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    메조-마크로 기공을 갖는 산화마그네슘 구조체의 제조방법
    13.
    发明公开
    메조-마크로 기공을 갖는 산화마그네슘 구조체의 제조방법 有权
    用MESO-MACRO PORES制备氧化镁结构的方法

    公开(公告)号：KR1020130126437A

    公开(公告)日：2013-11-20

    申请号：KR1020120121550

    申请日：2012-10-30

    Applicant: 한국과학기술연구원

    Inventor： 김상우 ,  김인호 ,  문동주

    IPC: B01J21/10 ,  B01J19/12 ,  B01J23/755 ,  B01J6/00

    Abstract: Provided are a method for manufacturing a magnesium oxide structure and the magnesium oxide structure manufactured thereby. The magnesium oxide structure manufactured by a method according to the present invention has meso-macro pores and improves a surface area and strength, thereby providing a catalyst with improved catalyst activation. [Reference numerals] (AA) Mesoporous precursor;(BB) Additive;(CC) Powder mixture;(DD) Porous powder shaped article;(EE) Meso-macro porous structure;(FF) Inorganic binder

    Abstract translation: 提供一种制造氧化镁结构体的方法及其制造的氧化镁结构体。 通过根据本发明的方法制造的氧化镁结构具有中孔 - 大孔，并且改善了表面积和强度，从而提供了催化剂活化改进的催化剂。 （AA）介孔前体;（BB）添加剂;（CC）粉末混合物;（DD）多孔粉末成型制品;（EE）中大孔多孔结构;（FF）无机粘合剂

    1,1-디플루오로에탄 제조용 촉매 및 1,1-디플루오로에탄제조방법
    17.
    发明公开
    1,1-디플루오로에탄 제조용 촉매 및 1,1-디플루오로에탄제조방법 失效
    用于制备1,1-二氟乙烯的催化剂及其制备方法

    公开(公告)号：KR1020020045235A

    公开(公告)日：2002-06-19

    申请号：KR1020000074615

    申请日：2000-12-08

    Applicant: 한국과학기술연구원

    Inventor： 안병성 ,  송정환 ,  문동주 ,  박건유

    IPC: B01J23/44 ,  B01J37/02

    CPC classification number: B01J37/22 ,  B01J21/18 ,  B01J23/44 ,  C07C17/23 ,  C07C19/08

    Abstract: PURPOSE: Provided is a palladium catalyst which is used in a dehydrochlorination reaction such as changing HCFC to HFC. Presented also are the catalyst and the reaction conditions that bring about the high yield at low temperature and maintain the activity and the selectivity for a long period of time. CONSTITUTION: The preparation method of the catalyst and reaction method comprise: continuously treating activated carbon with aqueous solutions of HF and HCl and dipping palladium into it; reducing the above catalyst with hydrogen at 200-300°C before the dehydrochlorination reaction; and making 1,1-difluoroethane from 1,1-difluoro-1-chloroethane using the above catalyst(Pd/C) by dehydrochlorination reaction at 240-300°C and feeding 1,1-difluoro-1-chloroethane and hydrogen gas in a ratio of 2-6.

    Abstract translation: 目的：提供一种钯催化剂，其用于脱氯化氢反应，例如将HCFC改为HFC。 还提出了在低温下产生高产率并长期维持活性和选择性的催化剂和反应条件。 构成：催化剂的制备方法和反应方法包括：用HF和HCl水溶液连续处理活性炭，并将钯浸入其中; 在脱氯化氢反应前，在200-300℃用氢还原上述催化剂; 并使用上述催化剂（Pd / C），在240-300℃下通过脱氯化氢反应从1,1-二氟-1-氯乙烷制备1,1-二氟乙烷，并加入1,1-二氟-1-氯乙烷和氢气 比例为2-6。

    디플루오로메탄과 1,1,1-트리플루오로에탄을 포함하는냉매 혼합물
    18.
    发明授权
    디플루오로메탄과 1,1,1-트리플루오로에탄을 포함하는냉매 혼합물 失效
    111-包含二氟甲磺酸和111-三氟乙烯的制冷混合物

    公开(公告)号：KR100333503B1

    公开(公告)日：2002-04-25

    申请号：KR1020010034611

    申请日：2001-06-19

    Applicant: 한국과학기술연구원

    Inventor： 이병권 ,  임종성 ,  권영수 ,  김홍곤 ,  문동주

    IPC: C09K5/04

    Abstract: 본발명은제 1 성분으로디플루오로메탄(CHF, HFC-32), 제 2 성분으로 1,1,1-트리플루오로에탄(CHCF, HFC-143a)를포함하고, 제 3 성분으로사이클로프로판(CH, RC-270), 1,1,1,2,3,3,3-헵타플루오로프로판(CFCHFCF, HFC-227ea), 1,1,1,2,2-펜타플루오로프로판(CHCFCF, HFC-245cb), 1,1,1,2,3,3-헥사플루오로프로판(CHFCHFCF, HFC-236ea), 부탄(CH, R-600), 비스(디플루오로메틸)에테르(CHFOCHF, HFE-134) 및펜타플루오로에틸메틸에테르(CFCFOCH, HFE-245)로이루어진군 중에서선택된어느한 성분으로이루어진 HCFC-22 대체용냉매혼합물을제공한다.

    활성탄에 담지된 팔라듐 촉매 및 그의 제조 방법과, 이를 이용한 염화불화탄소로부터 불화탄화수소의 제법
    19.
    发明公开
    활성탄에 담지된 팔라듐 촉매 및 그의 제조 방법과, 이를 이용한 염화불화탄소로부터 불화탄화수소의 제법 失效
    钯催化剂支持的活性炭，其制备方法和氯化氢与氢氟烃的氢化反应使用制备的催化剂

    公开(公告)号：KR1020010017372A

    公开(公告)日：2001-03-05

    申请号：KR1019990032851

    申请日：1999-08-11

    Applicant: 한국과학기술연구원

    Inventor： 문동주 ,  안병성 ,  정문조 ,  박건유

    IPC: B01J23/44

    CPC classification number: B01J23/44 ,  B01J37/0009 ,  B01J37/02 ,  C07C17/23 ,  C07C21/00

    Abstract: PURPOSE: Disclosed are a palladium catalyst supported on active carbon, a preparation method thereof and a hydrogenation reaction of chlorofluorocarbon to hydrofluorocarbon using the prepared catalyst. CONSTITUTION: The active carbon used as catalyst support is pretreated with a basic solution of 0.2-1M NaOH at 60-80deg.C for 1-5hours two or five times. And the acid treatment of a hydrochloric acid may be also conducted whenever after the base treatment or the hydrogen fluorine treatment or before loading of palladium species. The palladium species is impregnated by the adsorption precipitation method or the co-precipitation method. The hydrogenation reaction, dehalogenation, of chlorofluorocarbon to hydrofluorocarbon is selectively preformed to increase the yield of HFC-32.

    Abstract translation: 目的：公开了使用制备的催化剂负载在活性炭上的钯催化剂，其制备方法和氯氟烃与氢氟烃的氢化反应。 构成：将用作催化剂载体的活性炭用0.2-1M NaOH的碱性溶液在60-80℃预处理1-5小时两次或五次。 每当碱处理或氢氟处理之后或钯物质负载之前，盐酸的酸处理也可以进行。 通过吸附沉淀法或共沉淀法浸渍钯物质。 选择性地进行氯氟烃与氢氟烃的氢化反应脱卤，以提高HFC-32的产率。

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