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    실릴알킬벤조산 유도체 및 그의 제조 방법
    11.
    发明授权
    실릴알킬벤조산 유도체 및 그의 제조 방법 失效
    苯乙烯基苯甲酸衍生物及其制备方法

    公开(公告)号：KR100258158B1

    公开(公告)日：2000-06-01

    申请号：KR1019980012351

    申请日：1998-04-08

    Applicant: 한국과학기술연구원

    Inventor： 유복렬 ,  정일남 ,  조은정

    IPC: C07F7/02

    Abstract: PURPOSE: Provided are a novel silylalkyl benzoic acid derivative which is a precursor of silylalkyl benzoamide working as effective bactericide. And its manufacturing method is also provided. CONSTITUTION: The novel silylalkyl benzoic acid derivative is represented by the formula (3), wherein R is hydrogen, or a methyl group; n is 1 or 2; and X is hydrogen, meta or para-fluoro, chloro, or methyl group. And its manufacturing method is characterized by the following steps of: i) reacting a silylalkylated benzene derivative of the formula (1) with methyl grignard at 0-50 deg.C in the presence of aluminum chloride as catalyst under nitrogen gas to manufacture a trimethylsilylalkyl benzene derivative of the formula (2); and ii) oxidizing the benzene derivative at 100-150 deg.C in the presence of acetic acid cobalt as catalyst.

    Abstract translation: 目的：提供作为有效杀菌剂的甲硅烷基烷基苯甲酰胺的前体的新型甲硅烷基烷基苯甲酸衍生物。 并提供其制造方法。 构成：新型甲硅烷基烷基苯甲酸衍生物由式（3）表示，其中R是氢或甲基; n为1或2; 和X是氢，间位或对氟，氯或甲基。 其制造方法的特征在于以下步骤：i）在氮化铝存在下，在0-50℃下使式（1）的甲硅烷基烷基化的苯衍生物与甲基格氏体反应，制备三甲基甲硅烷基 式（2）的苯衍生物; 和ii）在乙酸钴作为催化剂存在下，在100-150℃氧化苯衍生物。

    실릴알킬벤조아미드 유도체, 그의 제조방법 및그를 유효성분으로 하는 농원예용 살진균제
    16.
    发明授权
    실릴알킬벤조아미드 유도체, 그의 제조방법 및그를 유효성분으로 하는 농원예용 살진균제 失效
    苯乙烯苯甲酸酯，其制备方法和农用化学品

    公开(公告)号：KR100250958B1

    公开(公告)日：2000-04-15

    申请号：KR1019980011273

    申请日：1998-03-31

    Applicant: 한국과학기술연구원

    Inventor： 유복렬 ,  정일남 ,  조은정 ,  김경미

    IPC: C07F7/10

    Abstract: PURPOSE: Provided are a silylalkylbenzoamid derivative of the formula (1) and its manufacturing method. And fungicide is also provided which containing the derivative as an active ingredient. CONSTITUTION: The silylalkylbenzoamid of the formula (1) is manufactured by treating silylalkylbenzoic acid derivative of the formula (2) with thiochloride to obtain benzoylchloride derivative; then reacting primary or secondary amine of the formula (3). Wherein R1 is hydrogen or linear or branched alkyl of C1-C4; R2 is branched or linear alkyl of C1-C4, cycloalkyl of C1-C6, aryl, phenyl, ortho-, meta-, or para-chlorophenyl; R3 is hydrogen or methyl group; X is hydrogen, meta- or para-fluoro, chloro or methyl group; Me is methyl group; and n is 1 or 2.

    Abstract translation: 目的：提供式（1）的甲硅烷基烷基苯并酰胺衍生物及其制备方法。 并且还提供含有衍生物作为活性成分的杀真菌剂。 构成：式（1）的甲硅烷基烷基苯甲酰胺通过用氯化盐处理式（2）的甲硅烷基烷基苯甲酸衍生物制得苯甲酰氯衍生物; 然后使式（3）的伯胺或仲胺反应。 其中R1是氢或C1-C4的直链或支链烷基; R2是C1-C4的支链或直链烷基，C1-C6的环烷基，芳基，苯基，邻 - ，间 - 或对 - 氯苯基; R3是氢或甲基; X是氢，间 - 或对 - 氟，氯或甲基; 我是甲基; n为1或2。

    유기 실란기 함유 4급 암모늄염 및 그의 제조방법
    19.
    发明授权
    유기 실란기 함유 4급 암모늄염 및 그의 제조방법 失效
    含有氨基甲酸酯的组合物及其制备方法

    公开(公告)号：KR100142146B1

    公开(公告)日：1998-07-01

    申请号：KR1019940015933

    申请日：1994-07-04

    Applicant: 한국과학기술연구원

    Inventor： 정일남 ,  한준수 ,  연승호 ,  조은정

    IPC: C07F7/18

    Abstract: 본 발명은 일반식(Ⅰ)으로 표시되는, 유기 실란 4급 암모늄염 및 그의 제조방법을 제공한다.

    상기식에서 R
    1 은 (RO)
    3 Si 또는 (MeO)
    3 SiCH
    2 ［(MeO)
    3 Si］CH이고, R
    2 는 H 또는 (RO)
    3 Si이며, Me는 메틸기이고 R은 탄소수 1-4개인 알킬기를 나타낸다.
    본 발명의 유기 실란은 섬유류의 위생 처리제로서 유용하다.

    폴리실라잔 및 그것의 제조방법
    20.
    发明授权
    폴리실라잔 및 그것의 제조방법 失效
    多晶硅及其制造方法

    公开(公告)号：KR1019970007491B1

    公开(公告)日：1997-05-09

    申请号：KR1019930008311

    申请日：1993-05-14

    Applicant: 한국과학기술연구원

    Inventor： 정일남 ,  이규환 ,  조은정

    IPC: C08G77/54

    Abstract: Polysilazane(I), which is useful as precursor of ceramic materials such as silicon nitride or carbonized silicon nitride being used as important material of ceramic industry, was prepared by the reaction of bis-silylmethane dissolved in organic solvent with or without methyl dichlorosilane and ammonia to give low molecular weight polysilazane, which is polymerized to give the title polysilazane(I). In formula, R1 and R2 are methyl or amide; if R2 is amide, R1 is methyl or hydrogen; 0.1

    Abstract translation: 用作陶瓷工业重要材料的陶瓷材料如氮化硅或碳化氮化硅的前体的聚硅氮烷（I）是通过溶解在有机溶剂中的双甲硅烷基甲烷与不含甲基二氯硅烷和氨的反应来制备的 得到聚合得到标题聚硅氮烷（I）的低分子量聚硅氮烷。 在式中，R 1和R 2是甲基或酰胺; 如果R2是酰胺，则R1是甲基或氢; 0.1

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