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    DIELECTRIC BARRIER DISCHARGE PLASMA METHOD AND APPARATUS FOR SYNTHESIZING METAL PARTICLES
    223.
    发明申请
    DIELECTRIC BARRIER DISCHARGE PLASMA METHOD AND APPARATUS FOR SYNTHESIZING METAL PARTICLES 审中-公开
    用于合成金属颗粒的介电阻挡放电等离子体方法和装置

    公开(公告)号：WO2016095035A1

    公开(公告)日：2016-06-23

    申请号：PCT/CA2015/051326

    申请日：2015-12-15

    Applicant: UNIVERSITÉ LAVAL

    Inventor： FORTIN, Marc-André ,  BOUCHARD, Mathieu ,  SARRA-BOURNET, Christian ,  TURGEON, Stéphane

    IPC: B22F9/24 ,  C25C5/02

    CPC classification number: C25C7/06 ,  B22F1/0014 ,  B22F1/0018 ,  B22F9/12 ,  B22F9/16 ,  B22F2301/255 ,  B22F2999/00 ,  C25C1/20 ,  C25C5/02 ,  C25C7/00 ,  C25C7/02 ,  H05H1/00 ,  H05H1/2406 ,  H05H2001/2412 ,  H05H2242/10 ,  H05H2245/124 ,  B22F9/24 ,  B22F2202/13 ,  B22F2201/013 ,  B22F2201/02 ,  B22F2201/03 ,  B22F2201/04 ,  B22F2201/05 ,  B22F2201/10 ,  B22F2201/50

    Abstract: A dielectric barrier discharge (DBD) plasma apparatus for synthesizing metal particles is provided. The DBD plasma apparatus includes an electrolyte vessel for receiving an electrolyte solution comprising metal ions; an electrode spaced-apart from the electrolyte vessel; a dielectric barrier interposed between the electrolyte vessel and the electrode such that, when the electrolyte solution is present in the electrolyte vessel, the dielectric barrier and an upper surface of the electrolyte solution are spaced-apart from each other and define a discharge area therebetween; and gas inlet and outlet ports in fluid communication with the discharge area such that supplying gas in the discharge area while applying an electrical potential difference between the electrode and the electrolyte solution cause a plasma to be produced onto the electrolyte solution, the plasma interacting with the metal ions and synthesizing metal particles. A method for synthesizing metal particles using a DBD plasma apparatus is also provided.

    Abstract translation: 提供了一种用于合成金属颗粒的电介质阻挡放电（DBD）等离子体装置。 DBD等离子体装置包括用于接收包含金属离子的电解质溶液的电解质容器; 与电解质容器间隔开的电极; 插入在电解质容器和电极之间的电介质阻挡层，使得当电解质溶液存在于电解质容器中时，电介质阻挡层和电解质溶液的上表面彼此间隔开并限定其间的放电面积; 以及与放电区域流体连通的气体入口和出口端口，使得在电极和电解质溶液之间施加电位差的同时在排出区域中供应气体导致在电解质溶液上产生等离子体，等离子体与 金属离子和合成金属颗粒。 还提供了使用DBD等离子体装置合成金属颗粒的方法。

    非水電解質二次電池とその負極材料、負極材料の製造方法
    228.
    发明申请
    非水電解質二次電池とその負極材料、負極材料の製造方法 审中-公开
    非水电解质二次电池及其负极电极材料及其生产负极电极材料的方法

    公开(公告)号：WO2007072704A1

    公开(公告)日：2007-06-28

    申请号：PCT/JP2006/324715

    申请日：2006-12-12

    Applicant: 松下電器産業株式会社 ,  山本 輝明 ,  長谷川 正樹 ,  美藤 靖彦

    Inventor： 山本 輝明 ,  長谷川 正樹 ,  美藤 靖彦

    IPC: H01M4/38 ,  B22F1/00 ,  H01M4/02 ,  H01M4/04 ,  H01M10/40

    CPC classification number: H01M10/052 ,  B22F1/02 ,  B22F9/002 ,  B22F2998/00 ,  B22F2998/10 ,  H01M4/0488 ,  H01M4/13 ,  H01M4/131 ,  H01M4/139 ,  H01M4/366 ,  H01M4/38 ,  H01M4/386 ,  H01M4/485 ,  Y02E60/122 ,  Y02P70/54 ,  Y10T29/49108 ,  C22C1/1084 ,  B22F2201/11 ,  B22F2201/03 ,  B22F2201/05 ,  B22F1/0059 ,  B22F3/02

    Abstract: A negative-electrode material (10) for nonaqueous-electrolyte secondary cells which comprises an alloy (11) comprising silicon and a transition metal and, formed on the surface of the alloy (11), a silicon oxide film (12) and a transition-metal oxide film (13); a nonaqueous-electrolyte secondary cell; and a process for producing the negative-electrode material (10) for nonaqueous-electrolyte secondary cells. With respect to negative-electrode materials of the kind shown above for use in nonaqueous-electrode secondary cells represented by lithium secondary cells, investigations have been made on techniques for inhibiting the size reduction caused by a volume change during charging. However, an investigation has not been sufficiently made on the thicknesses of the silicon oxide film and transition-metal oxide film. None of the conventional techniques can give a negative-electrode material for nonaqueous-electrolyte secondary cells which has satisfactory withstand overvoltage characteristics, which are one of important properties required of memory-backup power supplies. In the negative-electrode material (10) for nonaqueous-electrolyte secondary cells, the ratio of the thickness of the transition-metal oxide film (13) to the thickness of the silicon oxide film (12) is from 0.44 to less than 1. This constitution is intended to improve withstand overvoltage characteristics.

    Abstract translation: 一种用于非水电解质二次电池的负极材料（10），其包括含有硅和过渡金属的合金（11），并且在合金（11）的表面上形成氧化硅膜（12）和过渡金属 - 氧化物膜（13）; 非水电解质二次电池; 和非水电解质二次电池用负极材料（10）的制造方法。 关于用于由锂二次电池表示的非水电极二次电池中使用的上述类型的负极材料，已经对用于抑制由充电期间体积变化引起的尺寸减小的技术进行了研究。 然而，对氧化硅膜和过渡金属氧化物膜的厚度尚未充分进行研究。 常规技术中没有一种能够提供具有令人满意的耐过电压特性的非水电解质二次电池的负极材料，这是存储备用电源所需的重要特性之一。 在非水电解质二次电池用负极材料（10）中，过渡金属氧化物膜（13）的厚度与氧化硅膜（12）的厚度的比例为0.44〜小于1。 该结构旨在提高耐受过电压特性。

    SOFT MAGNETIC COMPOSITE MATERIALS
    229.
    发明申请
    SOFT MAGNETIC COMPOSITE MATERIALS 审中-公开
    软磁复合材料

    公开(公告)号：WO2006135324A1

    公开(公告)日：2006-12-21

    申请号：PCT/SE2006/000722

    申请日：2006-06-15

    Applicant: HÖGANÄS AB ,  SKÅRMAN, Björn ,  YE, Zhou ,  JANSSON, Patricia

    Inventor： SKÅRMAN, Björn ,  YE, Zhou ,  JANSSON, Patricia

    IPC: H01F1/24 ,  B22F1/02 ,  H01F3/08

    CPC classification number: B22F3/02 ,  B22F1/0062 ,  B22F3/24 ,  B22F2003/241 ,  B22F2003/248 ,  B22F2998/00 ,  B22F2998/10 ,  B22F2999/00 ,  H01F1/14 ,  H01F1/24 ,  H01F1/33 ,  H01F3/08 ,  H01F27/255 ,  H01F41/0246 ,  Y10T428/12028 ,  B22F1/02 ,  B22F1/0003 ,  B22F3/1021 ,  B22F2201/00 ,  B22F2201/02 ,  B22F2201/10 ,  B22F2201/05

    Abstract: The present invention concerns a process for the manufacture of soft magnetic composite components comprising the steps of : die compacting a powder composition comprising a mixture of soft magnetic, iron or iron-based powder, the core particles of which are surrounded by an electrically insulating, inorganic coating, and an organic lubricant in an amount of 0.05 to 1.5 % by weight of the composition, said organic lubricant being free from metal and having a temperature of vaporisation less than the decomposition temperature of the coating; ejecting the compacted body from the die; heating the compacted body in a non reducing atmosphere to a temperature above the vaporisation temperature of the lubricant and below the decomposition temperature of the inorganic coating for removing the lubricant from the compacted body, and subjecting the obtained body to heat treatment at a temperature between 3000C and 600°C in water vapour. The invention also concerns soft magnetic composite components having a transverse rupture strength of at least 100 MPa, a permeability of at least 700 and a core loss at 1 Tesla and 400 Hz of at most 70W/kg.

    Abstract translation: 本发明涉及一种用于制造软磁性复合材料组件的方法，包括以下步骤：模压粉末组合物，该粉末组合物包含软磁性，铁或铁基粉末的混合物，其核心颗粒被电绝缘的， 无机涂层和有机润滑剂，其含量为组合物重量的0.05-1.5％，所述有机润滑剂不含金属，其蒸发温度小于涂层的分解温度; 将压实体从模具中弹出; 将压实体在非还原性气氛中加热至高于润滑剂蒸发温度的温度，并低于无机涂层的分解温度，以从压实体中除去润滑剂，并将所得体在300℃的温度下进行热处理 和600℃的水蒸汽。 本发明还涉及具有至少100MPa的横向断裂强度，至少700的渗透性和1特斯拉和400Hz至多70W / kg的磁芯损耗的软磁性复合材料组件。

    PROCESSES FOR SINTERING ALUMINUM AND ALUMINUM ALLOY COMPONENTS
    230.
    发明申请
    PROCESSES FOR SINTERING ALUMINUM AND ALUMINUM ALLOY COMPONENTS 审中-公开
    用于烧结铝和铝合金部件的方法

    公开(公告)号：WO2005066380A1

    公开(公告)日：2005-07-21

    申请号：PCT/US2003/038469

    申请日：2003-12-01

    Applicant: EX ONE CORPORATION ,  LIU, Jianxin

    Inventor： LIU, Jianxin

    IPC: C22C1/04

    CPC classification number: B22F3/225 ,  B22F3/1007 ,  B22F2998/00 ,  B22F2999/00 ,  C22C1/0416 ,  Y02P10/295 ,  B22F3/008 ,  B22F3/1055 ,  B22F2201/02 ,  B22F2201/05

    Abstract: Methods for sintering aluminum powder comprise providing aluminum powder and heating the aluminum powder in a nitrogen atmosphere containing a partial pressure of water vapor in the range of about 0.001 kPa to about 0.020 kPa to sinter the aluminum powder to a transverse rupture strength of at least about 13.8 MPa. The aluminum powder is not pressed together by a mechanical force that substantially deforms particles of said aluminum powder either prior to or during the step of heating. Articles comprising sintered aluminum powder. The sintered aluminum powder has a transverse rupture strength of at least about 13.8 MPa. The microstructure of the sintered aluminum powder contains no compositional concentration gradients indicative of the use of a sintering aid and no evidence of particle deformation having occurred by an application of a mechanical force prior to or during the sintering of the aluminum powder.

    Abstract translation: 烧结铝粉的方法包括提供铝粉末并在含有约0.001kPa至约0.020kPa范围内的水蒸气分压的氮气气氛中加热铝粉，以将铝粉末烧结至至少约的横向断裂强度 13.8MPa。 铝粉末不通过在加热步骤之前或加热步骤期间使铝粉末的颗粒基本上变形的机械力而被压在一起。 包含烧结铝粉末的制品。 烧结铝粉末的横向断裂强度为至少约13.8MPa。 烧结铝粉末的微观结构不包含指示使用烧结助剂的组成浓度梯度，并且在铝粉烧结之前或期间不施加机械力而没有发生颗粒变形的迹象。

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