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公开(公告)号:DE4014977A1
公开(公告)日:1991-11-14
申请号:DE4014977
申请日:1990-05-10
Applicant: BASF AG
Inventor: GRAF HERMANN DR , STUEBINGER ADOLF DR , LORENZ KLAUS DR , SCHAFFER ORTWIN DR , STORK KARL DR
IPC: C08G14/02
Abstract: Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde can be obtained by (A) preparing a homogeneous reaction mixture in sulfuric acid from the phenolmonosulfonic acid and dihydroxydiphenyl sulfone in the molar ratio of from 3:1 to 10:1, with the proviso that the water content of the mixture is not more than 10% of the total weight of the components, and the mixture contains from 0.3 to 1.5 moles of sulfuric acid per mole of dihydroxydiphenyl sulfone, at from 100 DEG to 180 DEG C., (B) subsequently, at from 40 DEG to 90 DEG C., carrying out a precondensation with 1 to 2 moles of formaldehyde and 0.5 to 1.5 moles of urea per mole of phenol units present in aqueous medium, (C) partially neutralizing the reaction mixture, (D) adding to the partially neutralized reaction mixture 0 to 0.5 mole of phenol per mole of phenol units present and then 0.1 to 0.8 mole of formaldehyde per mole of phenol units then present, (E) further condensing at from 40 DEG to 90 DEG C., (F) shifting the pH of the reaction mixture into the neutral range and (G) subsequently acidifying with a weak acid.
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22.
公开(公告)号:AT15487T
公开(公告)日:1985-09-15
申请号:AT83101935
申请日:1983-02-28
Applicant: BASF AG
Inventor: GRAF HERMANN DR , ZEEH BERND DR , SCHAEFER PETER DR , POMMER ERNST-HEINRICH DR , AMMERMANN EBERHARD DR
IPC: A01N37/46 , A01N37/50 , A01N43/08 , A01N43/16 , C07D307/33 , C07D307/66 , C07D309/30 , C07C131/00
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公开(公告)号:DE3328770A1
公开(公告)日:1985-02-28
申请号:DE3328770
申请日:1983-08-10
Applicant: BASF AG
Inventor: GRAF HERMANN DR , RENTZEA COSTIN DR , RICHARZ WINFRIED DR , FROEHLICH HELMUT DR , AMMERMANN EBERHARD DR , POMMER ERNST-HEINRICH DR
IPC: A01N43/58 , C07D237/18 , A01N41/02
Abstract: Pyridazinone derivatives of the formula I (I) where R1 is hydrogen, unsubstituted or substituted alkyl, cycloalkyl, or unsubstituted or substituted phenyl or is carboxyl, hydroxymethyl or -CH2O-COR3, where R3 is alkyl, or is -CH2O[CH2CH2O]pR4, where R4 is alkyl or phenyl and p is 1, 2 or 3, R2 is phenyl, unsubstituted or substituted vinyl or 2-propenyl, X is halogen, m is 1 or 2 and n is 1, 2, 3 or 4, and fungicides containing these compounds.
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公开(公告)号:AT164841T
公开(公告)日:1998-04-15
申请号:AT93107116
申请日:1993-05-03
Applicant: BASF AG
Inventor: GRAF HERMANN DR , DEUKER ERNST DR , WOLFF STEFAN DR , SCHUSTER LUDWIG DR , WACK SERGE , HARDT RICHARD
IPC: C07D229/00 , C07D251/34 , C08G18/79
Abstract: The invention relates to a process for brightening polyisocyanates containing isocyanurate and uretdione groups, characterised in that the demonomerised polyisocyanates containing isocyanurate and uretdione groups are treated with oxygen.
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公开(公告)号:ES2070362T3
公开(公告)日:1995-06-01
申请号:ES91107074
申请日:1991-05-02
Applicant: BASF AG
Inventor: GRAF HERMANN DR , STUEBINGER ADOLF DR , LORENZ KLAUS DR , SCHAFFER ORTWIN DR , STORK KARL DR
IPC: C08G14/02
Abstract: Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde can be obtained by (A) preparing a homogeneous reaction mixture in sulfuric acid from the phenolmonosulfonic acid and dihydroxydiphenyl sulfone in the molar ratio of from 3:1 to 10:1, with the proviso that the water content of the mixture is not more than 10% of the total weight of the components, and the mixture contains from 0.3 to 1.5 moles of sulfuric acid per mole of dihydroxydiphenyl sulfone, at from 100 DEG to 180 DEG C., (B) subsequently, at from 40 DEG to 90 DEG C., carrying out a precondensation with 1 to 2 moles of formaldehyde and 0.5 to 1.5 moles of urea per mole of phenol units present in aqueous medium, (C) partially neutralizing the reaction mixture, (D) adding to the partially neutralized reaction mixture 0 to 0.5 mole of phenol per mole of phenol units present and then 0.1 to 0.8 mole of formaldehyde per mole of phenol units then present, (E) further condensing at from 40 DEG to 90 DEG C., (F) shifting the pH of the reaction mixture into the neutral range and (G) subsequently acidifying with a weak acid.
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公开(公告)号:DE4215746A1
公开(公告)日:1993-11-18
申请号:DE4215746
申请日:1992-05-13
Applicant: BASF AG
Inventor: GRAF HERMANN DR , DEUKER ERNST DR , WOLFF STEFAN DR , SCHUSTER LUDWIG DR , WACK SERGE , HARDT RICHARD
IPC: C07D229/00 , C07D251/34 , C08G18/79
Abstract: The invention relates to a process for brightening polyisocyanates containing isocyanurate and uretdione groups, characterised in that the demonomerised polyisocyanates containing isocyanurate and uretdione groups are treated with oxygen.
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公开(公告)号:GR3002486T3
公开(公告)日:1992-12-30
申请号:GR910401133
申请日:1991-08-16
Applicant: BASF AG
Inventor: GRAF HERMANN DR , SCHUETZ FRANZ DR , SAUTER HUBERT DR , AMMERMANN EBERHARD DR , POMMER ERNST-HEINRICH DR
IPC: A01N43/54 , A01N43/56 , C07D403/04
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公开(公告)号:AT66221T
公开(公告)日:1991-08-15
申请号:AT88108360
申请日:1988-05-26
Applicant: BASF AG
Inventor: GRAF HERMANN DR , SCHUETZ FRANZ DR , SAUTER HUBERT DR , AMMERMANN EBERHARD DR , POMMER ERNST-HEINRICH DR
IPC: A01N43/54 , A01N43/56 , C07D403/04
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公开(公告)号:DE3673101D1
公开(公告)日:1990-09-06
申请号:DE3673101
申请日:1986-09-04
Applicant: BASF AG
Inventor: GRAF HERMANN DR , WAHL PETER DR , RENTZEA COSTIN DR , SAUTER HUBERT DR , AMMERMANN EBERHARD DR , POMMER ERNST-HEINRICH DR
IPC: A01N43/90 , C07D487/04
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公开(公告)号:DE3718526A1
公开(公告)日:1988-12-22
申请号:DE3718526
申请日:1987-06-03
Applicant: BASF AG
Inventor: GRAF HERMANN DR , SCHUETZ FRANZ DR , SAUTER HUBERT DR , AMMERMANN EBERHARD DR , POMMER ERNST-HEINRICH DR
IPC: A01N43/54 , A01N43/56 , C07D403/04 , C09D5/14
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