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    NANOPARTICLE COMPOSITION AND METHODS OF MAKING THE SAME
    22.
    发明公开
    NANOPARTICLE COMPOSITION AND METHODS OF MAKING THE SAME 审中-公开
    纳米粒子组合物及其制备方法

    公开(公告)号：EP2506967A4

    公开(公告)日：2015-09-09

    申请号：EP10833706

    申请日：2010-06-17

    Applicant: LOCKHEED CORP

    Inventor： ZINN ALFRED A ,  LU PAUL P

    IPC: B01J23/72 ,  B22F1/00 ,  B22F9/24 ,  B82Y30/00 ,  C01B32/50 ,  C22B15/00

    CPC classification number: H01B1/22 ,  B22F1/0018 ,  B22F9/24 ,  B82Y30/00 ,  C22B15/0089 ,  Y10T428/2991

    Abstract: A method of fabricating copper nanoparticles includes heating a copper salt solution that includes a copper salt, an N,N-dialkylethylenediamine, and a C6-C18 alkylamine in an organic solvent to a temperature between about 30° C. to about 50° C.; heating a reducing agent solution that includes a reducing agent, an N,N-dialkylethylenediamine, and a C6-C18 alkylamine in an organic solvent to a temperature between about 30° C. to about 50° C.; and adding the heated copper salt solution to the heated reducing agent solution, thereby producing copper nanoparticles. A composition includes copper nanoparticles, a C6-C18 alkylamine and an N,N'-dialkylethylenediamine ligand. Such copper nanoparticles in this composition have a fusion temperature between about 100° C. to about 200° C. A surfactant system for the stabilizing copper nanoparticles includes an N,N'-dialkylethylenediamine and a C6-C18 alkylamine.

    ARTICLES CONTAINING COPPER NANOPARTICLES AND METHODS FOR PRODUCTION AND USE THEREOF
    23.
    发明公开
    ARTICLES CONTAINING COPPER NANOPARTICLES AND METHODS FOR PRODUCTION AND USE THEREOF 审中-公开
    随着对生产和使用铜纳米颗粒和方法第

    公开(公告)号：EP2694613A4

    公开(公告)日：2015-07-22

    申请号：EP12767418

    申请日：2012-03-04

    Applicant: LOCKHEED CORP

    Inventor： BEDWORTH PETER V ,  ZINN ALFRED A

    IPC: C09K5/14 ,  B22F1/00 ,  C22C9/00

    CPC classification number: C22C32/00 ,  B22F1/0018 ,  B22F3/02 ,  B22F3/20 ,  C09K5/00 ,  C09K5/14 ,  C22C9/00 ,  C22C32/001 ,  C22C32/0084 ,  H01B1/16 ,  H01B1/22 ,  H01L24/29 ,  H01L2224/838 ,  H01L2924/12042 ,  H01L2924/15747 ,  H01L2924/00

    Abstract: The present application relates to an article comprising a matrix material; and a plurality of copper nanoparticles in the matrix material that have been partially fused together; wherein the plurality of copper nanoparticles are less than about 20 nm in size, and the plurality of copper nanoparticles comprise a surfactant system comprising a bidentate diamine and one or more C6 - C18 alkylamines, wherein the article comprises about 10% to about 99.9% copper nanoparticles of the article by weight. The present application further relates to a method of joining two articles.

    Abstract translation: 制品含有在基体材料的铜纳米颗粒的基体材料和多元thathave已经至少部分熔合在一起进行说明。 铜纳米颗粒尺寸小于约20nm。 这种规模的铜纳米粒子成为温度融合在一起，并没有压力是比基体铜的低得多。 通常，熔化温度降低与增加施加压力和铜纳米颗粒的尺寸降低。 铜纳米颗粒的尺寸可以通过调节反应条件，包括，例如，表面活性剂体系，加入速率和温度而变化。 铜纳米颗粒thathave被至少部分熔合在一起可形成在基体材料的热传导渗滤通路。

    STABILIZED METAL NANOPARTICLES AND METHODS FOR PRODUCTION THEREOF
    28.
    发明专利
    STABILIZED METAL NANOPARTICLES AND METHODS FOR PRODUCTION THEREOF 未知

    公开(公告)号：SG192150A1

    公开(公告)日：2013-08-30

    申请号：SG2013056957

    申请日：2012-01-25

    Applicant: LOCKHEED CORP

    Inventor： ZINN ALFRED A

    Abstract: Processes for synthesizing metal nanoparticles, particularly copper nanoparticles, are described. The processes can involve reacting an insoluble complex of a metal salt with a reducing agent in a reaction mixture containing a primary amine first surfactant, a secondary amine second surfactant, and a diamine chelating agent third surfactant. More specifically, processes for forming copper nanoparticles can involve forming a first solution containing a copper salt, a primary amine first surfactant, a secondary amine second surfactant, and a diamine chelating agent third surfactant; allowing an insoluble complex of the copper salt to form from the first solution; combining a second solution containing a reducing agent with the insoluble complex; and forming copper nanoparticles from the insoluble complex. Such copper nanoparticles can be about 10 nm or smaller in size, more particularly about 3 nm to about 6 nm in size, and have a fusion temperature of about 200°C or lower.

    METAL NANOPARTICLES FORMED AROUND A NUCLEUS
    29.
    发明专利
    METAL NANOPARTICLES FORMED AROUND A NUCLEUS 未知

    公开(公告)号：SG11201502441SA

    公开(公告)日：2015-05-28

    申请号：SG11201502441S

    申请日：2013-09-26

    Applicant: LOCKHEED CORP

    Inventor： ZINN ALFRED A

    IPC: B22F9/20 ,  B32B5/16 ,  B82Y40/00

    Abstract: Metal nanoparticles and compositions derived therefrom can be used in a number of different applications. Methods for making metal nanoparticles can include providing a first metal salt in a solvent; converting the first metal salt into an insoluble compound that constitutes a plurality of nanoparticle seeds; and after forming the plurality of nanoparticle seeds, reacting a reducing agent with at least a portion of a second metal salt in the presence of at least one surfactant and the plurality of nanoparticle seeds to form a plurality of metal nanoparticles. Each metal nanoparticle can include a metal shell formed around a nucleus derived from a nanoparticle seed, and the metal shell can include a metal from the second metal salt. The methods can be readily scaled to produce bulk quantities of metal nanoparticles.

    NANOPARTICLE COMPOSITION AND METHODS OF MAKING THE SAME
    30.
    发明专利
    NANOPARTICLE COMPOSITION AND METHODS OF MAKING THE SAME 未知

    公开(公告)号：SG10201407670RA

    公开(公告)日：2014-12-30

    申请号：SG10201407670R

    申请日：2010-06-17

    Applicant: LOCKHEED CORP

    Inventor： ZINN ALFRED A ,  LU PAUL P

    IPC: C01B32/50

    Abstract: Nanoparticle Composition And Methods Of Making The Same Abstract A method of fabricating copper nanoparticies includes heating a copper salt solution that includes a copper salt, an N.N'-diaikylethylenediamine, and a C6-C18 alkylamine in an organic solvent to a temperature between about 30°C to about 50°C; heating a reducing agent solution that includes a reducing agent, an N,N'-dialkyiethylenediamine, and a C6-C18 alkylamine in an organic solvent to temperature between a about 30°C to about 50°C; and adding the heated copper salt solution to the heated reducing agent solution, thereby producing copper nanoparticies. A composition includes copper nanoparticies, a C6-C18 alkylamine and an N.N'-diaikyiethylenediamine iigand. Such copper nanoparticies in this composition have a fusion temperature between about 100°C to about 200°C. A surfactant system for the stabilizing copper nanoparticies includes an N.N'-dialkylethylenediamine and a C6-C18 alkylamine. Fig. 1 -16-

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