11.
    发明专利
    未知

    公开(公告)号:DE59905958D1

    公开(公告)日:2003-07-17

    申请号:DE59905958

    申请日:1999-11-25

    Applicant: BASF AG

    Abstract: Method of purifying triethanolamine prepared by reacting aqueous ammonia with ethylene oxide in the liquid phase under pressure and at elevated temperature by removing excess ammonia, water and monoethanolamine from the reaction product, reacting the resulting crude product with ethylene oxide at temperatures of from 110 to 180° C., and then rectifying the mixture in the presence of phosphorous or hypophosphorous acid or compounds thereof.

    13.
    发明专利
    未知

    公开(公告)号:DE19855383A1

    公开(公告)日:2000-06-08

    申请号:DE19855383

    申请日:1998-12-01

    Applicant: BASF AG

    Abstract: The invention relates to a method for purifying triethanolamine which is produced by reacting aqueous ammonia with ethylene oxide in the liquid phase under pressure and at an increased temperature. To this end, excess ammonia, water and monoethanolamine are separated from the reaction product. The thus obtained crude product is reacted with ethylene oxide at temperatures of from 110 to 180 DEG C and is rectified in the presence of phosphorous or hypophosphorous acid or the compounds thereof.

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