUTION: This method for producing the organic peroxide, comprising reacting a cycloalkane with oxygen in the presence of a imide compound catalyst having an N-hydroxy(or N-oxo)cyclic imide skeleton to obtain the corresponding bis(1-hydroxycycloalkyl)peroxide. The imide compound catalyst includes a compound represented by formula (1) (R1 and R2 are each H, a halogen atom, an alkyl, an aryl, a cycloalkyl, or the like, or R1 and R2 may be bound to each other to form a double bond, or an aromatic or non-aromatic ring; X is O or HO) The cycloalkane includes a 5 to 15C cycloalkane.

    METHOD FOR PRODUCING POLYACRYLAMIDE-BASED POLYMER
    168.
    发明专利
    METHOD FOR PRODUCING POLYACRYLAMIDE-BASED POLYMER 失效

    公开(公告)号：JP2002145918A

    公开(公告)日：2002-05-22

    申请号：JP2000345822

    申请日：2000-11-13

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C08F4/00 ,  C08F20/00 ,  C08F20/56

    Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing a low-molecular weight polyacrylamide-based polymer. SOLUTION: This method comprises polymerizing an α,β-unsaturated carboxylic acid amide of formula (1) (wherein, Ra, Rb, Rc, Rd and Re are each H or a hydrocarbon group; at least two of Ra, Rb and Rc may be bound to each other to form a ring together with the adjoining one or two carbon atom(s); and Rd and Re may be bound to each other to form a ring together with the adjoining nitrogen atom) in the presence of an imide compound catalyst having an N-hydroxy or N-oxo cyclic imido skeleton and a radical-forming compound to obtain the objective polyacrylamide-based polymer composed of recurring unit of formula (2) (wherein, Ra, Rb, Rc, Rd and Re are each the same as mentioned above).

    METHOD FOR PRODUCING KETAL COMPOUND
    169.
    发明专利
    METHOD FOR PRODUCING KETAL COMPOUND 审中-公开

    公开(公告)号：JP2002060363A

    公开(公告)日：2002-02-26

    申请号：JP2001238204

    申请日：2001-08-06

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07C41/50 ,  C07B61/00 ,  C07C43/303

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a ketal compound, comprising oxidizing a diol compound with a halogen acid compound in high conversion and in high selectivity. SOLUTION: This method for producing a ketal compound comprises oxidizing a diol with an oxidation reactant comprising a halogen acid represented by the formula: M(XO3)n [M is H or a metal; X is a halogen atom; (n) is 1 or the valence of the metal M] or a salt thereof (bromic acid, iodic acid, their alkali metal salts, or the like) and a reducing inorganic compound (a sulfite, a bisulfite, a thiosulfite, a pyrosulfite, or the like) to produce the corresponding hydroxyketone compound, thus producing the ketal compound which is the addition product of the hydroxyketone to the diol.

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