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公开(公告)号：KR1020150090729A
公开(公告)日：2015-08-06
申请号：KR1020140011697
申请日：2014-01-29
Applicant: 국방과학연구소
Abstract: 본발명은 CPD(cyclopentadiene) 또는 DCPD(dicyclopentadiene)로부터 Pd 촉매를이용하여높은수율로 TCPD(tricyclopentadiene)를합성할수 있는방법에관한것으로, 질소환경이나고압에서의반응이아닌일반적인환경에서도재현성과효율이높은합성을가능하게했으며, 기존의 TCPD합성에가장큰 한계가되었던낮은수득률문제점을해결할수 있는장점이있다.
Abstract translation: 本发明涉及通过使用钯催化剂从高产率生产得到的环戊二烯（CPD）或二环戊二烯（DCPD）的三环戊二烯（TCPD）的合成方法，其中该方法通过反应既不能高效又可重复地合成 氮气也不在高压下，但即使在一般环境中; 并且具有解决先前关于低产率的问题的优点，这是传统TCPD综合的最大限制。
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公开(公告)号：KR1020120102381A
公开(公告)日：2012-09-18
申请号：KR1020110020508
申请日：2011-03-08
Applicant: 국방과학연구소
CPC classification number: C10L1/232 , C10L1/02 , C10L1/183 , C10L10/00 , C10L2200/04
Abstract: PURPOSE: A liquid fuel composition is provided to improve the thermal stability of exo-tetrahydrodicyclopentadiene(exo-THDCP) by adding a thermal stabilizer into the exo-THDCP. CONSTITUTION: A liquid fuel composition includes exo-THDCP as liquid fuel and a thermal stabilizer. 0.1 to 5.0 weight% of one or more selected from tetrahydroquinoline, benzyl alcohol, and tetrahydroquinoxaline is added into the exo-THDCP as the thermal stabilizer. The tetrahydroquinoline is represented by chemical formula 2. In chemical formula 2, R1 is CH_2; n is 2 or 3; and R2 is H, CH_3, or C_2H_5. The tetrahydroquinoxaline is represented by chemical formula 4. In chemical formula 4, R1 is H, CH_3, or C_2H_5; and R2 is H, CH_3, or C_2H_5.
Abstract translation: 目的：提供液体燃料组合物，以通过向外部THDCP中加入热稳定剂来改善外四氢二环戊二烯（exo-THDCP）的热稳定性。 构成：液体燃料组合物包含作为液体燃料的外加THDCP和热稳定剂。 将0.1〜5.0重量％的四氢喹啉，苄醇和四氢喹喔啉中的一种或多种添加到作为热稳定剂的外部THDCP中。 四氢喹啉由化学式2表示。在化学式2中，R 1是CH 2; n为2或3; R2是H，CH_3或C_2H_5。 四氢喹喔啉由化学式4表示。在化学式4中，R 1是H，CH 3或C 2 H 5; R2是H，CH_3或C_2H_5。
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公开(公告)号：KR1020110087923A
公开(公告)日：2011-08-03
申请号：KR1020100007580
申请日：2010-01-27
Applicant: 국방과학연구소
CPC classification number: B01J19/24 , B01J2219/24 , G01N33/22
Abstract: PURPOSE: A batch-type reactor for preventing the leakage of an internal pressure and an experimental method using the same are provided to maintain a pressure in the inside of a main body due to the deformation of a sealing unit generated at high temperature. CONSTITUTION: A receiving chamber receives a target which is capable of being heated based on heat at one end part of a main body(110). A cover(120) is mounted at another end part of the main body to cover an opening. A sealing unit is arranged between the cover and the main body to seal the receiving chamber. A cooling module is formed between the sealing unit and one end part of the main body in order to control the amount of heat transferred to the sealing unit.
Abstract translation: 目的：提供一种用于防止内部压力泄漏的分批式反应器和使用其的实验方法，以便由于在高温下产生的密封单元的变形而保持主体内部的压力。 构成：容纳室容纳能够在主体（110）的一个端部处基于热量加热的靶。 盖（120）安装在主体的另一端部以覆盖开口。 密封单元布置在盖和主体之间以密封接收室。 在密封单元和主体的一个端部之间形成冷却模块，以便控制传递到密封单元的热量。
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公开(公告)号：KR1020110079302A
公开(公告)日：2011-07-07
申请号：KR1020090136320
申请日：2009-12-31
Applicant: 국방과학연구소
IPC: C10L1/12
CPC classification number: C10L1/1208 , C10L2250/00 , C10L2300/20
Abstract: PURPOSE: A carbon slurry fuel composition and a producing method thereof are provided to secure the excellent dispersion stability and mobility of a carbon solid particle. CONSTITUTION: A producing method of a carbon slurry fuel composition comprises the following steps: inserting liquid fuel, a carbon solid particle, and a surfactant into a mixing container; and stirring the added components. The surfactant is based on polysobutenyl succinimide, and is obtained by reacting polyisobutenyl succinic anhydride with amine.
Abstract translation: 目的：提供一种碳浆燃料组合物及其制备方法，以确保碳固体颗粒的优异的分散稳定性和流动性。 构成：碳浆燃料组合物的制造方法包括以下步骤：将液体燃料，碳固体颗粒和表面活性剂插入混合容器中; 并搅拌添加的组分。 表面活性剂是基于聚异丁烯基琥珀酰亚胺，通过使聚异丁烯基琥珀酸酐与胺反应得到。
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公开(公告)号：KR1019990054992A
公开(公告)日：1999-07-15
申请号：KR1019970074895
申请日：1997-12-27
Applicant: 국방과학연구소
IPC: C30B7/06
Abstract: 본 발명은 각종 고체 로켓용 추진제나 폭약등에서 산화제로 사용되는 ε형 HNIW의 결정 크기를 원하는 값으로 제어하기 위한 결정화 방법에 관한 것으로, 회분식 결정화기에서 ε형 HNIW 결정을 종(seed)으로 사용하는 본 발명을 통해 수십에서 수천 ㎛에 이르는 크기 범위 내에서 목적으로 하는 결정 크기와 좁은 입도 분포를 갖는 ε형 HNIW 결정을 제조하는 것이다.
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Patent Agency Ranking
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公开(公告)号：KR1020160071038A
公开(公告)日：2016-06-21
申请号：KR1020140178252
申请日：2014-12-11
Applicant: 국방과학연구소
IPC: C07C2/08 , C07C13/605 , B01J31/02 , B01J23/74
CPC classification number: C07C2/08 , B01J23/74 , B01J31/02 , C07C13/605 , Y10S585/924
Abstract: 본발명은이온성액체촉매를사용하여디시클로펜타디엔(dicyclopentadiene)과시클로펜타디엔(cyclopentadiene)의소중합체인트리시클로펜타디엔(tricyclopentadiene)을효과적으로제조하는방법에관한것으로, 더욱상세하게는양이온촉매전구체로트리에틸아민클로라이드(triethylamine chloride, TEAC)이나 1-뷰틸-3-메틸이미다졸륨클로라이드(1-butyl-3-methylimidazolium chloride, BMIC)를포함하며, 음이온촉매전구체로삼염화철(iron(Ⅲ) chloride, FeCl)이나염화구리(copper chloride, CuCl)가포함된촉매전구체로이루어진이온성액체촉매를사용하여디시클로펜타디엔과시클로펜타디엔의소중합반응을통해트리시클로펜타디엔을효과적으로제조하는방법에관한것이다.
Abstract translation: 本发明涉及通过使用离子液体催化剂有效制备作为二环戊二烯和环戊二烯的低聚物的三环戊二烯的方法，更具体地说，涉及通过使用离子液体催化剂将二环戊二烯和环戊二烯低聚而有效制备三环戊二烯的方法，包括 含有氯化三乙胺（TEAC）或作为阳离子催化剂前体的1-丁基-3-甲基咪唑氯化物（BMIC）和作为阴离子催化剂前体的氯化铁（IIICl）或氯化铜（CuCl）的催化剂前体。
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公开(公告)号：KR101616071B1
公开(公告)日：2016-04-27
申请号：KR1020150146886
申请日：2015-10-21
Applicant: 국방과학연구소
CPC classification number: Y02P20/582
Abstract: 본발명은노르보나디엔(norbornadiene, bicyclo(2.2.1)heptadiene-2,5, NBD)의이량화반응을통해서노르보나디엔이량체(norbornadiene dimer)를제조하는방법에관한것으로, 더욱상세하게는불균일계촉매(heterogeneous catalyst)로미세기공(micro pore)의제올라이트촉매와중형기공(meso pore)의알루미노실리케이트촉매를사용하여노르보나디엔의이량화반응(dimerization reaction)을촉진시켜서노르보나디엔이량체를제조하는방법에관한것이다.
Abstract translation: 本发明涉及使用降冰片二烯（二环（2.2.1）庚二烯-2,5，NBD）的二聚反应的降冰片二烯二聚体的制备方法。 更具体地说，本发明的制备方法通过使用包含微孔沸石催化剂和中孔硅铝酸盐催化剂的多相催化剂促进降冰片二烯的二聚反应来制备降冰片二烯二聚体。
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公开(公告)号：KR101606405B1
公开(公告)日：2016-03-25
申请号：KR1020140026192
申请日：2014-03-05
Applicant: 국방과학연구소
Abstract: 본발명은연료의열안정도를향상시킬수 있는분산제와이의제조방법에대한것으로, 더욱상세하게는 PIBSA(Polyisobutenyl succinic anhydride)에아미노에테르기를포함하고있는물질(2,2'-(Ethylenedioxy)bis(ethylamine), 1,11-Diamino-3,6,9-trioxaundecanyl-11-ol, 1-Amino-3,6,9-trioxaundecanyl-11-ol, 등)을반응시켜 PIBSI 유도체를제조하여연료용분산제로활용하는것에대한발명이다. 이를이용하면, 액체연료(항공유, 경유, 휘발유)의열산화반응에의해생성되는탄소침적물의양을보다효과적으로감소시킬수 있다.
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公开(公告)号：KR1020160025290A
公开(公告)日：2016-03-08
申请号：KR1020140112342
申请日：2014-08-27
Applicant: 국방과학연구소
Abstract: 본발명은엔도-테트라하이드로트리(사이클로펜타디엔)의이성화반응을통해고부가가치연료인고밀도액체연료의원료물질로사용하기용이한엑소-테트라하이드로트리(사이클로펜타디엔)을제조하는방법에관한것이다. 구체적으로는불균질계고체산 촉매인제올라이트, 메조기공알루미노실리케이트, 12-텅스토인산세슘염의헤테로폴리산등을적용하여엔도-테트라하이드로트리 (사이클로펜타디엔)의이성화반응을통해엑소-테트라하이드로트리 (사이클로펜타디엔)을제조하는방법에관한것이다.
Abstract translation: 本发明涉及通过内四氢三环（环戊二烯）异构化制备外四氢三环（环戊二烯）的方法，其中外四氢三环戊二烯（环戊二烯）容易用作高密度液体燃料的原料，其为高 增值燃油。 具体地说，本发明涉及一种通过使用作为非均相基固体酸催化剂的沸石，介孔硅铝酸盐，12-碳酸铯盐的杂多酸，通过异四氢三环（环戊二烯）异构化生产外四氢三环（环戊二烯） 钨磷酸等。
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