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公开(公告)号：KR1020110051520A
公开(公告)日：2011-05-18
申请号：KR1020090108143
申请日：2009-11-10
Applicant: 한국화학연구원
CPC classification number: Y02P20/143 , Y02W30/70 , Y02W30/703 , C08J11/12 , C08J11/04
Abstract: PURPOSE: An apparatus for recovering a styrene monomer is provided to prevent the yield of a styrene monomer from being lowered in a long time operation by consecutively discharging residues and to maximized the yield of styrene monomer according to use of twin screw pyrolysis reactor. CONSTITUTION: An apparatus for recovering a styrene monomer includes: a pyrolysis reactor(1) causing the melting and pyrolysis by receiving waste polystyrene; a steam collector(4) for collecting steam vapor created in the pyrolysis reactor; a heat exchanger(5) by liquefying the steam vapor collected in the steam collector and converting into oil; an oil reservoir(7) storing the oil liquefied in the heat exchanger; and a residue drain part(3) for discharging the residue generated after pyrolysis.
Abstract translation: 目的：提供一种用于回收苯乙烯单体的装置，以通过连续排出残留物来长期保持苯乙烯单体的收率降低，并根据双螺杆裂解反应器的使用使苯乙烯单体的收率最大化。 构成：用于回收苯乙烯单体的装置包括：热解反应器（1），其通过接收废聚苯乙烯进行熔融和热解; 用于收集在热解反应器中产生的蒸汽蒸汽的蒸汽收集器（4） 热交换器（5），其通过液化收集在蒸汽收集器中并转化成油的蒸汽蒸气; 存储在所述热交换器中液化的油的储油部（7） 和用于排出热解后产生的残留物的残渣排出部分（3）。
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公开(公告)号：KR100874351B1
公开(公告)日：2008-12-16
申请号：KR1020060127916
申请日：2006-12-14
Applicant: 한국화학연구원
IPC: C09J163/00
Abstract: An epoxy adhesive using a fatty acid ester solvent is provided to prevent emission of volatile organic compounds causing environmental pollution, and to obtain an adhesive for a flooring material having excellent biodegradability. An adhesive composition for a flooring material comprises an epoxy resin and is obtained by using a fatty acid ester compound as a solvent. An adhesive composition for the adhesion of a flooring material comprises: 4-36 parts by weight of an epoxy resin, 5-35 parts by weight of a tackifier; 5-70 parts by weight of a filler, 1-20 parts by weight of a fatty acid ester solvent; and 0.001-2 parts by weight of a dispersant.
Abstract translation: 提供使用脂肪酸酯溶剂的环氧粘合剂以防止挥发性有机化合物的排放，从而导致环境污染，并且获得具有优异生物降解性的地板材料的粘合剂。 用于地板材料的粘合剂组合物包含环氧树脂并且通过使用脂肪酸酯化合物作为溶剂获得。 一种用于粘合地板材料的粘合剂组合物，包含：4-36重量份环氧树脂，5-35重量份增粘剂; 5-70重量份填料，1-20重量份脂肪酸酯溶剂; 和0.001-2重量份的分散剂。
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公开(公告)号：KR100868236B1
公开(公告)日：2008-11-11
申请号：KR1020070063596
申请日：2007-06-27
Applicant: 한국화학연구원
CPC classification number: B01J20/3078 , B01J20/261 , B01J20/28061 , B01J20/28071 , B01J20/3007
Abstract: A method of manufacturing adsorber is provided to recycle pyrolysis residue obtained thermally decomposes waste polystyrene as a raw material of the adsorber, to reduce environment contamination problem by waste, to secure steadily the raw material of the adsorber and to save a production cost. A waste polystyrene melt is injected in a pyrolysis reactor and a styrene monomer and a pyrolysis residue are manufactured at 350 ~ 400 °C. The manufactured pyrolysis residue is heated at 900 ~ 1000 °C under an inert atmosphere and separated into a volatile component and a solid carbide. The solid carbide perform an activation reaction at 900 ~ 1000 °C by an oxidative gas.
Abstract translation: 提供一种制造吸附剂的方法，用于回收热分解废聚苯乙烯作为吸附剂原料的热分解残渣，以减少废物的环境污染问题，稳定地获得吸附剂的原料并节省生产成本。 在热解反应器中注入废聚苯乙烯熔体，在350〜400℃下制造苯乙烯单体和热解残渣。 将制得的热解残渣在惰性气氛下在900〜1000℃下加热，分离成挥发性成分和固体碳化物。 固体碳化物通过氧化气体在900〜1000℃下进行活化反应。
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公开(公告)号：KR100524698B1
公开(公告)日：2005-11-01
申请号：KR1020030022662
申请日：2003-04-10
Applicant: 한국화학연구원
IPC: C07C4/04
CPC classification number: C08J11/24 , C08J2367/04
Abstract: 본 발명은 열분해 신공정으로 폐폴리스틸렌으로부터 스틸렌 단량체를 회수하는 방법에 관한 것으로서, 더욱 상세하게는 폐폴리스틸렌을 200 ∼ 300 ℃ 온도에서 30분 ∼ 5 시간 동안 용융하여 불용성 물질을 제거하며 분자량을 조절하는 전처리 과정을 실시한 후, 스크루우를 통해 열분해 반응기에 투입하여 반응속도를 증가시킴으로써 고수율의 스틸렌 단량체를 회수하는 방법에 관한 것이다.
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公开(公告)号：KR100124971B1
公开(公告)日：1997-11-28
申请号：KR1019940009778
申请日：1994-05-04
Applicant: 한국화학연구원
IPC: B09B3/00
Abstract: The method of processing food waste from the kitchen proceeds in the steps of i) filtering food wastes, ii) heating and decomposing the wastes for 1-2 hrs. under the temp. of 50-275 deg. C and 0.2-59 atm. pressure, iii) cooling it down, iv) and separating it into solidity material and residual fluid. The residual fluid is treated by the solvent of carbon tetrachloride or dichloro methane so as to extract oil. The solidity material may be used as fuel.
Abstract translation: 从厨房处理食物废物的方法步骤如下：i）过滤食物废物，ii）加热和分解废物1-2小时。 在温度下 50-275度 C和0.2-59 atm。 压力，iii）冷却，iv）并将其分离成固体材料和残留液体。 残余流体用四氯化碳或二氯甲烷的溶剂处理，以提取油。 固体材料可以用作燃料。
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Patent Agency Ranking
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公开(公告)号：KR101519361B1
公开(公告)日：2015-05-13
申请号：KR1020130047309
申请日：2013-04-29
Applicant: 한국화학연구원
IPC: C07C67/333 , C07C69/96 , B01J23/72 , B01J4/00
Abstract: 본 발명은 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법에 관한 것으로서, 더욱 상세하게는 디메틸카보네이트 합성 수율을 향상시킬 수 있도록 한 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법에 관한 것이다.
즉, 본 발명은 기상 고정층 연속흐름 반응기에 메탄올, 일산화탄소, 산소, 불활성기체(알곤, 질소)를 동시에 주입하는 통상적인 반응시스템을 개선하되, 디메틸카보네이트 반응 메카니즘에 따라 원료 주입 라인을 변경하는 개선을 통하여, 메탄올, 산소, 불활성기체를 같이 주입하고 일산화탄소를 별도로 반응기 내부에 주입할 수 있도록 함으로써, 메탄올, 일산화탄소, 산소, 불활성기체(알곤, 질소)를 동시에 주입하는 통상적인 반응시스템에 비하여 디메틸카보네이트 합성 수율을 향상시킬 수 있는 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법을 제공하고자 한 것이다.-
公开(公告)号：KR1020140128646A
公开(公告)日：2014-11-06
申请号：KR1020130047309
申请日：2013-04-29
Applicant: 한국화학연구원
IPC: C07C67/333 , C07C69/96 , B01J23/72 , B01J4/00
Abstract: 본 발명은 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법에 관한 것으로서, 더욱 상세하게는 디메틸카보네이트 합성 수율을 향상시킬 수 있도록 한 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법에 관한 것이다.
즉, 본 발명은 기상 고정층 연속흐름 반응기에 메탄올, 일산화탄소, 산소, 불활성기체(알곤, 질소)를 동시에 주입하는 통상적인 반응시스템을 개선하되, 디메틸카보네이트 반응 메카니즘에 따라 원료 주입 라인을 변경하는 개선을 통하여, 메탄올, 산소, 불활성기체를 같이 주입하고 일산화탄소를 별도로 반응기 내부에 주입할 수 있도록 함으로써, 메탄올, 일산화탄소, 산소, 불활성기체(알곤, 질소)를 동시에 주입하는 통상적인 반응시스템에 비하여 디메틸카보네이트 합성 수율을 향상시킬 수 있는 메탄올의 산화성 카르보닐화 반응에 의한 디메틸카보네이트 제조 장치 및 방법을 제공하고자 한 것이다.Abstract translation: 本发明涉及碳酸二甲酯制造装置和碳酸二甲酯制造方法，其通过甲醇的氧化羰基化反应，更具体地说，涉及通过氧化羰基化能够改善合成的甲醇的碳酸二甲酯制造装置和碳酸二甲酯制造方法 碳酸二甲酯的产率。 本发明改进了同时将甲醇，一氧化碳，氧气和惰性气体（氩气和氮气）同时注入气相固定床连续流动反应器的常规反应系统，并提供了碳酸二甲酯制造装置和碳酸二甲酯制造方法 与通过注入甲醇，氧气和惰性气体同时注入甲醇，一氧化碳，氧气和惰性气体（氩气和氮气）的常规反应体系相比，通过甲醇的氧化羰基化能够提高碳酸二甲酯的合成产率 同时通过根据碳酸二甲酯的反应机理改变原料诱导线的改进，将一氧化碳分别注入反应器的内部空间。
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公开(公告)号：KR1020120053308A
公开(公告)日：2012-05-25
申请号：KR1020100114514
申请日：2010-11-17
Applicant: 한국화학연구원
CPC classification number: B01J29/072 , C07C67/40 , C07C69/96
Abstract: PURPOSE: Supported copper catalysts for manufacturing dimethyl carbonate based on the oxidative carbonylation of methanol are provided to improve the selectivity of the catalyst to the dimethyl carbonate and to reduce the corrosivity of the catalyst. CONSTITUTION: Supported copper catalyst is catalyst supporting copper ions and metallic ions selected from alkali metals and alkali earth metals in zeolite supports. The content of the copper ions is between 30 and 100 parts by weight and the content of the metallic ions is between 1 to 30 parts by weight based on 100 parts by weight of the zeolite supports. Dimethyl carbonate is obtained by implementing the reaction of methanol, carbon monoxide, and oxygen under the catalyst in a batch type liquid-based reactor or a continuous type gas-based reactor.
Abstract translation: 目的：提供基于甲醇氧化羰基化制备碳酸二甲酯的负载铜催化剂，以提高催化剂对碳酸二甲酯的选择性，并降低催化剂的腐蚀性。 构成：负载型铜催化剂是一种催化剂，它支持选择碱金属和碱土金属的沸石载体中的铜离子和金属离子。 相对于100重量份的沸石载体，铜离子的含量为30〜100重量份，金属离子的含量为1〜30重量份。 通过在间歇式液体反应器或连续型气体基反应器中通过在催化剂下实施甲醇，一氧化碳和氧气的反应来获得碳酸二甲酯。
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公开(公告)号：KR100802987B1
公开(公告)日：2008-02-14
申请号：KR1020060079172
申请日：2006-08-22
Applicant: 한국화학연구원
CPC classification number: B09B3/0016 , B01D11/02 , B09B5/00 , B29B17/00 , F23G5/00 , F23G2209/28
Abstract: An evaporation system is provided to recover a solvent easily and improve recovery ratio of the solvent within a short time as compared with an existing batch type evaporation tank by evaporating a waste styrofoam slurry dissolved by a solvent, thereby recovering the solvent. As a solvent recovery equipment comprising a slurry storage tank, an evaporator(11), a heat exchanger and a recovery tank, a recovery equipment of a solvent from a waste styrofoam slurry is characterized in that the evaporator comprises: a first cylinder(14) and a second cylinder(15) which have different diameters and are integrally formed at upper and lower sides; a slurry inlet(16) and a gas outlet(17) formed on an upper portion of the first cylinder; a residue outlet(18) formed on the bottom of the second cylinder; a spring type reactant guide(19) which is disposed concentrically within the second cylinder and extends longitudinally to increase retention time of a reactant; and a conical slurry guide(20) which is formed on a boundary part between the first and second cylinders, and which has a plurality of holes formed along the circumference of the guide so that a predetermined amount of slurry can stay in the holes, and the holes are spaced from one another in an equal distance, wherein the slurry can flow down uniformly as a whole along an inner wall surface of the second cylinder while the slurry is discharged downward through the plural holes.
Abstract translation: 提供蒸发系统，通过蒸发由溶剂溶解的废发泡胶浆料，与现有的批式蒸发罐相比，在短时间内容易地回收溶剂并提高溶剂的回收率，从而回收溶剂。 作为包含浆料储罐，蒸发器（11），热交换器和回收罐的溶剂回收设备，来自废发泡胶浆料的溶剂的回收设备的特征在于，所述蒸发器包括：第一气缸（14） 以及具有不同直径且在上侧和下侧一体形成的第二圆筒（15）; 浆料入口（16）和形成在第一气缸上部的气体出口（17）; 残留物出口（18），形成在所述第二气缸的底部; 弹簧型反应物引导件（19），其同心地设置在第二圆筒内并纵向延伸以增加反应物的保留时间; 以及形成在第一和第二气缸之间的边界部分上的锥形浆料引导件（20），并且具有沿着引导件的圆周形成的多个孔，使得预定量的浆料可以停留在孔中，以及 孔彼此间隔相等，其中当浆料通过多个孔向下排出时，浆料可以沿着第二圆柱体的内壁表面整体均匀地向下流动。
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