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公开(公告)号:JPH0517023A
公开(公告)日:1993-01-26
申请号:JP19710491
申请日:1991-07-11
Applicant: AGENCY IND SCIENCE TECHN
Inventor: UEDA MINORU , UCHIDA KUNIO , ASO NOBORU
Abstract: PURPOSE:To provide a granular powder quantitative supply apparatus which can supply a small quantity of granular powder quantitatively without lowering the magnitude of vibration applied to a vibration type granular powder supply device to such a degree as to obstruct a flow of granular powder. CONSTITUTION:It is possible to freely control the space between a gate 3 for limiting the amount of passing of a granular powder flow F of a spiral surface 2 of the uppermost portion of a vibration type granular powder supply device and the outer peripheral wall 1 of the spiral surface, the distance of a supply hole 6 for granular powder from the gate 3, the position on the width of the spiral surface of the hold, and the diameter thereof.
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公开(公告)号:JP2000086218A
公开(公告)日:2000-03-28
申请号:JP26731898
申请日:1998-09-05
Applicant: AGENCY IND SCIENCE TECHN , OSHIMA SATORU , YUMURA MORIO , UCHIDA KUNIO , IGASAKI FUMIKAZU , KURIKI YASUNORI , NIWA SHUICHI , MIZUKAMI FUJIO , TOBA MAKOTO
Inventor: OSHIMA SATORU , YUMURA MORIO , UCHIDA KUNIO , IGASAKI FUMIKAZU , KURIKI YASUNORI , TANBA SHUICHI , MIZUKAMI FUJIO , TOBA MAKOTO
Abstract: PROBLEM TO BE SOLVED: To synthesize carbon nanotubes at a low temp. and in a high yield in the production of carbon nanotubes by the conventional vapor growth method and to obtain a catalyst for the synthesis. SOLUTION: A hydrocarbon oil contg. a catalyst consisting of a metal-contg. material is injected into a reactor kept at a high temp. in the presence of at least one thermal decomposition accelerator selected from cyanuric acid, isocyanuric acid and their derivs. and the hydrocarbon is thermally decomposed to synthesize the objective carbon nanotubes. The catalyst used in the synthesis of the carbon nanotubes consists of (i) a porous inorg. carrier, (ii) a metal and (iii) at least one thermal decomposition accelerator selected from cyanuric acid, isocyanuric acid and their derivs. The metal and the thermal decomposition accelerator are supported on the carrier.
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公开(公告)号:JPH09188600A
公开(公告)日:1997-07-22
申请号:JP99496
申请日:1996-01-08
Applicant: AGENCY IND SCIENCE TECHN
Inventor: TASAKA TEIJI , YODA SATOSHI , OSHIMA SATORU , YUMURA MORIO , UCHIDA KUNIO , KURIKI YASUNORI , IGASAKI FUMIKAZU
Abstract: PROBLEM TO BE SOLVED: To provide a carbon whisker having a diameter of μm order and easily handleable as an industrial product and provide its production process. SOLUTION: The carbon whisker has a diameter of 0.1-10μm. The whisker can be produced by generating arc discharge in an inert gas between an anode composed of graphite and a hydrogen-occluding metal and an arbitrary heat- resistant cathode to form a carbon deposit containing carbon whiskers on the cathode.
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公开(公告)号:JPH07256146A
公开(公告)日:1995-10-09
申请号:JP7408494
申请日:1994-03-18
Applicant: AGENCY IND SCIENCE TECHN
Inventor: IGASAKI FUMIKAZU , GOTO AKIHIRO , HORIUCHI YUKIHIKO , UCHIDA KUNIO
IPC: B03C7/02
Abstract: PURPOSE:To classify a large number of superfine particles into respective diameter ranges by utilizing the mobility of the particle by arranging an acicular electrode on the center axis of an outer tube, furnishing a tubular electrode to surround the tip of the acicular electrode and impressing a voltage between the electrodes. CONSTITUTION:A clean gas inlet hole 3 is provided at the center of one end 1A of an outer tube 1, a hole 2 to introduce a gas contg. superfine particles is furnished around the hole 3, and plural superfine particle discharge ports 7 to 9 are concentrically arranged on the outlet end. An acicular electrode 10 having a length of 70% of that of the outer tube 1 is furnished on the center axis of the outer tube 1, and further a tubular electrode 12 is provided on the outer periphery or inner periphery of the outer tube 1 to surround the tip of the acicular electrode 10. A power source 13 is furnished to impress a voltage between both electrodes 10 and 12. Consequently, the superfine particle entrained by a gas flows in the device by the mobility corresponding to the impressed voltage, and the particles are classified into respective diameter ranges and discharged from the discharge ports 7 to 9.
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公开(公告)号:JPH07216660A
公开(公告)日:1995-08-15
申请号:JP2603994
申请日:1994-01-28
Applicant: AGENCY IND SCIENCE TECHN
Inventor: OSHIMA SATORU , YUMURA MORIO , UCHIDA KUNIO , KURIKI YASUNORI , IGASAKI FUMIKAZU
Abstract: PURPOSE:To provide a process for the continuous mass-production of carbon nanotube while stabilizing electrical discharge and keeping the stability and reliability of the operation. CONSTITUTION:This apparatus for the continuous production of carbon nanotube is provided with a closed vessel 1, a cathode 2 placed in the closed vessel keeping the center axis in horizontal direction, an anode 6 horizontally placed in the closed vessel in a state opposite to the cathode face of the cathode and separating the center axis from the center of the cathode by a definite distance, driving mechanisms 4, 5 to continuously or intermittently rotate or reciprocate the cathode and the anode relative to each other, an anode-moving mechanism 7 for supporting and horizontally transferring the anode, an inert gas passing means 11 to pass an inert gas through the closed vessel, a power-supplying means 9 to apply a prescribed electric power between the anode and the cathode and a precipitate-removing means 8 to remove the substance precipitated on the cathode surface of the cathode.
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公开(公告)号:JPH0748111A
公开(公告)日:1995-02-21
申请号:JP21227093
申请日:1993-08-04
Applicant: AGENCY IND SCIENCE TECHN
Inventor: UCHIDA KUNIO , YUMURA MORIO , OSHIMA SATORU , KURIKI YASUNORI , YATSUSE KIYOSHI , IGASAKI FUMIKAZU
Abstract: PURPOSE:To provide a method capable of relatively easily removing carbon impurities from the carbon nanotubes containing the carbon impurities and obtaining the carbon nanotubes in a high quality. CONSTITUTION:The method for separating and purifying the carbon nanotubes comprises finely grinding carbon nanotubes containing carbon impurities into the fine product having an average particle diameter of $0.4 7mum, dispersing the finely ground product in a liquid, centrifuging the dispersion, filtering the formed supernatant containing fine particles having an average particle diameter of
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公开(公告)号:JPH02275752A
公开(公告)日:1990-11-09
申请号:JP9162289
申请日:1989-04-11
Applicant: AGENCY IND SCIENCE TECHN
Inventor: OTAKE TAKESHI , UCHIDA KUNIO , KAWAMURA MITSUTAKA , OKUBO TEIJI , IGASAKI FUMIKAZU
Abstract: PURPOSE:To obtain feedstock for mullite ceramics in low costs by forming a mixture of deironated and decarbonized coal ash and alumina and firing the products. CONSTITUTION:Alumina is added to deironated and decarbonized coal ash, the mixture is formed and fired to give the subject material. The ash is reduced less than 2wt.% in iron and less than 0.5wt.% in carbon. The deironation treatment is carried out by using a magnetic separator, when needed, followed by treatment with hydrochloric acid or sulfuric acid. The decarbonization is effected in order to reduce carbon residue (including unchanged coal) by calcinating at 800 to 900 deg.C after deironation. Unsatisfactory pretreatment forms foams during the firing of the formed products. The residual iron causes colored (red brown) products with market value reduced.
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公开(公告)号:JPH01122944A
公开(公告)日:1989-05-16
申请号:JP28144987
申请日:1987-11-06
Applicant: AGENCY IND SCIENCE TECHN
Inventor: OTAKE TAKESHI , KAWAMURA MITSUTAKA , UCHIDA KUNIO
Abstract: PURPOSE:To obtain the above molded product for burning hardly breaking or pulverizing in burning in the production of artificial light-weight aggregate and having improved mechanical strength, by applying an organic binder to the surface of the molded product of an inorganic material containing an inorganic binder. CONSTITUTION:An inorganic binder consisting of bentonite, clay, etc., is added to an inorganic material consisting of coal ash, garbage burnt ash, etc., at a ratio of 2-10wt.% and the blend is humidified to mold to a desired form. Furthermore, average particle size of the inorganic material is normally
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公开(公告)号:JPS62252354A
公开(公告)日:1987-11-04
申请号:JP9493486
申请日:1986-04-25
Applicant: AGENCY IND SCIENCE TECHN , MITSUBISHI HEAVY IND LTD
Inventor: KAWAMURA MITSUTAKA , OTAKE TAKESHI , UCHIDA KUNIO , SASAKI ATSUSHI , NOHARA HIDESHI , ITANO SHIGEO
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公开(公告)号:JP2001080912A
公开(公告)日:2001-03-27
申请号:JP25745799
申请日:1999-09-10
Applicant: AGENCY IND SCIENCE TECHN , OSHIMA SATORU , AGO HIROKI , YUMURA MORIO , UCHIDA KUNIO , IGASAKI FUMIKAZU , KURIKI YASUNORI
Inventor: OSHIMA SATORU , AGO HIROKI , YUMURA MORIO , UCHIDA KUNIO , IGASAKI FUMIKAZU , KURIKI YASUNORI
IPC: C01B31/02 , B01J27/043
Abstract: PROBLEM TO BE SOLVED: To industrially advantageously produce carbon nanotubes. SOLUTION: When a carbon-containing material is thermally decomposed in the presence of a catalyst substrate to produce carbon nanotubes, a series of steps, that is, (i) a step for thermally decomposing the carbon-containing material in the presence of the catalyst substrate to form the carbon nanotubes on the substrate, (ii) a step for separating the formed carbon nanotubes from the substrate, (iii) a step for applying and drying a catalyst fluid containing hyperfine catalyst particles on the substrate after the separation of the carbon nanotubes to regenerate the catalyst substrate and (iv) a step for thermally decomposing the carbon-containing material in the presence of the regenerated catalyst substrate to form the carbon nanotubes on the substrate are repeatedly carried out.
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