METHOD FOR REMOVING FORMIC ACID FROM A TRIOXANE-CONTAINING MIXTURE
    1.
    发明申请
    METHOD FOR REMOVING FORMIC ACID FROM A TRIOXANE-CONTAINING MIXTURE 审中-公开
    从三氧化物混合物中去除抗酸的方法

    公开(公告)号:WO2009027434A2

    公开(公告)日:2009-03-05

    申请号:PCT/EP2008061222

    申请日:2008-08-27

    CPC classification number: C07D323/06

    Abstract: The invention relates to a method for removing formic acid from a mixture that contains formaldehyde, trioxane, water and formic acid, by distillation. According to said method, at least one tertiary amine and/or an imine or a mixture thereof capable of deprotonation and conversion to a salt is added, prior to or during distillation, to the mixture in a catalytic amount or in an amount sufficient to form the salt with the entire amount of formic acid, and the formic acid/amine salt is removed in a liquid phase in the distillation sump.

    Abstract translation: 在对甲酸从甲醛,三恶烷,水和通过蒸馏甲酸含酸混合物中分离的方法进行之前的混合物中使用,或者在蒸馏过程中,至少一种叔胺和/或亚胺或它们的混合物,所述去质子的甲酸,并在 盐以催化量或足以与总量的甲酸盐化的量存在,并且将所形成的甲酸 - 胺盐在蒸馏塔底物中以液相排出。

    4.
    发明专利
    未知

    公开(公告)号:AT435854T

    公开(公告)日:2009-07-15

    申请号:AT05715706

    申请日:2005-03-03

    Applicant: BASF SE

    Abstract: Process for preparing ionic compounds comprising cations containing quaternary sp2-hybridized nitrogen atoms, which comprises reacting compounds containing a double-bonded nitrogen atom with a dialkyl sulfate with participation of both alkyl groups of the dialkyl sulfate and, if appropriate, subjecting the resulting ionic compound containing sulfate anions to an anion exchange.

    PROCESS FOR SEPARATING TRIOXANE FROM A TRIOXANE/FORMALDEHYDE/WATER MIXTURE BY MEANS OF PRESSURE SWING RECTIFICATION

    公开(公告)号:CA2701827A1

    公开(公告)日:2009-04-16

    申请号:CA2701827

    申请日:2008-09-22

    Applicant: BASF SE

    Abstract: The invention describes a method for separating trioxane from a supply flow I of formaldehyde, trioxane, and water, wherein a) a supply flow I containing formaldehyde as the main component and trioxane and water as the secondary components, is provided, b) the supply flow, a return flow V, and a return flow VII containing formaldehyde as the main component and water and trioxane as the secondary components, are fed into a first distillation step and are distilled at a pressure of 0.1 to 2.5 bars, wherein a flow II containing formaldehyde as the main component and water as the secondary component, and a flow III containing trioxane as the main component and water and formaldehyde as the secondary components, and a flow X containing water, trioxane and formaldehyde, are obtained, c) the flow III, optionally after separating low boilers from the flow III in a low boiler separating step, is distilled in a second distillation step at a pressure of 0.2 to 17.5 bars, wherein the pressure in the second distillation step is higher than the pressure in the first distillation step by 0.1 to 15 bars, wherein a flow IV, substantially consisting of trioxane, and the return flow V containing trioxane as the main component and water and formaldehyde as the secondary components, are obtained, d) the flow IV is purified in at least one further trioxane distillation step at a head pressure of 0.5 to 2 bars, wherein purified trioxane is obtained as the lateral removal flow is obtained in the reinforcement part of the column, d) the flow X, and optionally a flow IX containing water as the main component, are fed into a third distillation step and distilled at a pressure of 1 to 10 bars, wherein a flow VI substantially consisting of water, and a return flow VII containing formaldehyde as the main component and water and trioxane as the secondary component, are obtained.

    7.
    发明专利
    未知

    公开(公告)号:AT416163T

    公开(公告)日:2008-12-15

    申请号:AT05777970

    申请日:2005-08-03

    Applicant: BASF SE

    Abstract: Process for preparing quaternary ammonium compounds by reacting the corresponding tertiary sp 3 -hybridized amine or sp 2 -hybridized imine with dimethyl sulfite, wherein the reaction is carried out (i) in the presence of an inorganic or organic protic acid having a pK a of from 1.8 to 14, measured at 25° C. in aqueous solution; and (ii) at a temperature of from 10 to 100° C.

    8.
    发明专利
    未知

    公开(公告)号:DE502004007160D1

    公开(公告)日:2008-06-26

    申请号:DE502004007160

    申请日:2004-07-03

    Applicant: BASF SE

    Abstract: The invention relates to a process for the extractive removal of phenols, alcohols, amines, phoshines, hydroxylamines, hydrazines, oximes, imines, water, carboxylic acids, amino acids, hydroxamic acids, sulfinic acids, sulfonic acids, peroxycarboxylic acids, phosphonous acids, phosphinous acids, phosphonic acids, phosphinic acids or phosphoric acids from aprotic solvents by means of ionic liquids of the formula [K]n+[A]n-, where n, [K]+ and An- are defined as in the description.

    SYNTHESIS OF ZEOLITIC MATERIALS USING N,N-DIMETHYL ORGANOTEMPLATES
    9.
    发明公开
    SYNTHESIS OF ZEOLITIC MATERIALS USING N,N-DIMETHYL ORGANOTEMPLATES 审中-公开
    沸石材料的合成使用N,N-二甲基有机模板

    公开(公告)号:EP2753579A4

    公开(公告)日:2015-08-19

    申请号:EP12830164

    申请日:2012-09-06

    Applicant: BASF SE

    CPC classification number: C01B39/48 B01J29/7015

    Abstract: A process for the preparation of a zeolitic material having a structure comprising YO2 and X2O3 is provided, wherein said process comprises the steps of ( 1 ) providing a mixture comprising one or more ammonium compounds of which the ammonium cation has the formula (I): [R1R2NR3R4+(I) and further comprising one or more sources for Y02 and one or more sources for X2O3; (2) crystallizing the mixture provided in step ( 1 ); wherein Y is a tetravalent element, and X is a trivalent element, and wherein the ammonium compounds are preferably derivatized or underivatized N,N-dimethylpyrrolidinium compounds, Nu,Nu-dimethylpiperidinium compounds, Nu,Nu-dimethylhexahydroazepinium compounds, and mixtures thereof, and wherein the molar ratio of ammonium cation having the formula (I) to Y in the mixture provided in step (1) and crystallized in step (2) is equal to or greater than 0.25.

    Un procedimiento para producir cuero

    公开(公告)号:ES2927983T3

    公开(公告)日:2022-11-14

    申请号:ES17729853

    申请日:2017-06-12

    Applicant: BASF SE

    Abstract: La presente invención se refiere a un proceso para producir cuero en el que se usa ácido metanosulfónico (MSA) en la etapa de decapado a un valor de pH alto, y el uso de MSA es para mejorar la calidad del producto de cuero final así como para mejorar la impacto ambiental del licor residual. (Traducción automática con Google Translate, sin valor legal)

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