公开(公告)号：BRPI0611241A2

公开(公告)日：2010-12-07

申请号：BRPI0611241

申请日：2006-06-01

Applicant: BASF AG

Inventor： SCHERR GUENTER ,  ERHARDT RAINER ,  EICHFELDER ANDREAS ,  REIF MARTIN ,  HIRSCH STEFAN ,  SIEDER GEORG ,  HOLTMANN THOMAS ,  CIPRIAN JUERGEN ,  ASCHERL HERMANN ,  SCHNEIDER JOERG

IPC: C07D251/70

Abstract: The invention relates to a process for removing salts from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C 1 -C 13 -alkanol which optionally comprises one or two oxygen atoms as ether bonds and is optionally substituted by C 1 -C 4 -alkyl and/or hydroxyl, and also at least one alkali metal alkoxide or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, in which salts are removed from the reaction mixture by ion exchange over a cation exchanger and/or anion exchanger.

公开(公告)号：DE102005058855A1

公开(公告)日：2007-06-14

申请号：DE102005058855

申请日：2005-12-09

Applicant: BASF AG

Inventor： EICHFELDER ANDREAS ,  ERHARDT RAINER ,  REIF MARTIN ,  RUEBA EVA ,  SCHERR GUENTER ,  SCHNEIDER JOERG ,  WEILACHER DIETER

IPC: C08G12/42 ,  C09D7/12

Abstract: Process for the preparation of etherified melamine/formaldehyde condensates, in which first a methylolation of melamine with a formaldehyde component in the molar ratio of from 1:6 to 1:15, preferably at a pH of >7, is carried out. This is followed by an etherification of the resulting hydroxymethylation intermediate in the presence of a C1-C20-alkyl, preferably of a C1-C6-alcohol, particularly preferably of a C1-C4-alcohol, at a pH of 9.5 being established before, during and/or after the distillation. According to the invention, a plurality of hydroxymethylation, etherification and distillation steps follow in order to achieve an etherified melamine/formaldehyde condensate which is distinguished by a high degree of hydroxymethylation, a high solids content and a low viscosity.

公开(公告)号：NO20052782A

公开(公告)日：2005-06-15

申请号：NO20052782

申请日：2005-06-08

Applicant: BASF AG

Inventor： SCHERR GUENTER ,  SCHNEIDER JORG ,  SCHUPP HANS ,  EICHFELDER ANDREAS ,  ROBERT ALAIN ,  REIF MARTIN

IPC: C07D251/54 ,  C07D251/70

CPC classification number: C07D251/54 ,  C07D251/70

公开(公告)号：AU2003296653A1

公开(公告)日：2004-07-09

申请号：AU2003296653

申请日：2003-12-16

Applicant: BASF AG

Inventor： EICHFELDER ANDREAS ,  ROBERT ALAIN ,  REIF MARTIN ,  SCHNEIDER JORG ,  SCHERR GUNTER ,  SCHUPP HANS

IPC: C07D251/54 ,  C07D251/70

Abstract: In a process for preparing alkoxycarbonylaminotriazines, di- or triaminotriazines are reacted with cyclic carbonic esters and optionally with minor amounts of acyclic carbonic esters in the presence of an alcohol and of an alkali metal alkoxide or alkaline earth metal alkoxide as a base.

公开(公告)号：DE102005036584A1

公开(公告)日：2007-02-15

申请号：DE102005036584

申请日：2005-08-01

Applicant: BASF AG

Inventor： ERHARDT RAINER ,  EICHFELDER ANDREAS ,  RUEBA EVA ,  SCHERR GUENTER ,  REIF MARTIN

IPC: C08G12/42 ,  B05D7/26 ,  C03C17/32 ,  C04B41/48 ,  C09D161/32 ,  D21H19/26

公开(公告)号：DE102005025855A1

公开(公告)日：2006-12-14

申请号：DE102005025855

申请日：2005-06-06

Applicant: BASF AG

Inventor： SCHNEIDER JOERG ,  SCHERR GUENTER ,  ERHARDT RAINER ,  EICHFELDER ANDREAS ,  REIF MARTIN ,  HIRSCH STEFAN ,  SIEDER GEORG ,  HOLTMANN THOMAS ,  CIPRIAN JUERGEN ,  ASCHERL HERMANN

IPC: C07D251/18 ,  A61K31/53

Abstract: The invention relates to a process for preparing free-flowing, pulverulent alkoxycarbonylaminotriazine from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C1-C13-alkanol which optionally comprises one or two oxygen atoms in the form of ether bonds and is optionally substituted by C1-C4-alkyl and/or hydroxyl, and also at least one alkali metal or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, by atomizing and drying the reaction mixture in a spray drier.

公开(公告)号：DE102005025901A1

公开(公告)日：2006-12-07

申请号：DE102005025901

申请日：2005-06-06

Applicant: BASF AG

Inventor： SCHNEIDER JOERG ,  SCHERR GUENTER ,  ERHARDT RAINER ,  EICHFELDER ANDREAS ,  REIF MARTIN ,  HIRSCH STEFAN ,  SIEDER GEORG ,  HOLTMANN THOMAS ,  CIPRIAN JUERGEN ,  ASCHERL HERMANN

IPC: C07D251/40

公开(公告)号：BR0317303A

公开(公告)日：2005-11-08

申请号：BR0317303

申请日：2003-12-16

Applicant: BASF AG

Inventor： SCHNEIDER JOERG ,  SCHERR GUENTER ,  SCHUPP HANS ,  EICHFELDER ANDREAS ,  ROBERT ALAIN ,  REIF MARTIN

IPC: C07D251/54 ,  C07D251/70

Abstract: In a process for preparing alkoxycarbonylaminotriazines, di- or triaminotriazines are reacted with cyclic carbonic esters and optionally with minor amounts of acyclic carbonic esters in the presence of an alcohol and of an alkali metal alkoxide or alkaline earth metal alkoxide as a base.

公开(公告)号：DE10218617A1

公开(公告)日：2003-11-06

申请号：DE10218617

申请日：2002-04-25

Applicant: BASF AG

Inventor： SCHNEIDER JOERG ,  SCHERR GUENTER ,  SCHUPP HANS ,  EICHFELDER ANDREAS ,  ROBERT ALAIN ,  REIF MARTIN

IPC: C07D251/18 ,  C07D251/70 ,  C07D251/54

Abstract: Production of alkoxycarbonylamino-triazine compounds comprises reaction of a triazine with carboxylic acid esters in the presence of an alcohol and a base. The triazine is reacted with dimethyl carbonate and a 2-13C alcohol whose hydrocarbon group contains ether groups, in the presence of an alkali or alkaline earth methanolate as base. Process for the production of alkoxycarbonylamino-triazine compounds of formula (I) comprises reaction of a triazine of formula (II) with carboxylic acid esters in the presence of an alcohol and a base. The triazine of formula (II) is reacted with dimethyl carbonate and a 2-13C alcohol whose hydrocarbon group contains ether groups, in the presence of an alkali or alkaline earth methanolate as base. Y1 = H, 1-4C alkyl or phenyl, optionally substituted by 1-4C alkyl, alkoxy or halogen, or NR5R6; R1-R6 = H, COOX or X, provided that at least one of R1-R6 is COOX; X = 1-13C alkyl optionally containing 1-2 ether linkages; Y2 = H, 1-4C alkyl, amine or phenyl optionally substituted by 1-4C alkyl, alkoxy or halogen whereby when Y2 is not amine at least one of R1-R4 is H.

公开(公告)号：DE10151564A1

公开(公告)日：2003-04-30

申请号：DE10151564

申请日：2001-10-23

Applicant: BASF AG

Inventor： SCHNEIDER JOERG ,  SCHERR GUENTER ,  SCHUPP HANS ,  EICHFELDER ANDREAS ,  ROBERT ALAIN ,  REIF MARTIN

IPC: C07D251/18 ,  C07D251/70

Abstract: Production of alkoxycarbonylamino-triazine compounds comprises reaction of a triazine with carboxylic acid esters in the presence of an alcohol and a base. The triazine is reacted with dimethyl carbonate and a 2-13C alcohol whose hydrocarbon group contains ether groups, in the presence of an alkali or alkaline earth methanolate as base. Process for the production of alkoxycarbonylamino-triazine compounds of formula (I) comprises reaction of a triazine of formula (II) with carboxylic acid esters in the presence of an alcohol and a base. The triazine of formula (II) is reacted with dimethyl carbonate and a 2-13C alcohol whose hydrocarbon group contains ether groups, in the presence of an alkali or alkaline earth methanolate as base. Y = H, 1-4C alkyl or phenyl, optionally substituted by 1-4C alkyl, alkoxy or halogen, or NR R ; R -R = H, COOX or X, provided that at least one of R -R is COOX; X = 1-13C alkyl optionally containing 1-2 ether linkages; Y = H, 1-4C alkyl, amine or phenyl optionally substituted by 1-4C alkyl, alkoxy or halogen whereby when Y is not amine at least one of R -R is H.