12.
    发明专利
    未知

    公开(公告)号:DE1190929B

    公开(公告)日:1965-04-15

    申请号:DEB0073156

    申请日:1963-08-17

    Applicant: BASF AG

    Abstract: Adiponitrile is purified by cooling the liquid or heating the solid so as to produce a suspension of adiponitrile crystals in liquid adiponitrile at a temperature of below 2.0 DEG C., separating the crystals, e.g. on a filter press, vacuum filter, pressure filter or in a centrifuge, washing the crystals, e.g. with pure liquid adiponitrile or with water or an organic liquid, and returning the separated liquid adiponitrile, with or without the wash liquid, to the first or another crystallization zone. The wash liquid may be pure adiponitrile obtained by partly melting the separated solid adiponitrile, e.g. while still in the separation apparatus.

Patent Agency Ranking