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    Method of producing amide or lactam
    27.
    发明专利
    Method of producing amide or lactam 审中-公开
    生产酰胺或乳酸菌的方法

    公开(公告)号：JP2012056845A

    公开(公告)日：2012-03-22

    申请号：JP2010198223

    申请日：2010-09-03

    Applicant: Chiba Univ ,  Ube Industries Ltd ,  国立大学法人 千葉大学 ,  宇部興産株式会社

    Inventor： SATO TOMOJI ,  HOSHINO HIDEAKI ,  SUGIMOTO TSUNEMI

    IPC: C07D227/087 ,  C07B61/00

    Abstract: PROBLEM TO BE SOLVED: To provide a method of producing an amide or a lactam according to the Beckmann rearrangement of an oxime compound, capable of producing the same at a high conversion and a high yield without producing a large amount of byproducts such as ammonium sulfate.SOLUTION: An oxime compound is rearranged in the presence of a compound represented by formula (1) in a solvent, i.e., a lactone to produce a corresponding amide or lactam (in the formula, R, Rand Reach independently represent a hydrogen atom, a halogen atom, an alkyl group, an alkyl group substituted with a halogen atom, an aryl group, an aralkyl group, a cycloalkyl group, a hydroxyl group, an aryloxy group, an alkoxy group substituted with an halogen atom, a mercapto group, a carboxyl group, a substituted oxycarbonyl group, an acyl group, an acyloxy group, a nitro group, a sulfone group, a cyano group, an amino group, or an oxyamino group; and L represents a leaving group).

    Abstract translation: 待解决的问题：提供一种根据肟化合物的Beckmann重排制备酰胺或内酰胺的方法，其能够以高转化率和高收率生产，但不产生大量的副产物，例如 作为硫酸铵。 解决方案：在溶剂（即内酯）中，在式（1）表示的化合物存在下，将肟化合物重排，生成相应的酰胺或内酰胺（式中，R SB POS =“POST” > 1 ，R 2 和R 3 各自独立地表示氢原子，卤素原子，烷基 被卤素原子，芳基，芳烷基，环烷基，羟基，芳氧基，被卤素原子取代的烷氧基取代的烷基，巯基，羧基，取代的氧羰基 酰基，酰氧基，硝基，砜基，氰基，氨基或氧基氨基; L表示离去基团）。 版权所有（C）2012，JPO＆INPIT

    Adsorbing material
    28.
    发明专利
    Adsorbing material 有权
    吸附材料

    公开(公告)号：JP2011218330A

    公开(公告)日：2011-11-04

    申请号：JP2010093024

    申请日：2010-04-14

    Applicant: Ube Industries Ltd ,  宇部興産株式会社

    Inventor： KAIISO KOJI ,  ABE MASANORI ,  SUGIMOTO TSUNEMI

    IPC: B01J20/26 ,  C02F1/28 ,  C08J9/26 ,  C09K3/00 ,  C09K17/18

    Abstract: PROBLEM TO BE SOLVED: To provide an adsorbing material that includes new porous polyamide particles and is excellent in adsorption efficiency and adsorption ability.SOLUTION: The adsorbing material includes the polyamide particle, wherein an appearance shape of the particle is substantially spherical and the particle having an outer surface with through pores and an interior with independent pores is spongy.

    Abstract translation: 要解决的问题：提供包含新的多孔聚酰胺颗粒的吸附材料，并且吸附效率和吸附能力优异。 解决方案：吸附材料包括聚酰胺颗粒，其中颗粒的外观形状基本上是球形的，具有通孔的外表面和具有独立孔的内部的颗粒是海绵状的。 版权所有（C）2012，JPO＆INPIT

    Method for producing amide or lactam
    29.
    发明专利
    Method for producing amide or lactam 审中-公开
    生产酰胺或乳酸菌的方法

    公开(公告)号：JP2011088883A

    公开(公告)日：2011-05-06

    申请号：JP2010040718

    申请日：2010-02-25

    Applicant: Chiba Univ ,  Ube Industries Ltd ,  国立大学法人 千葉大学 ,  宇部興産株式会社

    Inventor： SATO TOMOJI ,  HOSHINO HIDEAKI ,  SUGIMOTO TSUNEMI ,  KASHIWAGI KOICHI

    IPC: C07D225/02 ,  B01J27/10 ,  B01J31/02 ,  C07B61/00 ,  C07D201/04

    CPC classification number: Y02P20/52

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an amide or a lactam by which the amide or the lactam can be formed in high conversion and high yield without forming a large amount of byproducts such as ammonium sulfate in the method for producing the amide or the lactam by a Beckmann rearrangement reaction of an oxime compound. SOLUTION: The method for producing the amide or lactam includes rearranging the oxime compound in the presence of a compound represented by general formula (1) (wherein, R 1 , R 2 and R 3 are each independently hydrogen, halogen, alkyl, alkyl substituted with halogen, aryl, aralkyl, cycloalkyl, hydroxy, aryloxy, alkoxy substituted with halogen, mercapto, carboxy, substituted oxycarbonyl, acyl, acyloxy, nitro, sulfone, cyano, amino or oxyamino; and L is a leaving group) by using a nitrile compound or a mixture of the nitrile compound and an aliphatic hydrocarbon as a solvent to produce the corresponding amide or lactam. COPYRIGHT: (C)2011,JPO&INPIT

    Abstract translation: 待解决的问题：提供一种制备酰胺或内酰胺的方法，通过该方法可以以高转化率和高产率形成酰胺或内酰胺，而不形成大量的副产物如硫酸铵。 通过肟化合物的贝克曼重排反应生成酰胺或内酰胺。 解决方案：制备酰胺或内酰胺的方法包括在通式（1）表示的化合物的存在下重新排列肟化合物（其中，R 1 ，R / SB>和R SB 3各自独立地为氢，卤素，烷基，被卤素，芳基，芳烷基，环烷基，羟基，芳氧基，被卤素取代的烷氧基，巯基，羧基，取代的氧羰基，酰基 ，酰氧基，硝基，砜基，氰基，氨基或氧基氨基; L为离去基团），通过使用腈化合物或腈化合物和脂族烃作为溶剂的混合物来制备相应的酰胺或内酰胺。 版权所有（C）2011，JPO＆INPIT

    Method for separating sulfur component in organic solution
    30.
    发明专利
    Method for separating sulfur component in organic solution 审中-公开
    在有机溶液中分离硫组分的方法

    公开(公告)号：JP2011016765A

    公开(公告)日：2011-01-27

    申请号：JP2009163211

    申请日：2009-07-10

    Applicant: Ube Industries Ltd ,  宇部興産株式会社

    Inventor： MATSUMOTO HIROSHI ,  SUGIMOTO TSUNEMI

    IPC: C07D201/16 ,  C07D201/04 ,  C07D225/02

    Abstract: PROBLEM TO BE SOLVED: To efficiently separate a sulfur component from an organic solution containing the sulfur component and especially in a production of lactam by subjecting a cycloalkanone oxime to a Beckmann rearrangement using a sulfur compound such as thionyl chloride to efficiently separate the sulfur component from the reaction mixture.SOLUTION: The method for separating a sulfur component in an organic solution includes treating the organic solution containing the sulfur component with an aqueous alkali solution, namely, washing the organic solution containing the sulfur component with an aqueous alkali solution.

    Abstract translation: 要解决的问题：通过使用硫化合物如亚硫酰氯使环烷酮肟进行贝克曼重排，从而有效地将硫成分从含有硫成分的有机溶液中分离，特别是在内酰胺的生产中，以有效地将硫成分从 反应混合物。溶液：用于分离有机溶液中的硫成分的方法包括用碱水溶液处理含有硫成分的有机溶液，即用碱水溶液洗涤含有硫成分的有机溶液。

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