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    ORGANOTEMPLATE-FREE SYNTHETIC PROCESS FOR THE PRODUCTION OF A ZEOLITIC MATERIAL OF THE CHA-TYPE STRUCTURE
    22.
    发明公开
    ORGANOTEMPLATE-FREE SYNTHETIC PROCESS FOR THE PRODUCTION OF A ZEOLITIC MATERIAL OF THE CHA-TYPE STRUCTURE 审中-公开
    SYNTHENTISCHES过程而不有机模板剂制备具有CHA-施工沸石

    公开(公告)号：EP2776369A4

    公开(公告)日：2015-08-05

    申请号：EP12847478

    申请日：2012-11-09

    Applicant: BASF SE

    Inventor： MAURER STEFAN ,  JIN HANPENG ,  YANG JEFF ,  MÜLLER ULRICH

    IPC: C01B39/46 ,  B01J29/70 ,  B01J29/85 ,  C01B39/54

    CPC classification number: B01J29/7015 ,  B01J2229/186 ,  C01B39/46

    Abstract: The present invention relates to an organotemplate-free synthetic process for the production of a zeoiitic material having a CHA-type framework structure comprising YO2, X2O3, and optionally comprising Z2O5, wherein said process comprises the steps of: (1 ) providing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and seed crystals having a CHA framework structure, wherein the CHA framework structure of the seed crystals comprises YO2, X2O3, and optionally comprises Z2O5; and (2) crystallizing the mixture obtained in step (1 ); wherein Y is a tetravaient element, X is a trivalent element, and Z is a pentavalent element, wherein optionally one or more sources for Z2O5 are further provided in step (1 ), and wherein if the CHA framework of the seed crystals does not contain Z2O5, the seed crystals then have a Y02 : X2O3 molar ratio of 5 or greater than 5.

    BIMENTAL-EXCHANGEDZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USETHEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx
    25.
    发明公开
    BIMENTAL-EXCHANGEDZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USETHEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx 审中-公开
    BIMETALL-AUSGETAUSCHTER ZEOLITH-BETA AUS ORGANOTEMPLATE-FREIER SYNTHESE UND VERWENDUNG DAVON IN DER SELKKTIVEN KATALYTISCHEN NOX-REDUKTION

    公开(公告)号：EP3097054A4

    公开(公告)日：2017-08-30

    申请号：EP14877063

    申请日：2014-12-30

    Applicant: BASF SE ,  TOKYO INST TECH

    Inventor： FEYEN MATHIAS ,  MAURER STEFAN ,  MÜLLER ULRICH ,  BAO XINHE ,  ZHANG WEIPING ,  DE VOS DIRK ,  GIES HERMANN ,  XIAO FENG-SHOU ,  YOKOI TOSHIYUKI ,  YILMAZ BILGE

    IPC: B01J29/76 ,  B01D53/94 ,  B01J29/00 ,  C01B39/00

    CPC classification number: B01D53/9418 ,  B01D2255/20738 ,  B01D2255/20761 ,  B01D2255/502 ,  B01J29/7615 ,  B01J37/0203 ,  B01J37/04 ,  B01J37/30 ,  B01J2229/183 ,  B01J2229/186 ,  B01J2229/34 ,  C01B39/026 ,  C01B39/46

    Abstract: The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO2 and X2O3, wherein said process comprises the steps of (1) preparing a mixture comprising one or more sources for YO2 and one or more sources for X2O3; (2) crystallizing the mixture obtained in step (1); (3) subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu; and (4) subjecting the Cu ion-exchanged zeolitic material obtained in step (3) to an ion-exchange procedure with Fe; wherein Y is a tetravalent element, and X is a trivalent element, wherein the mixture provided in step (1) and crystallized in step (2) further comprises seed crystals comprising one or more zeolitic materials having a BEA-type framework structure, and wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as a structure-directing agent, as well as to the zeolitic material having a BEA frame work structure per se, and to its use, in particular in a method for the treatment of NOx by selective catalytic reduction (SCR).

    Abstract translation: 本发明涉及生产具有包含YO 2和X 2 O 3的BEA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）制备包含一种或多种YO 2源和一种或多种 X2O3来源; （2）使步骤（1）中获得的混合物结晶; （3）使步骤（2）中获得的具有BEA型骨架结构的沸石材料与Cu进行离子交换程序; （4）将步骤（3）中获得的Cu离子交换沸石材料与Fe进行离子交换程序; 其中Y是四价元素，并且X是三价元素，其中步骤（1）中提供并在步骤（2）中结晶的混合物还包含含有一种或多种具有BEA型骨架结构的沸石材料的晶种，并且其中 在步骤（1）中提供并在步骤（2）中结晶的混合物不含有作为结构导向剂的有机模板以及具有BEA框架结构本身的沸石材料，特别是其用途 在通过选择性催化还原（SCR）处理NOx的方法中。

    SYNTHESIS OF ZEOLITIC MATERIALS USING N,N-DIMETHYL ORGANOTEMPLATES
    28.
    发明公开
    SYNTHESIS OF ZEOLITIC MATERIALS USING N,N-DIMETHYL ORGANOTEMPLATES 审中-公开
    沸石材料的合成使用N，N-二甲基有机模板

    公开(公告)号：EP2753579A4

    公开(公告)日：2015-08-19

    申请号：EP12830164

    申请日：2012-09-06

    Applicant: BASF SE

    Inventor： YILMAZ BILGE ,  BERENS ULRICH ,  SWAMINATHAN VIJAY NARAYANAN ,  MÜLLER ULRICH ,  IFFLAND GABRIELE ,  SZARVAS LASZLO

    IPC: C01B39/02 ,  B01J29/70 ,  C01B39/04 ,  C01B39/10 ,  C01B39/54

    CPC classification number: C01B39/48 ,  B01J29/7015

    Abstract: A process for the preparation of a zeolitic material having a structure comprising YO2 and X2O3 is provided, wherein said process comprises the steps of ( 1 ) providing a mixture comprising one or more ammonium compounds of which the ammonium cation has the formula (I): [R1R2NR3R4+(I) and further comprising one or more sources for Y02 and one or more sources for X2O3; (2) crystallizing the mixture provided in step ( 1 ); wherein Y is a tetravalent element, and X is a trivalent element, and wherein the ammonium compounds are preferably derivatized or underivatized N,N-dimethylpyrrolidinium compounds, Nu,Nu-dimethylpiperidinium compounds, Nu,Nu-dimethylhexahydroazepinium compounds, and mixtures thereof, and wherein the molar ratio of ammonium cation having the formula (I) to Y in the mixture provided in step (1) and crystallized in step (2) is equal to or greater than 0.25.

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