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公开(公告)号：KR100495674B1
公开(公告)日：2005-06-16
申请号：KR1020030041729
申请日：2003-06-25
Applicant: 한국과학기술연구원
IPC: H01M4/139
Abstract: 본 발명은 기판에 음의 바이어스 전압을 인가하면서 상온에서 상기 기판 상에 양극 활물질을 증착시켜, 열처리 공정을 거치지 않고 결정화된 양극 박막을 형성시키는 것을 특징으로 하는, 전기 화학적 특성이 우수한 전 고상 박막전지용 양극 박막의 제조방법, 이러한 방법으로 제조된 양극 박막 및 이를 이용한 전 고상 리튬 박막전지에 관한 것이다.
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公开(公告)号：KR100404733B1
公开(公告)日：2003-11-07
申请号：KR1020010032800
申请日：2001-06-12
Applicant: 한국과학기술연구원
IPC: H01M4/64
Abstract: PURPOSE: A current collector coated with a metal, an electrode employing the current collector and a lithium battery containing the electrode are provided to improve the conductivity and to allow the potential distribution on the surface of an electrode to be maintained uniformly, thereby enhancing the utilization rate of an electrode and the cycle characteristic and the charge/discharge characteristic of a battery. CONSTITUTION: The current collector is a foil, a punched foil, an expanded foil or a porous plate made of copper, nickel, aluminum or titanium, and whose both faces are coated with a metal with a thickness of several nm to several micrometers uniformly. Preferably the metal coating the current collector is selected from the group consisting of Ni, Cu, Ti, V, Cr, Mn, Fe, Co, Zn, Mo, W, Ag, Au, Ru, Pt, Ir, Al, Sn, Bi, Si, Sb and their alloys. The electrode comprises a lithium electrode made by coating the current collector with lithium; a carbon-coated carbon electrode; and a metal compound-coated metal compound electrode. The lithium battery comprises a cathode and an anode according to the electrode; a polypropylene or polyethylene separation membrane; and a polymer electrolyte or a solid electrolyte.
Abstract translation: 目的：提供涂有金属的集电器，采用集电器的电极和包含电极的锂电池，以提高导电性并使电极表面上的电位分布保持均匀，由此提高利用率 电极的速率和循环特性以及电池的充电/放电特性。 构成：集电器是由铜，镍，铝或钛制成的箔片，冲孔箔片，膨胀箔片或多孔板，并且它们的两个表面均匀涂覆有厚度为几纳米至几微米的金属。 优选地，集电器的金属涂层选自由Ni，Cu，Ti，V，Cr，Mn，Fe，Co，Zn，Mo，W，Ag，Au，Ru，Pt，Ir，Al，Sn， Bi，Si，Sb及其合金。 该电极包括通过用锂涂覆集流体而制成的锂电极; 碳涂覆的碳电极; 和金属化合物涂覆的金属化合物电极。 根据电极，锂电池包括阴极和阳极; 聚丙烯或聚乙烯分离膜; 和聚合物电解质或固体电解质。
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公开(公告)号：KR1020040037666A
公开(公告)日：2004-05-07
申请号：KR1020020066248
申请日：2002-10-29
Applicant: 한국과학기술연구원
CPC classification number: B82Y30/00 , C01G51/42 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/64 , C01P2006/40
Abstract: PURPOSE: Provided is a preparation method of LiCoO2 powder with nanosize particles and homogeneous particle size distribution by modifying the surface of (Li,Co)-precursors as starting materials and thermal treating. CONSTITUTION: The nanosize LiCoO2 powder is prepared by the following steps of: preparing (Li,Co)-precursors, starting materials, by dissolving Li-acetate and Co-acetate in water and freeze-drying mixed solution; surface-modifying (Li,Co)-precursor powder containing 100-130% of Li, by mixing precursor powder with soluble salt such as K2SO4, (NH4)2CO3, NaCl or KCl in a weight ratio of 6:1 through the mechanical process such as ball milling; heating to 400deg.C at 3deg.C/min and holding for 6hrs to form low-temperature polymorph, and then heating to 800deg.C and holding for 12hrs to get LiCoO2 powder with high-temperature polymorph; washing obtained powder with water to remove soluble salt of the surface of LiCoO2 powder. The resultant LiCoO2 powder is applied to the preparation of positive electrodes and metal oxides powder.
Abstract translation: 目的：提供具有纳米尺寸颗粒的LiCoO2粉末的制备方法，通过改变（Li，Co） - 前体的表面作为起始材料和热处理，均匀的粒度分布。 构成：通过以下步骤制备纳米尺寸的LiCoO2粉末：通过将Li-乙酸酯和乙酸钴溶解在水中并冷冻干燥混合溶液制备（Li，Co） - 前体，原料; 通过机械过程将前体粉末与可溶性盐如K 2 SO 4，（NH 4）2 CO 3，NaCl或KCl以6:1的重量比混合，将表面改性（Li，Co） - 前体粉末含有100-130％的Li 如球磨; 加热至400℃，保持6小时，形成低温多晶型，然后加热至800℃，保持12小时，得到高温多晶型LiCoO2粉末; 用水洗涤得到的粉末，以除去LiCoO2粉末表面的可溶性盐。 将所得的LiCoO 2粉末用于正极和金属氧化物粉末的制备。
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公开(公告)号：KR1020020074070A
公开(公告)日：2002-09-28
申请号：KR1020020010611
申请日：2002-02-27
Applicant: 지에스나노텍 주식회사 , 한국과학기술연구원
CPC classification number: B42D25/415 , B42D25/36
Abstract: PURPOSE: A method for coating a parylene polymer protection layer with good water resistance, heat resistance and chemicals resistance on a plastic card and its coating cartridge are provided, to improve the adhesion strength of the parylene polymer layer to the substrate. CONSTITUTION: The method comprises the steps of optionally washing a plastic card with isopropyl alcohol and highly pure water; optionally coating any one metal selected from the group consisting of Al, Cu, Ni and Pt on the surface of the plastic card; dipping a plastic card into the solution containing xylene and 1-15 wt% of trichlorovinylsilane to pretreat the card; optionally drying the card(substrate) sufficiently; and condensing the pyrolyzed vapor phase parylene monomer on the surface of a substrate to make the parylene polymer be coated on the surface. Also the method comprises the steps of coating a Li thin film on the some part of a plastic card; and condensing the pyrolyzed vapor phase parylene monomer on the surface of a substrate to make the parylene polymer be coated on the surface.
Abstract translation: 目的：提供一种在塑料卡及其涂料盒上涂覆具有良好的耐水性，耐热性和耐化学性的聚对二甲苯聚合物保护层的方法，以提高聚对二甲苯聚合物层与基材的粘附强度。 方案：该方法包括以下步骤：用异丙醇和高纯度水洗涤塑料卡; 任选地在塑料卡的表面上涂覆选自Al，Cu，Ni和Pt中的任一种金属; 将塑料卡浸入含有二甲苯和1-15重量％三氯乙烯基硅烷的溶液中预处理卡; 任选地对卡片（基材）充分干燥; 并将热解的气相聚对二甲苯单体在基材的表面上冷凝，使得聚对二甲苯聚合物涂覆在表面上。 此外，该方法包括在塑料卡的某部分上涂布Li薄膜的步骤; 并将热解的气相聚对二甲苯单体在基材的表面上冷凝，使得聚对二甲苯聚合物涂覆在表面上。
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公开(公告)号：KR1020140070468A
公开(公告)日：2014-06-10
申请号：KR1020130147569
申请日：2013-11-29
Applicant: 한국과학기술연구원
IPC: G01N33/563 , G01N33/53
Abstract: The present invention provides a method for diagnosing a biomarker and a biomarker diagnosis kit using a magnetic particle and a quantum dot for quantitative analysis. The method for diagnosing a biomarker comprises; (i) a step of providing magnetic particles in which a first antibody capable of collecting a biomarker is fixated on the surface using a linker; (ii) a step of providing quantum dots in which a second antibody capable of detecting the biomarker is fixated on the surface; (iii) a step of targeting and sandwiching the biomarker by the magnetic particles and the quantum dots; (iv) a step of selectively separating the quantum dots which targets and sandwiches the biomarker between the quantum dots; and (v) a step of quantifying the concentration of the biomarker by measuring the optical density or fluorescent density of the separated quantum dots.
Abstract translation: 本发明提供一种使用磁性粒子和量子点进行定量分析的生物标志物和生物标志物诊断试剂盒的诊断方法。 诊断生物标志物的方法包括： （i）提供磁性颗粒的步骤，其中使用接头将能够收集生物标志物的第一抗体固定在表面上; （ii）提供量子点的步骤，其中能够检测生物标志物的第二抗体固定在表面上; （iii）通过磁性粒子和量子点靶向和夹持生物标志物的步骤; （iv）选择性地分离在量子点之间靶向和夹持生物标志物的量子点的步骤; 和（v）通过测量分离的量子点的光密度或荧光密度来量化生物标志物的浓度的步骤。
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Patent Agency Ranking
公开(公告)号：KR100485336B1
公开(公告)日：2005-04-27
申请号：KR1020027016795
申请日：2000-06-12
Applicant: 한국과학기술연구원
IPC: H01M4/02
Abstract: 본 발명은 집전체 상에 10Å - 100 ㎛ 두께의 리튬층 또는 리튬 합금층과, 1Å - 10 ㎛ 두께의 다공성 금속층 또는 다공성 탄소층이 순차 적층된 다층 구조의 리튬 전극, 이의 제조방법 및 이를 포함하는 리튬전지를 제공한다. 보다 구체적으로는, 구리 또는 니켈 집전체 상에 10Å - 100 ㎛ 두께의 리튬층 또는 리튬 합금층과 1Å - 10 ㎛ 두께의 다공성 금속층 또는 다공성 탄소층을 차례로 형성시키는 것에 의하여 제조되는 다층 구조의 리튬 전극, 이의 제조방법 및 이를 포함하는 리튬전지를 제공한다.
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公开(公告)号：KR100447791B1
公开(公告)日：2004-09-08
申请号：KR1020027013108
申请日：2001-01-31
Applicant: 한국과학기술연구원
IPC: H01M4/38
Abstract: PURPOSE: A lithium-metal composite electrode, its preparation method and a lithium battery using the electrode are provided, to improve the conductivity of an electrode and to maintain the potential distribution of the surface of an electrode, thereby enhancing the utilization rate, the cycle lifetime and the charge/discharge efficiency of a battery. CONSTITUTION: The lithium-metal composite electrode comprises the mixture of lithium particle or lithium alloy particle and a metal. The metal is selected from the group consisting of Ni, Cu, Ti, V, Cr, Mn, Fe, Co, Zn, Mo, W, Ag, Au, Ru, Pt, Ir, Al, Sn, Bi, Si, Sb and their alloys. The lithium alloy is an alloy of the metal selected from the group consisting of Al, Sn, Bi, Si, Sb, B and their alloys, and lithium. The method comprises the steps of evaporation-depositing the lithium or lithium alloy and the metal on the current collector simultaneously by using the thin film making technique; and compressing the deposited one with a pressure of 10-100 kg/cm¬2.
Abstract translation: 目的：提供锂金属复合电极及其制备方法和使用该电极的锂电池，以提高电极的导电性并保持电极表面的电位分布，从而提高利用率，循环 寿命和电池的充电/放电效率。 构成：锂 - 金属复合电极包含锂颗粒或锂合金颗粒与金属的混合物。 金属选自由Ni，Cu，Ti，V，Cr，Mn，Fe，Co，Zn，Mo，W，Ag，Au，Ru，Pt，Ir，Al，Sn，Bi，Si，Sb 和他们的合金。 锂合金是选自Al，Sn，Bi，Si，Sb，B及其合金和锂的金属的合金。 该方法包括以下步骤：通过使用薄膜制造技术同时在集电器上蒸发沉积锂或锂合金和金属; 并用10-100kg / cm 2的压力压缩沉积的沉积物。
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公开(公告)号：KR100445792B1
公开(公告)日：2004-08-25
申请号：KR1020010032338
申请日：2001-06-09
Applicant: 한국과학기술연구원
IPC: H01M10/36
Abstract: 본 발명은 폴리프로필렌, 폴리에틸렌, 폴리비닐리덴플로라이드 또는 부직포 등의 분리막의 한 면에 박막제조기술에 의하여 리튬과 금속이 다층구조 또는 복합구조 형태로 수 ㎛ 내지 수십 ㎛ 두께로 피복되어 분리막과 일체화된 리튬전극을 제공한다. 또한, 상기의 리튬 전극을 이용하여 전지 용량, 고율 충방전 특성 및 싸이클 수명 특성이 향상된 리튬전지를 제공한다.
Abstract translation: 目的：提供一种在体内结合有分隔膜的锂电极和采用该电极的一次或二次锂电池，以提高电池的容量，充电/放电效率和寿命。 构成：锂电极与分隔膜结合在一起，分隔膜的一侧涂覆有锂和多层结构或复合结构的金属，厚度为几到几十微米。 金属选自Li，Al，Sn，Bi，Si，Sb，Ni，Cu，Ti，V，Cr，Mn，Co，Zn，Mo，W，Ag，Au，Ru，Pt及其它 合金。 分隔膜包含选自PP，PE，PVdF和非织造材料的材料。 二次锂电池包含锂电极和选自LiCoO2，LiNiO2，LiNiCoO2，LiMn2O4，V2O5和V6O13的正极活性材料。 一次锂电池包括锂电极和选自MnO2，（CF）n和SOCl2的正极活性材料。
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公开(公告)号：KR1019990086305A
公开(公告)日：1999-12-15
申请号：KR1019980019240
申请日：1998-05-27
Applicant: 한국과학기술연구원
IPC: H01M4/32
Abstract: 본 발명은 종래의 AB
5 계 니켈/금속수소 축전지의 한계인 고용량화와 AB
2 계 니켈/금속수소 축전지의 싸이클 수명, 자기방전율, 초기활성화 등의 문제점을 해결하기 위한 것으로서, AB
2 계 수소저장합금에 La을 첨가하고 불소화 처리를 행한 후 전극을 제조한 경우, 일정량의 La이 첨가되면 금속수소전극의 평탄압력이 낮아지고 사용 가능한 수소저장량의 증가에 의해 전극용량의 증가 및 우수한 싸이클 수명, 우수한 급속충방전특성, 또한 안정한 LaF
3 화합물의 형성으로 수소저장합금의 부식이 억제되었기 때문에 자기 방전율이 대폭 감소하고, 전해질에 KF를 일정량 첨가하므로써, 용액에 첨가한 불소가 니켈전극에 작용하여 니켈전극의 용량 및 싸이클 수명을 향상시키도록 한 니켈/금속수소 축전지의 제조방법을 제공한다.-
20.发明公开전 고상 박막전지용 양극 박막, 그 제조방법 및 이를이용한 리튬 박막전지 失效正极电极薄膜，通过蒸发沉积积极电极活性材料的准备方法，将负极偏压施加到底板，以及所有含有正极电极薄膜的固体锂电池电池
公开(公告)号：KR1020050001542A
公开(公告)日：2005-01-07
申请号：KR1020030041729
申请日：2003-06-25
Applicant: 한국과학기술연구원
IPC: H01M4/139
Abstract: PURPOSE: A positive electrode thin film for an all solid lithium thin film battery, its preparation method and an all solid lithium thin film battery containing the positive electrode thin film are provided, to improve electrochemical properties without heating process. CONSTITUTION: The positive electrode thin film is prepared by vapor depositing a positive electrode active material at a room temperature with impressing a negative bias voltage of 0 V to -70 V (except 0 V) by using a radio-frequency power supply device to a substrate, to form a crystallized positive electrode thin film on the substrate. Preferably the substrate is a silicon substrate, glass, a polymer or a metal substrate with a low melting point; and the positive electrode active material is a composite oxide of lithium and a transition metal. Preferably the positive electrode thin film has an initial discharge capacity of 63 μAh/cm2·μ m and a discharge capacity of 30 μAh/cm2·μm at about 65-300 cycle, and has a microcrystalline structure having a thickness of 200-500 nm and a size of 5-30 nm.
Abstract translation: 目的：提供一种全固体锂薄膜电池的正极薄膜及其制备方法和含有正极薄膜的全固体锂薄膜电池，以提高电化学性能，无需加热工艺。 构成：正电极薄膜是通过在室温下蒸镀正极活性物质，通过使用射频电源装置施加0V至-70V的负偏压（0V除外）来制备的。 在基板上形成结晶化的正极薄膜。 优选地，所述衬底是具有低熔点的硅衬底，玻璃，聚合物或金属衬底; 正极活性物质是锂和过渡金属的复合氧化物。 优选的是，正极薄膜的初期放电容量为63μAh/ cm 2·μm，放电容量为约30〜300μA/ cm，约为65-300次，具有厚度为200〜500nm的微晶结构 尺寸为5-30nm。
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