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公开(公告)号：KR100734181B1
公开(公告)日：2007-07-02
申请号：KR1020060066094
申请日：2006-07-14
Applicant: 전남대학교산학협력단
Abstract: A spinning syringe is provided to make it possible to manufacture a dual fiber when a nanofiber is manufactured through electro-spinning, by constituting the spinning syringe in a dual type so as to spin two types of material simultaneously. A spinning syringe is composed of a small syringe(10), a large syringe(20), and a piston(30). A nozzle(11) is inserted into a front side of the small syringe. A rear side of the small syringe is opened, and a first solution is put into the small syringe through the rear side of the small syringe. The small syringe is inserted into the large syringe through an opened rear side of the large syringe. A dual nozzle(23) has a first spinning groove and a second spinning groove at an outer circumference of the first spinning groove. The nozzle of the small syringe is contacted with the first groove of the dual nozzle. The dual nozzle is filled with a second solution. The piston is inserted into the large syringe, and a joining pole(32) is extended from a front side of the piston in a longitudinal direction of the piston. The joining pole is screw-joined to a small syringe pressing body(31), wherein the small syringe pressing body presses an inside of the small syringe to spin the first solution. The piston is screw-joined to a large syringe pressing body(33), wherein the large syringe pressing body presses the second solution within the large syringe.
Abstract translation: 提供纺丝注射器以通过电纺丝来制造纳米纤维时通过以双重类型构造纺丝注射器以同时纺制两种类型的材料来制造双纤维。 旋转注射器由小注射器（10），大注射器（20）和活塞（30）组成。 喷嘴（11）插入小注射器的前侧。 小注射器的后侧被打开，并且第一溶液通过小注射器的后侧被放入小注射器中。 小注射器通过大注射器的打开后侧插入大注射器。 双喷嘴（23）在第一旋转槽的外周具有第一旋转槽和第二旋转槽。 小注射器的喷嘴与双喷嘴的第一凹槽接触。 双喷嘴充满第二种解决方案。 活塞插入到大型注射器中，接合杆（32）从活塞的前侧沿活塞的纵向延伸。 接合杆与小型注射器按压体（31）螺纹结合，小型注射器按压体按压小型注射器的内部而旋转第一溶液。 活塞与大注射器按压体（33）螺纹连接，大注射器按压体按压大注射器内的第二溶液。
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22.发明授权리튬 고분자 전지용 술폰화 바인더, 이를 함유하는 전극조성물 및 이 전극 조성물을 함유하는 리튬 고분자 전지 失效用于锂聚合物电池的磺化粘合剂，含磺化粘合剂的电极组合物和含电极组合物的锂聚合物电池
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公开(公告)号：KR1020130131003A
公开(公告)日：2013-12-03
申请号：KR1020120054715
申请日：2012-05-23
Applicant: 전남대학교산학협력단
Abstract: The present invention relates to a graphite nanofiber and a production method thereof. The production method of the graphite nanofiber comprises the steps of: mixing a carbon fiber precursor material and a solvent to obtain a mixed solution; adding a metal precursor and homogenizing the mixed solution; adding silicon oxide and homogenizing the mixed solution; producing fibers by electrospinning the homogenized mixed solution; and thermally treating the produced fibers. The graphite nanofiber produced by the method has a structure where graphite sheets are vertically arranged with respect to the nanofiber axis, and contains graphene, catalyst metal particles, and silicon compounds to be used for an electrode material of a solar cell or a secondary battery. [Reference numerals] (AA) Start;(BB) End;(S11) Mix a carbon fiber precursor material and a solvent to obtain a mixed solution;(S12) Add a metal precursor and firstly homogenize the mixed solution;(S13) Add silicon oxide and secondly homogenize the mixed solution;(S14) Produce fibers by electrospinning the homogenized mixed solution;(S15) Thermally treat the fibers;(S16) Obtain graphene-containing graphite nanofibers
Abstract translation: 石墨纳米纤维及其制造方法技术领域本发明涉及石墨纳米纤维及其制造方法。 石墨纳米纤维的制造方法包括以下步骤：将碳纤维前体材料和溶剂混合以获得混合溶液; 加入金属前体并均化混合溶液; 加入氧化硅并均化混合溶液; 通过电纺均匀混合溶液生产纤维; 并对所生产的纤维进行热处理。 通过该方法制造的石墨纳米纤维具有石墨片相对于纳米纤维轴垂直布置的结构，并且包含用于太阳能电池或二次电池的电极材料的石墨烯，催化剂金属颗粒和硅化合物。 （AA）开始（BB）结束;（S11）将碳纤维前体材料和溶剂混合，得到混合溶液;（S12）添加金属前体，首先使混合溶液均化;（S13）添加 氧化硅，二次均化混合溶液;（S14）静电纺丝均质混合液生产纤维;（S15）热处理纤维;（S16）获得含石墨烯的石墨纳米纤维
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Patent Agency Ranking
公开(公告)号：KR1020120005403A
公开(公告)日：2012-01-16
申请号：KR1020110067689
申请日：2011-07-08
Applicant: 전남대학교산학협력단
CPC classification number: H01M4/38 , B82Y30/00 , B82Y40/00 , C22C12/00 , C22C13/00 , C22C29/12 , C22C47/00 , C22C49/00 , D01D5/0007 , D01F1/10 , D01F9/14 , H01M4/0471 , H01M4/131 , H01M4/133 , H01M4/583 , H01M4/625 , Y10S977/948
Abstract: PURPOSE: A method for fabricating carbon nano fiber containing intermetallic compounds is provided to property control the size of the compounds and diameter of the fiber. CONSTITUTION: A method for fabricating carbon nano fiber containing intermetallic compounds comprises a step of adding two or more metal precursors to a carbon fiber precursor material to prepare a fiber precursor composition; and a step of spinning the fiber precursor composition at 220-300°C by 0.1~10°C/minutes and performing thermal treatment at final temperature for 0.5-5 hours. The fiber precursor composition further contains polyvinyl pyrrolidone resin and oxygen atoms.
Abstract translation: 目的：提供一种制备含有金属间化合物的碳纳米纤维的方法，以控制化合物的尺寸和纤维的直径。 构成：制造含有金属间化合物的碳纳米纤维的方法包括将两种或更多种金属前体加入到碳纤维前体材料中以制备纤维前体组合物的步骤; 以及在220-300℃下将纤维前体组合物纺丝0.1〜10℃/分钟，在最终温度下进行热处理0.5〜5小时的工序。 纤维前体组合物还含有聚乙烯吡咯烷酮树脂和氧原子。
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公开(公告)号：KR100967697B1
公开(公告)日：2010-07-07
申请号：KR1020080033331
申请日：2008-04-10
Applicant: 전남대학교산학협력단 , 리트머스화학 주식회사
IPC: C07C233/04 , C07C231/02
Abstract: 본 발명은 저독성 폴리에스터계 분체도료의 경화제로 유용한 2-하이드록시 아마이드 화합물, 이의 제조방법 및 이를 경화제의 주성분으로 포함하는 폴리에스터 분체도료 조성물에 관한 것이다.
분체도료, 저독성, 폴리에스터, 경화제, β-HAA, 2-하이드록시-N,N,N',N'-테트라키스(2-하이드록시에틸)알킬아마이드, 2-하이드록시 아마이드-
公开(公告)号：KR100952945B1
公开(公告)日：2010-04-15
申请号：KR1020080020834
申请日：2008-03-06
Applicant: 전남대학교산학협력단
Abstract: 본 발명은 폴리아크릴로나이트릴(Polyacrylonitrile)과 망간전구체의 혼합 고분자 용액을 전기방사하여 나노섬유를 제조하고 이를 산화안정화, 탄화, 활성화한 나노사이즈의 포어를 갖는 흡착제에 관한 것이다. 보다 상세하게는 벤젠(Benzene), 톨루엔(Toluene), 크실렌(Xylene)등의 휘발성유기화합물(VOCs)을 효과적으로 흡착시킬 수 있는 섬유상 흡착제에 관한 것으로, 본 발명의 섬유상 흡착제는 평균직경이 200 ~ 400 nm이며, 비표면적이 853 내지 1300 m
2 /g, 미세세공의 직경인 약 5.6 내지 6.0 Å, 중대기공의 직경이 59 내지 91 Å이며, 종래 입상활성탄에 비하여 휘발성유기화합물의 흡착력이 매우 우수하다.
섬유상 흡착제, 휘발성유기화합물, 폴리아크릴로나이트릴, 망간전구체, 흡착, 혼합 전기방사-
公开(公告)号：KR1020090107837A
公开(公告)日：2009-10-14
申请号：KR1020080033331
申请日：2008-04-10
Applicant: 전남대학교산학협력단 , 리트머스화학 주식회사
IPC: C07C233/04 , C07C231/02
Abstract: PURPOSE: A 2-hydroxy amide compound is provided to suppress generation of micro holes and to improve mechanical strength and heat resistance. CONSTITUTION: A 2-hydroxy amide compound is represented by chemical formula 1, wherein A is linear or branched (C1~C7) alkylene; R1 ~ R4 are selected from linear or branched (C1~C7) alkyl in which at least one -OH is substituted. The 2-hydroxy amide compound is pure (S)-stereoisomer, pure (R)-stereoisomer or their mixture.
Abstract translation: 目的：提供2-羟基酰胺化合物以抑制微孔的产生并提高机械强度和耐热性。 构成：2-羟基酰胺化合物由化学式1表示，其中A是直链或支链（C1〜C7）亚烷基; R1〜R4选自其中至少一个-OH被取代的直链或支链（C1〜C7）烷基。 2-羟基酰胺化合物是纯的（S） - 立体异构体，纯（R） - 立体异构体或它们的混合物。
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公开(公告)号：KR1020090095725A
公开(公告)日：2009-09-10
申请号：KR1020080020834
申请日：2008-03-06
Applicant: 전남대학교산학협력단
CPC classification number: B01J20/262 , B01D53/72 , B01J20/0222 , B01J20/28004 , B01J20/28023 , B01J20/28066 , B01J20/3085 , B82Y40/00
Abstract: A fibrous adsorbent for VOC absorption using a fiber precursor composition and a manufacturing method thereof are provided to offer excellent adsorption capacity of volatile organic compounds rapidly. A manufacturing method of a fibrous adsorbent for VOC absorption using a fiber precursor composition includes the following steps of: producing a fiber precursor compound by adding a fibrous adsorbent for VOC absorption using a fiber precursor composition 0.1 ~ 5 weight% in polyacrylo nitrile resin dissolved liquid after dissolving polyacrylo nitrile resin in a solvent; producing the fiber by adding voltage of 20 ~ 30kV with the fiber precursor compound; stabilizing the fiber in air atmosphere for 0.5 ~ 3 hours; carbonizing the oxidized and stabilized fiber in the inert atmosphere or a vacuum state to temperature of 800 ~ 1000°C; and activating the carbonized fiber in the steam atmosphere.
Abstract translation: 提供了使用纤维前体组合物进行VOC吸收的纤维状吸附剂及其制造方法，能够迅速提供优异的挥发性有机化合物的吸附能力。 使用纤维前体组合物的VOC吸收用纤维吸附剂的制造方法包括以下步骤：通过在聚丙烯腈树脂溶解液中使用0.1〜5重量％的纤维前体组合物添加吸收VOC的纤维吸附剂来制造纤维前体化合物 将聚丙烯腈树脂溶解在溶剂中后， 用纤维前体化合物加入20〜30kV的电压生产纤维; 在空气中稳定纤维0.5〜3小时; 将氧化稳定的纤维在惰性气氛中或真空状态下碳化至800〜1000℃的温度; 并在蒸汽气氛中活化碳化纤维。
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