EVAPORATION PREVENTING DEVICE
    11.
    发明专利

    公开(公告)号:JPH02125199A

    公开(公告)日:1990-05-14

    申请号:JP27650088

    申请日:1988-11-01

    Abstract: PURPOSE:To sharply reduce the liquid nitrogen usage quantity by feeding nitrogen gas in a Dewar bottle and making the inner pressure the same as the pressure of the ambient air or slightly higher at the time of the ordinary operation in the Dewar bottle for a charged particle detector or the like. CONSTITUTION:An object to be cooled 2 in a Dewar bottle 3 is immersed in liquid nitrogen 1, and the cold end 10 of a helium gas circulation type adiabatic expansion refrigerator is fitted to the upper port of the Dewar bottle 3 with an O-ring seal 9. After the operation of the refrigerator is started, the nitrogen gas of a nitrogen gas cylinder 12 is fed into the Dewar bottle 3 while being controlled by a pressure reducing flow control valve 11 so that the inner pressure is made the same as the pressure of the ambient air or slightly higher. The valve 11 is closed after the temperature equilibrium is attained, and the operation of only the refrigerator is continued. The usage quantity of liquid nitrogen is sharply reduced, and the maintenance and management can be simplified.

    PRODUCTION OF COMPOSITE THERMOELECTRIC MATERIAL

    公开(公告)号:JPH11323402A

    公开(公告)日:1999-11-26

    申请号:JP14655898

    申请日:1998-05-11

    Abstract: PROBLEM TO BE SOLVED: To provide a method for finely dispersing a magnesium-silicon compound thermoelectric material, ceramics hollow particles, ceramics particles, etc., in an iron-silicon compound thermoelectric material. SOLUTION: A powdery mixture which comprises iron powder, silicon powder, cobalt powder and their inevitable metallic elements, in which atomic ratio of silicon to iron is 1:2 and 2 to 16% in atomic ratio of iron atoms are replaced with cobalt atoms and a powdery mixture in which atomic ratio of silicon to magnesium is 2:1 are simultaneously compounded at 5:1 to 1:1 by weight ratio and are subjected to a mechanical alloying treatment. Further the ceramics hollow particles are added to an obtained powder so as to be 20:1 to 1:1 by a weight ratio and then the mixture is subjected to the mechanical alloying treatment to produce a powdery mixture in which clear generation of ferrous-silicon compounds is suppressed. The obtained powder is sintered to obtain a sintered compact in which iron disilicide and magnesium silicide are alloyed at nanometer level or a sintered compact in which ceramics hollow particles are uniformly dispersed.

    INSTRUMENT FOR MEASURING CONSTANT-TEMPERATURE TRANSFORMATION, METHOD FOR MEASURING CONSTANT-TEMPERATURE TRANSFORMATION AND METHOD FOR MEASURING RESIDUAL AUSTENITE QUANTITY

    公开(公告)号:JPH02236444A

    公开(公告)日:1990-09-19

    申请号:JP5627789

    申请日:1989-03-10

    Abstract: PURPOSE:To rapidly execute temp. control and to determine a constant-temp. transformation curve of high accuracy by using a cooling medium having a large cooling power and making transformation measurement by a non-contact type system using magnetic force. CONSTITUTION:A high-temp. heating furnace 19 is heated up to the austenite area of about 900 deg.C and a sample is hung by a stainless steel wire 22 down to the position shown by 8b and is fixed by means of a clip 23. After the sample is held for a prescribed period of time, the clip 23 is removed to allow the sample to fall into a salt bath. The falling time of this time is recorded by a photoelectric tube and is determined as the time for starting the measurement of a change in the magnetic force. The sample is immediately cooled and the constant- temp. transformation is started. The magnetism of the sample is increased by the transformation in such a manner and the loss of weight generated by attracting a magnet 2 is indicated on a balance 1 and is displayed on a recorder. Since the balance 1 is of an electromagnetic balance type, the position of a tray is not displaced in a vertical direction even if the load changes. the distance between the sample and the magnet 5 does not, therefore, change and the influence on the load is not affected. The constant-temp. transformation curve of the high accuracy is obtd. in this way.

    THERMOELECTRIC MATERIAL CONTAINING DISPERSED SHORT THIN METALLIC WIRES AND ITS MANUFACTURE

    公开(公告)号:JP2000277815A

    公开(公告)日:2000-10-06

    申请号:JP8275999

    申请日:1999-03-26

    Abstract: PROBLEM TO BE SOLVED: To obtain a method for dispersing short thin metallic wires in a thermoelectric material composed of a magnesium-silicon compound and a thermoelectric material having superior thermoelectric characteristic. SOLUTION: A magnesium-silicon compound sintered body, in which short and thin metallic wires are uniformly scattered is obtained, in such a way that mixed powder in which the formation of a magnesium-silicon compound is clearly confirmed by X-ray diffraction is manufactured by mechanically alloying magnesium powder, silicon powder, and their inevitable metallic elements at an atomic ratio of 2:1 between magnesium atoms and silicon atoms. Then, after the short and thin metallic wires are mixed in the mixed powder at a rate of 5-30 vol.% with respect to 100 vol.% powder and the powder is dried, the powder is sintered under pressure.

    METHOD FOR FINING METALLOGRAPHIC STRUCTURE

    公开(公告)号:JPH1190615A

    公开(公告)日:1999-04-06

    申请号:JP27533097

    申请日:1997-09-22

    Abstract: PROBLEM TO BE SOLVED: To provide a method for fining metallographic structure. SOLUTION: This method for fining the metallographic structure is the one, in which cavitations (voids) in the molten metal are formed by giving high energy vibrating force to the metal during solidifying, newly formed solid crystal grains are crushed and decomposed with impact pressure generated when the cavitations disappear to fine the structure of the material. For example, in a device composed of electrodes 11 which applies AC current to a metallic sample 10 and an electromagnet 12 which impresses DC magnetic field, a high energy electromagnetic vibrating force is given to the metallic sample during the processing of the solidification by simultaneously impressing the electric current and the magnetic field, and the solid crystal grains are crushed and decomposed to execute the formation of the fine structure.

    PRODUCTION OF BULKY AMORPHOUS ALLOY MATERIAL SOLIDIFIED BY QUICK COOLING

    公开(公告)号:JPH08232027A

    公开(公告)日:1996-09-10

    申请号:JP3554495

    申请日:1995-02-23

    Abstract: PURPOSE: To produce a bulky (solid) material solidified by quick cooling, e.g. an amorphous alloy and to extend the application range of the material. CONSTITUTION: Starting material having a prescribed compsn. is melted, mixed and primarily solidified in a bulky state and the surface of the resultant solidified formed body is coated with a thin coating film having a higher m.p. than the solidified body. The coated solidified formed body is heated to a temp. above the m.p. of the solidified body and below the m.p. of the coating material and then it is solidified by quick cooling. The objective bulky material solidified by quick cooling is obtd. and the application range of the material is considerably extended.

    FORMATION OF CONTROLLING METALLIC STRUCTURE IN SOLID-LIQUID COEXISTING STATE

    公开(公告)号:JPH08103858A

    公开(公告)日:1996-04-23

    申请号:JP26135494

    申请日:1994-09-30

    Abstract: PURPOSE: To easily enable the formation of a material having uniform quality without defect by controlling fluid condition at the time of filling up a base material of solid-liquid coexistence in a mold through a porous body. CONSTITUTION: The solid-liquid coexisting material 3 is held in a container 2 of a solid-liquid coexisting body holding part (a) and pressed in the metallic mold 5 of a forming part (b) fitted with a stainless steel-made wire net 4 with a piston 1 and formed. The fluid condition of the metal material in the solid- liquid coexisting state is controlled at the time of filling the solid-liquid coexisting material 3 into the mold of the metallic mold 5, etc., through the porous body like wire net 4, etc., to restrain the entrapment of atmospheric gas into the forming body. The material 3 is made to be one kind selected from the metal or complex material containing metal and ceramic and/or plastic. By this method, the grain distribution and the shape of solid phase grains can be controlled.

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