PREPARATION OF LIQUID FORMULATIONS OF BASIC AZO DYES

    公开(公告)号:CA2424959A1

    公开(公告)日:2003-10-11

    申请号:CA2424959

    申请日:2003-04-10

    Applicant: BASF AG

    Abstract: A process for preparing liquid formulations of dyes of the general formula I (see formula I) where Y is chlorine or bromine, Z is hydrogen, chlorine, bromine, sulfonic ester, nitro or optionally substituted sulfamoyl, X is -O- or (see formula II) R is alkylene optionally interrupted by oxygen, (see formulas III or IV) m is 1 or 2, n is 0 or 1, p is 0, 1 or 2, An.THETA. is the equivalent of an anion, R1 and R2 are independently hydrogen, optionally substituted alkyl, alkenyl, cycloalkyl, aralkyl or aryl or combine with the joining nitrogen to form a heterocycle, R3 is hydrogen or optionally substituted alkyl, B is hydrogen or C1- to C4-alkyl, B1 is hydrogen, hydroxyl, C1- to C4-alkoxy or C1- to C4-alkyl, where R4 is optionally substituted alkyl and R5 is hydrogen or C1- to C4-alkyl, and the radical may also be an optionally substituted piperazine radical, by diazotizing an amine of the formula II and then coupling the diazonium salt onto a compound of the formula III and also optionally adding solubilizing additives, comprises effecting said diazotizing at a pH set to an acidic value using pure methanesulfonic acid or at least 20 mol% mixtures of methanesulfonic acid in monobasic acids.

    17.
    发明专利
    未知

    公开(公告)号:ES2093531T3

    公开(公告)日:1996-12-16

    申请号:ES94911934

    申请日:1994-03-21

    Applicant: BASF AG

    Abstract: PCT No. PCT/EP94/00873 Sec. 371 Date Sep. 29, 1995 Sec. 102(e) Date Sep. 29, 1995 PCT Filed Mar. 21, 1994 PCT Pub. No. WO94/23114 PCT Pub. Date Oct. 13, 1994A process for dyeing celluose-containing textile material with indigo comprises using an aqueous solution of leuco indigo prepared by catalytic hydrogenation and, after the leuco indigo has gone onto the textile material, converting it back into the pigment form in a conventional manner by air oxidation.

    19.
    发明专利
    未知

    公开(公告)号:DE102005044521A1

    公开(公告)日:2007-03-22

    申请号:DE102005044521

    申请日:2005-09-16

    Applicant: BASF AG

    Abstract: A process for coating a surface comprises said surface being coated with particles (A) comprising a core (a) and at least one envelope (b) other than said core (a), and optionally with at least one hydrophobicizing agent (B) and thereafter thermally treated.

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